• Title/Summary/Keyword: milling time

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Micro-deformation behavior of Brittle Hf-based Metallic Glass during Mechanical Milling (기계적 합금화 공정에 의한 Hf계 비정질 분말의 미세변형거동 관찰)

  • Kim, Song-Yi;Lee, A-Young;Cha, Eun-Ji;Kwon, Do-Hun;Hong, Sung-Uk;Lee, Min-Woo;Kim, Hwi-Jun;Lee, Min-Ha
    • Journal of Powder Materials
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    • v.25 no.3
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    • pp.246-250
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    • 2018
  • In this study, we investigate the deformation behavior of $Hf_{44.5}Cu_{27}Ni_{13.5}Nb_5Al_{10}$ metallic glass powder under repeated compressive strain during mechanical milling. High-density (11.0 g/cc) Hf-based metallic glass powders are prepared using a gas atomization process. The relationship between the mechanical alloying time and microstructural change under phase transformation is evaluated for crystallization of the amorphous phase. Planetary mechanical milling is performed for 0, 40, or 90 h at 100 rpm. The amorphous structure of the Hf-based metallic glass powders during mechanical milling is analyzed using differential scanning calorimetry (DSC) and X-ray diffraction (XRD). Microstructural analysis of the Hf-based metallic glass powder deformed using mechanical milling reveals a layered structure with vein patterns at the fracture surface, which is observed in the fracture of bulk metallic glasses. We also study the crystallization behavior and the phase and microstructure transformations under isothermal heat treatment of the Hf-based metallic glass.

Correlation between Acoustic Intensity and Ground Particle Size in Alumina Ball Mill Process

  • Cho, Kyeong-Sik;Kim, Soo-Hyun;Lee, Young Hun
    • Journal of the Korean Ceramic Society
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    • v.55 no.3
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    • pp.275-284
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    • 2018
  • In the ball milling process of ceramic powders, according to economic considerations for industrial applications, it is very important to quickly determine the optimum process condition with the maximum grinding efficiency. However, it is still difficult to determine the optimum condition for a ball mill with respect to the various process parameters, such as the rotational speed and the milling time. Ball milling was carried out at the same starting conditions with given amounts of alumina powders, balls and water, and was conducted slower or faster or a critical rotational speed was just determined by observing the angular position of the slurry in a semi-translucent polyethylene laboratory container. With respect to the different rotational speeds, which were slower or faster than the critical rotational speed, the particle size distribution of the grained powders and the acoustic intensity caused by cascading of the balls led to various behaviors. From the results of the particle size distribution and the acoustic signal analysis in the ball milling, there was one rotational speed that made the finest milled powder with maximum acoustic intensity. As a result, there was a correlation between the ground particle size and the acoustic intensity, which yields the interpretation that it can be possible in-situ to determine the optimum condition of ball milling by acoustic signal without repeated measurement efforts.

Pysicochemical and Milling Characteristics of Paddy Rice with Harvesting Times (수확시기별 벼의 도정 및 이화학특성)

  • Kim, Sum-Lim;Song, Jin;Son, Jong-Rok;Hwang, Hung-Goo;Shin, Jin-Chul;Choi, Hae-Choon;Choi, Young-Keun;Min, Young-Koo;Kim, Ki-Jong
    • Applied Biological Chemistry
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    • v.44 no.3
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    • pp.179-184
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    • 2001
  • To investigate the effects of harvesting times on physicochemical and milling properties of rice, milling tests were performed applying laboratory milling systems. Milling and head rice yields were highest in rice harvested at the 45 days after heading at 76.49 and 94.43%, respectively. Milled rice grain harvested 45 days after heading showed the highest minimum viscosity, as shown in the amylogram curves, as well as the lowest consistency viscosity. Protein and amylose contents were highest in rice harvested at 35 days after heading, whereas the instrumental taste score was highest 45 days after heading.

