• Journal of the Korean Society of Industry Convergence
• /
• v.4 no.1
• /
• pp.27-34
• /
• 2001

Refining of powder particles and their dissolution into the Al matrix during mechanical alloying(MA) were investigated by using X-ray diffraction(XRD) transmission electron microscopy (TEM) functions of alloy composition, milling time and ball to powder ratio(BPR). It is found that Ti particles less than 20nm are observed in a dark field image of mechanically alloyed Al-10wt%Ti whose XHD pattern exhibits no Ti peak. The observed change of lattice constant of AI indicates that about 1 wt%Ti can he solved in Al after MA for a long time, independent of alloy composition, milling time and BPR, suggesting that most of Ti particles arc retained in the Al matrix. It is concluded that the disappearance of XRD peaks in mechanically alloyed Al-10wt%Ti is not simply attributable to the dissolution of Ti into Al, but associated mainly with extreme refining and/or heavy straining of Ti Particles.

• Textile Coloration and Finishing
• /
• v.5 no.2
• /
• pp.134-138
• /
• 1993

Wool, silk and nylon 6 fabrics were treated with low-temperature plasma under atmospheric pressure of acetone/argon or helium/argon for 30 and 180 sec, and then dyed with leveling type acid dye, C.I. Acid Red 18 and milling type acid dye, C.I. Acid Blue 83. In spite of short time of the plasma treatment for thirty seconds, the color depth of wool fabrics was increased remarkably with both of the plasma gases, aceton/argon or helium/argon and with the kinds of dyes i.e., levelin type or milling type. But the atmosperic low-temperature plasmas did not increase the depth of silk and nylon 6 fabrics dyed with both of the acid dyes regardless of the teated time and plasma gases. It seems that low-temperature plasma by atmospheric-pressure discharge is effective for improvement of dyeing of wools as is the same way with the low-temperature plasma by glow discharge. The kinds of plasma gases and treated time did not influnce the depth of wool fabric pretreted with the atmosperic low-temperature plasmas.

• Journal of the Korean Society for Precision Engineering
• /
• v.13 no.9
• /
• pp.31-37
• /
• 1996

This Paper is concerned with effective signal identification method for tool breakage and micro chipping using discrete wavelet transform of feed motor current in milling operations. The wavelet transform uses an analyzing waveletfunction which is localized in both frequency and time domain to detect subtle time localized changes in input signals. The changing pattern of wavelet coefficient is continuously compared to detect tool breakage and micro chipping over one spindle revolution. The results indicate that the wavelet transform can identify tool failure with much greater sensi- tivity than the time domain monitoring and frequency domain monitoring such as FFT. Experimental results are presented to support the proposed scheme.

• Journal of Hydrogen and New Energy
• /
• v.10 no.1
• /
• pp.49-57
• /
• 1999

In order to study the effect of high energy ball milling on the $Mg_2Ni+Ni$, $Mg_2Ni+0.5Ni+0.5Al$ powders, we have investigated on the discharge properties, microstructures. The powder size of samples decreased as ball milling time. From the XRD results, the crystal structure of $Mg_2Ni+Ni$ mixed powders were changed to amorphous or nano-structure after 60hr ball milling. The discharge capacities of both $Mg_2Ni+Ni$ and $Mg_2Ni+0.5Ni+0.5Al$ powders increased, with increasing ballmilling time, the maximum capacity(342mAh/g) was shown for the 60 hrs ballmilled $Mg_2Ni+Ni$ sample. The capacity decreased drastically after a few charge-discharge cycles.

• Journal of Powder Materials
• /
• v.12 no.6 s.53
• /
• pp.387-392
• /
• 2005

The p-type semiconductor $Bi_2Te_3-Sb_2Te_3$ thermoelectric materials were fabricated by melting, milling and sintering process and their thermoelectric properties were characterized. The compound materials were ball-milled with milling time and the powders were sintered by spark plasma sintering process. The ball milled powders had equiaxial shape and approedmately $1\~3{\mu}m$ in size. The figure of meritz of sintered thermoelectric materials decreased with milling time because of lowered electrical resistivity. The thermoelectric properties of $Bi_2Te_3-Sb_2Te_3$ materials have been discussed in terms of electrical property with ball mill process.

