• 제목/요약/키워드: mixed casting

검색결과 96건 처리시간 0.025초

Fe계 나노결정립 분말과 페라이트 복합체의 전자파 흡수특성 (Electromagnetic Wave Absorption Behavior of a Fe-based Nanocrystalline Alloy mixed with a Ferrite Powder)

  • 구숙경;이민혁;문병기;송용설;손근용;박원욱
    • 한국분말재료학회지
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    • 제15권4호
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    • pp.292-296
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    • 2008
  • The electromagnetic (EM) wave absorption properties of the $Fe_{73}Si_{16}B_7Nb_3Cu_1$ nanocrystalline powder mixed with 5 to 20 vol% of Ni-Zn ferrites has been investigated in a frequency range from 100MHz to 10GHz. Amorphous ribbons prepared by a planar flow casting process were pulverized and milled after annealing at 425 for 1 hour. The powder was mixed with a ferrite powder at various volume ratios to tape-cast into a 1.0mm thick sheet. Results showed that the EM wave absorption sheet with Ni-Zn ferrite powder reduced complex permittivity due to low dielectric constant of ferrite compared with nanocrystalline powder, while that with 5 vol% of ferrite showed relatively higher imaginary part of permeability. The sheet mixed with 5 vol% ferrite powder showed the best electromagnetic wave absorption properties at high frequency ranges, which resulted from the increased imaginary part of permeability due to reduced eddy current.

Water-IsopropanoI 혼합물의 투과증발 분리를 위한 poly(vinyl alcohol)-phosphomoIybdic heteropolyacid 혼합막 (Mixed matrix membranes of poly(vinyl alcohol) loaded with phosphomolybdic heteropolyacid for the pervaporation separation of water-isopropanol mixtures)

  • ;최형우;문정미;박지혜;홍성표;탁태문
    • 한국막학회:학술대회논문집
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    • 한국막학회 2008년도 춘계 총회 및 학술발표회
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    • pp.51-57
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    • 2008
  • Mixed matrix membranes of poly(vinyl alcohol) (PVA), loaded with phosphomolybdic heteropolyacid (HPA) and crosslinked with glutaraldehyde have been prepared by the solution casting technique. Pervaporation (PV) experiments have been performed at $30^{\circ}C$ to separate water-isopropanol feed mixtures containing 10 to 40 wt.% of water. The membranes were characterized by DSC and DMTA to understand their thermal behavior and mechanical strength properties. At high content (i.e. 7 wt.% with respect to weight of PVA) of HPA, the mixed matrix membranes could extract water efficiently on the permeate side with a selectivity of 90,000 and a flux of 0.032 $kg/m^2h$ for 10 wt.% of water containing feed mixture (the lowest feed composition of water studied). Flux of the mixed matrix membranes decreased with increasing concentrations of HPA.

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다공성 세라믹스와 다공질층을 포함하는 적층체의 제조에 관한 연구;I. 기공구조 (Fabrication of Porous Ceramics and Multi-layered Ceramics Containing Porous Layers; I. Pore Structure)

  • 이해원;윤복규;송휴섭
    • 한국세라믹학회지
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    • 제31권9호
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    • pp.1044-1052
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    • 1994
  • Tape casting technique was successfully applied to produce porous ceramics and multi-layered ceramics containing porous layers, where spherical hollow polymer particles were introduced as pore precursors. In the presence of extreme differences in density and size between Al2O3 and pore precursor particles, hindered settling was effective in preventing segregation of component particles and packing behavior of mixed powders was improved through bimodal packing. There were two transitions in packing behavior of mixed powders. The first transition took place at 40~50 vol% pore precursor addition, where majority of pores changed from close to open pore state. The other transition occured at 60~70 vol% pore precursor addition, where pore precursor particles formed a continuous network structure.

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Polyethersulfone과 ZnO 나노입자로 조성된 혼합기질막의 제조와 특성 평가 (Preparation and Characterization of Mixed Matrix Membrane Consisting of Polyethersulfone and ZnO Nanoparticles)

