• Journal of Technologic Dentistry
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• v.23 no.1
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• pp.9-19
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• 2001

Microstructure and phase transformation of Ti-Ni-Cu alloy powders produced by using attrition milling method were studied. Mixed powders of Ti-(50-X)Ni-XCu ($X=0{\sim}20$ at%) in composition range were mechanically alloyed for maximum 20 hours by using SUS 1/4" ball in argon atmosphere. Ball to powder ratio was 50: 1 and impeller speed was 350rpm. Mechanically alloyed with attrition millimg method. powder was heat treated at the temperature up to $850^{\circ}C$ for 1 hour in the $10^{-6}$ torr vacuum. Ti-Ni-Cu alloy powders have been fabricated by attrition milling method. and then phase transformation behaviours and microstructual properties of the alloy powders were investigated to assist in improving the the high damping capacity of Ti-Ni-Cu shape memory alloy powders. The results obtained are as follows: 1. After heat treating of fully mechanically alloyed powder at $850^{\circ}C$ for 1hour. most of the B2 and B 19' phases was formed and $TiNi_3$ were coexisted. 2. The B 19' martensite were formed in Ti-Ni-Cu alloy powders whose Cu-content is less than 5a/o. where as the B19 martensite in those whose Cu-content is more than 10at%. 3. The powders of as-milled Ti-Ni-Cu alloys whose Cu-contents is less than 5at% are amorphous. whereas those of as-milled Ti-Ni-Cu alloys whose Cu-content is more than 10at% are crystalline. This means that Cu addition tends to suppress amorphization of Ti-Ni alloy powders.

• Korean Journal of Materials Research
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• v.26 no.3
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• pp.136-142
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• 2016

To study the dispersion factors of silica sol prepared from fumed silica powder, we prepared silica sol under an aqueous system using a batch type bead mill. The dispersion properties of silica sol have a close relationship to dispersion factors such as pH, milling time and speed, the size and amount of zirconia beads, the solid content of fumed silica, and the shape and diameter of the milling impellers. Especially, the silica particles in silica sol were found to show dispersion stability on a pH value above 7, due to the electrostatic repulsion between the particles having a high zeta potential value. The shape and diameter of the impellers installed in the bead mill for the dispersion of fumed silica was very important in reducing the particle size of the aggregated silica. The median particle size ($D_{50}$) of silica sol obtained after milling was also optimized according to the variation of the size and amount of the zirconia beads that were used as the grinding medium, and according to the solid content of fumed silica. The dispersion properties of silica sol were investigated using zeta potential, turbiscan, particle size analyzer, and transmission electron microscopy.

• Journal of Biosystems Engineering
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• v.25 no.1
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• pp.39-46
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• 2000

This work was conducted to study the operating characteristics of a grinding system designed to obtain fine rice husk ash powder. To find better utilizing of rice husk, a valuable by-product from rice production, once the rice husk was incinerated and the thermal energy was recovered from the furnace, the ash was fed and pulverized in the grinding system resulting a fine powder to be used as a supplementary adding material to the portland cement manufacturing . The rice husk ash grinding system consisted of a high speed centrifugal fan for the preliminary coarse milling and a dry-type stirred ball mill for the subsequent fine grinding . Total grinding time 9 5, 15, 30, 45 min), impeller speed (250, 500, 750 rpm) , and mixed ratio (4.8, 7.9, 14.9) were three operating factors examined for the performance of a stirred ball mill used for the fine grinding of ash. With the stirred ball mill used in this study, the minimum attianable mean diameter of rice husk ash powder appeared to be 2 ${\mu}{\textrm}{m}$. During the find grinding, the difference in specific surface area of powder showed an increase and the grinding energy efficiency decreased with the increase in total grinding time, impeller speed ,and mixed ratio. For the operating conditions employed , the resulting mean diameter of fine ash powder, specific energy input, and grinding energy efficiency were in the range of 1.79 --16.04${\mu}{\textrm}{m}$, 0.072-5.226kWh/kg, an d1.11-12.15$m^2$/Wh, respectively. Grinding time of 30 min , impeller speed of 750 rpm, and mixed ratio of 4.8 were chosen as the best operating conditions of the stirred ball mill for fine grinding . At these conditions, mean particle diameter of the fine ash, grinding energy efficiency, grinding throughtput, and specific energy input were 2.73${\mu}{\textrm}{m}$, 3.95$m^2$/Wh, 0.25kg/h, and 1.22kWh/kg, respectively.