• Journal of the Korean Academy of Esthetic Dentistry
• /
• v.9 no.1
• /
• pp.82-90
• /
• 2000

In esthetic dentistry, color and strength are basic requirements for the long-term success of the restorative materials. Several all ceramic systems have been introduced to esthetic dentistry recently. However, the inherent natures of ceramic material, the application of all ceramic system is mainly limited to single tooth restorations. With the improvement of material science, the alumina and zirconia/alumina composite power and block can be applied to fabrication of all ceramic bridges. The conventional inceram core fabrication takes time for sintering however, the shaping of block with a copy milling machine can reduce great amount of time. The block is easy to manipulate and prepare in any shape accurately. This clinical report demonstrates the application of all ceramic ante rior 3 unit bridge with a alumina block in CELAY system.

• Journal of Hydrogen and New Energy
• /
• v.22 no.4
• /
• pp.527-533
• /
• 2011

CNFs had been well addressed due to numerous promising applications in science and technology. Besides the same physicochemical properties of ordinary carbon materials such as active carbons and carbon black, they exhibit specific, e.g., tubular or fibrous structures, a large surface area, high electrical conductivity stability, as well as extremely high mechanical strengh and modulus, which make them a superior material for electrochemical capacitors. In this study, CNFs were pretreated by mechanical milling with different time in mortar and pestle. The milled CNFs were used as active material of electrode whose electrochemical property was tested to find physicochemical characterization variation. CNF electrode milled for 5 min has the highest electric capacitance. XPS spectrum were employed to explore changes in functional group induced from mechanical milling. Crystal size was calculated to analyze change of peak from different milling time by XRD. The CNF milled for 5 min has the largest crystal size and the highest electric capacitance.

• Proceedings of the KIEE Conference
• /
• 1997.11a
• /
• pp.305-307
• /
• 1997

Gd-doped $CeO_2$, ultrafine powders were synthesized by the glycine-nitrate process and then their sintering and electrical characteristics were analysed using the dilatometric and AC impedance measurements. In the dilatometric measurements green bodies from the synthesized powders after milling shrinked to about $1470^{\circ}C$ in appearance and then expanded thermally with the increase of the heating temperature, whereas those from the synthesized powders before milling continuously shrinked to the temperatures of $1600^{\circ}C$. It may be due to the change of the packing density of the synthesized powders by milling. In the AC impedance measurements, the electrical resistivity of the Gd-doped $CeO_2$ bodies from the as-milled powders, sintered at $1500^{\circ}C$ with the increase of the sintering time, showed the minimum value at the sintering time of 10h. The minimum total resistivity of the Gd-doped $CeO_2$ bodies sintered at $1500^{\circ}C$ for 10h seems to result from the lowest activation energy by the combination between the activation energies for the resistivities at the grain interior and grain boundary.

• Journal of Korea Foundry Society
• /
• v.11 no.6
• /
• pp.455-462
• /
• 1991

The formation of brittle intermetallic compound such as $VAl_3$ tends tp lower the toughness of V-Al alloys. Also, due to the high melting point of vanadium, it is difficult to make that alloy by previous ingot metallurgy method. To depress the technique has been adopted. The effect of particle size and milling time on the phase has been thoroughly studied. For mechanical alloying, SPEX mixed/mill has been used. The milling time and the composition of V and Al are varied to find the optimum condition of forming amorphous phase. The X-Ray Diffrection pattern, microstructure detection, microhandess test, experiments are carried out to analyze MA product. When the final step is reached, no lamellar-structure is detected. The steady state condition is observed after 8 hours and 10 hours milling for 15wt.%Al and 30wt.%Al alloy, respectively. The microhardness continuously increases up to 10 hours after then it remains constant.

• Journal of the Korean Ceramic Society
• /
• v.35 no.10
• /
• pp.1055-1060
• /
• 1998

The effects of particle size distribution have been investigated on the high frequency low loss Mn-Zn fer-rites. The particle size distribution was controlled by milling time. Zirconia ball and engineering plastic jar were employed to avoid iron contamination from the milling media. As increasing the milling time BET value was increased from 0.55 to 3.21m2/g and mean particle size was decreased from 2.1 $\mu\textrm{m}$ to 1.0$\mu\textrm{m}$ The large specific surface area of initial powder resulted in the high density of sintered core. However starting powders with high BET lead to inhomogeneous grain growth as well as poor electromagnetic pro-perties at sintering temperature above 1300$^{\circ}C$.