  • 이승훈;이민수;염경호
    • 멤브레인
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    • 제26권6호
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    • pp.463-469
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    • 2016
  • Polyethersulfone (PES) 고분자 상변환막의 성능을 향상시키기 위해 PES 고분자에 나노 크기의 ZnO 무기입자를 함침시킨 혼합기질막(mixed matrix membrane)을 제조하고 특성을 평가하였다. PES-ZnO 혼합기질막은 ZnO 나노입자를 PES 대비 최대 0.375 wt%의 낮은 비율로 첨가시킨 PES-ZnO-NMP(N-methyl-1-pyrrolidone)로 이루어진 캐스팅 용액을 사용하여 상변환법을 통해 제조하였다. 제조된 혼합기질 막의 물성과 특성은 막의 단면구조 관찰, 접촉각 측정, 인장강도 측정, 순수 투과량 측정 및 BSA 단백질 용액의 한외여과 실험을 통해 평가하였다. 이 결과 혼합기질 막은 PES 고분자 matrix에 함유된 ZnO 나노입자로 인해 막의 친수성이 증가하여 막오염 발생이 억제되어 투과량이 증가하였다. ZnO 나노입자는 혼합기질막의 제조에 있어 막오염의 발생 억제와 투과량 증가에 유용하게 사용될 수 있는 무기물 첨가제임을 알 수 있다.

3DARModeler : 증강현실 환경 3D 모델링 시스템 (3DARModeler: a 3D Modeling System in Augmented Reality Environment)

  • 도반 트리엔;이정규;이종원
    • 한국게임학회 논문지
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    • 제9권5호
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    • pp.127-136
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    • 2009
  • 본 논문에서 3DARModeler 라는 증강현실 환경에서의 3D 모델링 시스템에 대해서 제시 한다. 이 시스템은 3D 객체(모델)를 만들기 위해 객체 호출, 텍스쳐 적용, 애니메이션, 광원추정, 그림자 등의 기능들이 포함된 간단한 3D Studio Max라고 볼 수 있다. 3DARModeler는 3D 모델을 만들기 위한 효과적이고 편리한 상호작용 방법들을 제시한다. 3DARModeler 시스템의 주사용자는 컴퓨터 그래픽, 모델링 기술에 관한 많은 지식을 갖추지 않은 비전문가들을 대상으로 한다. 사용자들은 기본 객체를 선택, 객체들의 속성 부여, 여러 객체들의 결합을 통하는 방법으로 사용자가 실세계에서 직접 모델링을 하는 것과 같이 간단하고 직관적인 방법의 모델링을 가능하도록 한다.

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Fe-(8.5~36.9) wt% Cr합금의 600~800℃, (N2,H2S,수증기)-혼합 가스분위기에서의 부식 (Corrosion of Fe-(8.5~36.9) wt% Cr Alloys at 600~800℃ in (N2, H2S, H2O)-Mixed Gases)

  • 김민정;이동복
    • 대한금속재료학회지
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    • 제50권3호
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    • pp.218-223
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    • 2012
  • Fe-(8.5, 18.5, 28.3, 36.9) wt% Cr alloys were corroded between 600 and $800^{\circ}C$ for up to 70 h in a 1 atm gas mixture that consisted of 0.0242 atm of $H_2S$, 0.031 atm of water vapor, and 0.9448 atm of nitrogen gas. Their corrosion resistance increased with an increment in the Cr content. The Fe-8.5%Cr alloy corroded fast, forming thick, fragile, nonadherent scales that consisted primarily of an outer FeS layer and an inner (Fe, Cr, O, S)-mixed layer. The outer FeS layer grew into the air by the outward diffusion of $Fe^{2+}$ ions, whereas the inner mixed layer grew by the inward diffusion of oxygen and sulfur ions. At the interface of the outer and inner scales, voids developed and cracking occurred. The Fe-(18.5, 28.3, 36.9)% Cr alloys displayed much better corrosion resistance than the Fe-8.5Cr alloy, because thin $Cr_2O_3$ or $Cr_2S_3$ scales formed.

무연 Cu-Zn-Sn 청동의 조직과 주조성에 미치는 Bi 및 Sb 첨가의 영향 (Influence of Bismuth and Antimony Additions on the Structures and Casting Properties of Lead-free Cu-Zn-Sn Bronze Castings)

  • 박흥일;박성익;김성규
    • 한국주조공학회지
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    • 제32권2호
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    • pp.91-97
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    • 2012
  • The effects of Bi and Sb additions on the microstructures and casting properties in lead-free Cu-Zn-Sn broze were investigated. (1) When only Bi was added to the bronze, Bi was precipitated on the ${\delta}$ phase of ${\alpha}$ dendrite cell boundary. When Bi and Sb were added together, Bi was precipitated on the ${\delta}_A$ which was the Sb-rich area in the ${\delta}$ phase. (2) The addition of Sb accelerated the formation of ${\delta}$ phase, and when Sb, Bi and Pb were added, Bi and Pb were precipitated as mixed solution in the ${\delta}_A$ phase. (3) The combined addition of Sb and Bi resulted in the suppression of shrinkage due to the complementary effects of the mass feeding of ${\alpha}$-dendrite cluster covered with ${\delta}$ phase and sealing of micro-shrinkage in the ${\delta}$ phase by solidification expansion of Bi.