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Comparison of rice flour properties of different cultivars using wet and dry milling processes

  • Park, Jiyoung;Lee, Seuk-Ki;Park, Hye-Young;Choi, Hye-Sun;Cho, Dong-Hwa;Han, Sang-Ik;Lee, Kyung Ha;Oh, Sea-Kwan
    • Proceedings of the Korean Society of Crop Science Conference
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    • 2017.06a
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    • pp.286-286
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    • 2017
  • We conducted to compare the characteristics of rice flours according to the different milling processes. Five rice varieties (Oryza sativa L.) with different amylose content were prepared by wet and dry milling processes. The moisture contents of wet-milled rice flours (WMR) was mostly three-time higher than those of dry-milled flours (DMR). Water absorption index (WAI), water solubility index (WSI) and swelling power (SP) increased in proportion to temperature ($50-90^{\circ}C$). WAI, WSI, SP of DMR showed higher value than those of WMR. Baeokchal (BOC) which is waxy rice cultivar was significantly high level of WSI. Pasting properties of DMR except BOC cultivar resulted in higher peak viscosity, trough viscosity, final viscosity and Setback. The levels of resistant starch in the four cultivars except Dodamssal (DDS) were under 1% irrespective of Milling processes, whereas the resistant starch contents of DMR and WMR in DDS was 9.18 and 6.27, respectively. Damaged starch content of WMR were less than those of DMR, moreover, negative correlation was observed between amylose content and damaged starch of rice cultivars. These results suggest that the properties of rice flour varied depending on the milling methods and varieties, and it could be a reference for selecting the appropriate processing purposes.

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The Physical Properties Variation of Grout Materials and Improvement of Grouting Effects on Application of High Performance Injection Equipment (고성능 주입장비의 적용에 따른 주입재의 물성변화 및 주입효과 증진에 관한 연구)

  • 천병식;김진춘;김백영
    • Journal of the Korean Geotechnical Society
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    • v.19 no.4
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    • pp.179-190
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    • 2003
  • The grout based on solution type makes it difficult to get the improvement of ground strength and the effefct of water curtain because it has lower strength and durability than suspension type. Nowadays, the technology of particle acceleration, that enhance the material permeability, such as grout based on solution type, and inexpensive grout, is being required. For these reasons, in this study, using wet milling system, we evaluated physical properties of manufactured factors such as water-cement ratio of particles before being milled, optimum milling capacity by controlling milling time and rpm, viscosity of materials, permeation coefficient, and unconfined compressive strength. Also, using micro wet milling apparatus which could manufacture ordinary Portland cement and high speed shear mix which could forcefully separate conglomerate particles in situ, we performed electrical resistivity investigation and falling head permeability tests to analyze differences of grouting effects. From these results, we found that the permeability of the applied equipment was much superior, and in the case of using high speed shear mixer, particles of grout material were well separated.

Micro EDM Milling Using Deionized Water as Dielectric Fluid (탈수이온수를 절연액으로 사용한 미세 방전 밀링)

  • Chung, Do-Kwan;Kim, Bo-Hyun;Chu, Chong-Nam
    • 한국신재생에너지학회:학술대회논문집
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    • 2005.06a
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    • pp.546-549
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    • 2005
  • Micro EDM milling using deionized water as dielectric fluid was investigated. After machining micro grooves using deionized water with different voltage. capacitance. and resistivity of deionized water, machining characteristics were investigated. The wear of a tool electrode and the machining time can be reduced by using deionized water instead of kerosene. Micro hemispheres were machined in deionized water and kerosene and their machining characteristics were compared.

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A Study on Preparation of Nano size cement particle by Mechanical method (기계적 방법에 따른 나노 시멘트 입자의 제조에 관한 연구)

  • Jo Byung-Wan;Park Jong-Bin
    • Proceedings of the Korea Concrete Institute Conference
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    • 2004.05a
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    • pp.216-219
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    • 2004
  • Due to the recent amazing achievements in nano technology. preparation of cement nano particles by mechanical method are examined to improve their properties. The experimental results show that the particle size after 3 hr milling were about 500nm. The SEM photographs of specimens also reveal that average sizes of cement particles are gradually decreased by milling time. And in the TG/DSC, influence of the alcohol is showed strongly. The value of TG of the crushed cement was larger than that of the non-crushed cement. That is also judged to be cause the alcohol.

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An Experimental Study on the Real-Time Tool Breakage Detection in teh Face Milling (정면밀링 가공시 실시간 공구파손검출에 관한 실험적 연구)

  • 김영일;사승윤;최영규;유봉환
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1994.10a
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    • pp.9-14
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    • 1994
  • The modern CNC machine require increasingly an exact monitoring and control of cutting process. They are to make final taret which construct full automation factories as unmanned system. In this study, we decided that we develop new techique to monitor and detect tool breakage on the machining operation using face milling machine with multi-point throwaway tips. The technology in which the tool is illuminated by an beam of Laser is used by image of tool fracture through CCD camera.

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