• Journal of Powder Materials
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• v.8 no.4
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• pp.253-257
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• 2001

The effects of mechanical alloying conditions on the formation of Mn-sulfide powders were analyzed. Impeller rotating speed, lubricant coating and added amounts of process control agent(stearic acid) were selected as a process control factor. MnS compounds are synthesized in 3 hours by mechanical alloying at the alternative milling condition. Discontinuous rotating speed of 1200rpm for 4 minutes and 1000rpm for 1 minute shows more effects on the compound formation of MnS. After coating of lubricant on the wall, elementary Mn and sulfur were partially remained by mechanical alloying. The friction effects of the wall and grinding media on the powders are significantly important to form the compound of MnS.

• Transactions of the Korean Society of Machine Tool Engineers
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• v.15 no.3
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• pp.53-58
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• 2006

This study deals with the method of post-processing in the automatic tool path generation for 5-axis NC machining. The 5-axis NC machining cannot only cope with the manufacturing of complicated shapes, but also offers numerous advantages such as reasonable tool employment, great reduction of set-up process and so on. Thus 5-axis NC machining has been used for aircraft parts, mold and die as well as for complicated shapes such as impeller, propeller and rotor. However, most of the present CAM systems for 5-axis NC machining have limited functions in terms of tool collision, machine limits and post-processing. Especially 5-axis machine configurations are various according to the method which the rotational axes are adapted with the table and spindle. For that reason, In many cases the optimal numerical control (NC) data cannot be obtained or considerable time is consumed. To solve this problem, we applied a general post-processor for 5-axis NC machining. The validity of this post-processor should be experimentally confirmed by successfully milling to a helix shaped workpiece.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.10a
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• pp.370-374
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• 2005

This study deals with the method of post-processing in the automatic tool path generation for 5-axis NC machining. The 5-axis NC machining cannot only cope with the manufacturing of complicated shapes, but also offers numerous advantages such as reasonable tool employment, great reduction of set-up process and so on. Thus 5-axis NC machining has been used fur aircraft parts, mold and die as well as for complicated shapes such as impeller, propeller and rotor. However, most of the present CAM systems for 5-axis NC machining have limited functions in terms of tool collision, machine limits and post-processing. Especially 5-axis machine configurations are various according to the method which the rotational axes are adapted with the table and spindle. For that reason, in many cases the optimal numerical control (NC) data cannot be obtained or considerable time is consumed. To solve this problem, we applied a general post-processor fur 5-axis NC machining. The validity of this post-processor should be experimentally confirmed by successfully milling to a helix shaped workpiece.

• Korean Journal of Materials Research
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• v.5 no.6
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• pp.627-632
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• 1995

W-Cu composites utilize the high electrical conductivity of copper and arc erosion resistance of tungsten to provide properties better suited to electrical contact applications than either tungsten or copper alone. W-Cu composite materials were milled in an attritor with an impeller speed of 300rpm for various milling times. The milled powders were compacted at 300MPa into cylinders, 16m in diameter, and approximately 4m high. Sintering was performed in dry H$_2$at temperature ranging from 1200$^{\circ}C$ to 1400$^{\circ}C$. Samples were sectioned and were polished for scanning electron microscopy (SEM) of microstructures. Homogeneous W-Cu composites were formed after 10 hours mechanical alloying and could be attained 99% density at 1330$^{\circ}C$. As mechanical alloying time increased, Fe-concentration was increased linearly. Intermetallic compound formation interupted the growth of W particles Increased hardness.