용융탄산염형 연료전지의 전해질 매트릭스에 관한 연구 (Cold Rolling Process for the Matrix Fabrication of the Mcfc)

  • 박상길;노창주
    • 수산해양기술연구
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    • 제27권2호
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    • pp.125-131
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    • 1991
  • Electrolyte matrix fabrication process can be classifed as hot pressing, tape casting, callendering, electrophoretic deposition. however, these have limits in practice. Hot pressing is cumbersome method, because of careful heating and cooling. Furthermore, the perfected tile is so fragile that it is difficult to fit in a cell. Therefore this method is not adequate for mass production of the electrolyte matrix. Using electrophoretic deposition method, a very thin matrix can be made, but many attempts of the electrolyte embeding were found to be failure. Tape casting and callendering methods are employed in most of the matrix fabrication for the present. But these methods require lots of water as a solvent, so that coating of the LiAlO sub(2) with electrolyte is difficult. Recently, hot roll milling method has been developed and the perfected matrix was proved to be free from crack. The method, however, needs a roller to make a matrix and a perfected matrix is carefully striped off from the cooled roller. Therefore, this method requires a long time due to the cooling process. The author proposes a cold rolling process. On this method, heated slurry of the LiAlO sub(2) mixed with binder, is rolled with a cold roller. The heated slurry dose not adhere to the roller, since contacted hot slurry is rapidly solidified. Therefore fabrication speed is increased, without getting rid of merits of the hot rolling process.

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동결주조 다공질 뮬라이트 세라믹스의 제조와 석탄회의 재활용 (Freeze Cast Porous Mullite Ceramics and Recycling of Coal Fly Ash)

  • 김규헌;윤석영;박홍채
    • 한국재료학회지
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    • 제26권2호
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    • pp.61-66
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    • 2016
  • In order to fabricate porous mullite ceramics with controlled pore structure and improved mechanical strength, a freeze casting route has been processed using camphene mixed with tertiary-butyl alcohol (TBA) and coal fly ash/alumina as the solvent and the ceramic material, respectively. After sintering, the solidification characteristics of camphene and TBA solvent were evident in the pore morphology, i.e., dendritic and straight pore channels formed along the solidification directions of camphene and TBA ice, respectively, after sublimation. Also, the presence of microcracks was observed in the bodies sintered at $1500^{\circ}C$, mainly due to the difference in solidification volume change between camphene and TBA. The compressive strength of the sintered bodies was found generally to be dependent, in an inverse manner, on the porosity, which was mainly determined by the processing conditions. After sintering at $1300{\sim}1500^{\circ}C$ with 30~50 wt% solid loading, the resulting mullite ceramics showed porosity and compressive strength values in ranges of 83.8~43.1% and 3.7~206.8 MPa, respectively.

반응소결법으로 제조한 Al기 복합재용 Fe-Al합금 예비성형체의 특성평가 (Characteristic Evaluation of the Fe-Al Alloy Preform Fabrication by Reactive Sintering Process for the Al Matrix Composites.)

  • 최답천;박성혁;주형곤
    • 한국주조공학회지
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    • 제19권6호
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    • pp.493-500
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    • 1999
  • Squeeze casting was used for fabricating a light metal base composite having high strength and wearresistance. Reactive sintering was used to prepare the preform of Squeeze casting. To utilize Fe-Al intermetallic compounds and SiC particle as a reinforcement, there needs to prepare Fe-Al mixed powder at 50, 60, 70at.%Al, and add SiC powder to the above mixture at 4, 7, 16, 24wt.%. The prepared mixture with SiC was reactive sintered in a tube furnace at $660^{\circ}C$ to get a porous hybrid preform of intermetallic compound and SiC. The preform prepared above was placed in a metal mold, preheated at $660^{\circ}C$ AC4C matrix was injected into the mold with the temperature of the melt at $610^{\circ}C$ After these processes, 66MPa was applied to the mold for 5 minute to finish the whole procedure. The maximum reaction temperature was increased with the increased Al amount, but decreased with the increased SiC amount. The density of the preform was decreased with SiC amount increase in the compacts due to swelling of the preform. An optical microscope was applied to observe the micro structure and the dispersion of the reinforcements. To analyze phases, We utilized XRD, EDS. Hardness test were chosen to get the information of mechanical properties. There were no significant changes in micro structure between the composite and preform. However, it was shown that uniform dispersion of the reinforcers and complete infiltration of the melt into the preform were achieved through the procedure of the squeeze casting. It was observed that the hardness of the composite is decreased with increased SiC amount, resulting from the volumetric expansion of the preform.

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