• Title/Summary/Keyword: microwave-processing

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Microwave Irradiation, A New Processing Method of Aconiti Tuber (마이크로파를 이용한 부자의 새로운 수치방법)

  • Yun-Choi, Hye-Sook;Yoo, Kyung-Sook;Lee, Sook-Youn;Lee, Youn-Hee;Kwak, Wie-Jong;Kim, Ki-Hyup
    • Korean Journal of Pharmacognosy
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    • v.21 no.4
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    • pp.284-289
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    • 1990
  • Crude Aconiti Tubers were irradiated with microwave for 5 or 10 min with or without $NaHCO_3$. Ten min-irradiation reduced the contents of aconitine and mesaconitine to the level of those of commercially available processed Aconiti tuber power which is prepared with the high pressure-high temperature technique. The contents of benzoylaconine of the 10 min-irradiated Aconiti tubers were also comparable to those of commerciallized processed Aconiti tuber powder. However, irradiation with 1% $NaHCO_3$ soln. resulted in the drastic reduction of all the three above alkaloids.

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Microwave Dielectric Properties of $Mg_4Nb_2O_9$ Ceramics Produced by a Sol-gel Route (솔-젤법에 의해 제조한 $Mg_4Nb_2O_9$ 세라믹스의 마이크로파 유전특성)

  • Lim, Sung-Woo;Lee, Sang-Wook;Bang, Jae-Cheol
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.281-282
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    • 2007
  • $Mg_4Nb_2O_9$ (MN) ceramics have been prepared by a sol-gel method. The powder characteristics, phase evolution, and microwave dielectric properties of the MN were investigated in various processing conditions such as sol-gel compositions, calcination, and sintering temperatures. A Qxfo value of 111,717 GHz with a ${\varepsilon}_r$ of 10.59 and a ${\tau}_f$ of $+1.736\;ppm/^{\circ}C$ was obtained after sintering at $1300^{\circ}C$ for 5 h.

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Fabrication of Microwave PECVD with Linear Antenna for large-scale deposition processing, and Analysis of Ar plasma characteristics using Electrostatic Probe and Temperature Characteristics (대면적 증착용 선형 초고주파 플라즈마 장치 제작 및 정전 탐침법을 이용한 Ar 플라즈마 특성 분석과 온도 특성 분석)

  • Han, Moon-Ki;Seo, Kwon-Sang;Kim, Dong-Hyun;Lee, Ho-Jun
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.64 no.3
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    • pp.422-428
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    • 2015
  • A 2.45GHz microwave plasma source with a linear antenna has been developed for low temperature large scale deposition processing. Microwave power is transmitted through WR340 waveguide and a copper rod, linear antenna, is located in a quartz tube. The power matching is effectively achieved by a linear antenna is located at ${\lambda}_g/4$ or $3{\lambda}_g/4$ from the end of WR340 waveguide. The Ar plasma was generated along the surface of quartz tube and a clear standing wave pattern with nearly 10cm wavelength was observed at Ar pressure of 200mTorr and 200W input power. The electron density and electron temperature were investigated by using the electrostatic probe. The electron density and electron temperature were highly measured near the surface of quartz tube. Ar plasma density along the quartz tube is mostly uniform despite standing wave set-up and antenna of long length. A uniform temperature was measured at 10~40cm distance from the end quartz tube and 5cm distance from the surface of quartz tube.

The microwave dielectric properties of $Bi_{(1-x)}Tm_xNbO_4$ (마이크로파 유전체 $Bi_{(1-x)}Tm_xNbO_4$의 유전특성)

  • Hwang, Chang-Gyu;Jang, Gun-Eik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07b
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    • pp.662-665
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    • 2002
  • The microwave dielectric properties and the microstructures of $Tm_2O_3$-modified $BiNbO_4$ ceramics were investigated. $Bi_{(1-x)}Tm_xNbO_4$ ceramics combined with orthorhombic and triclinic phases were identified at sintering temperatures of $920{\sim}960^{\circ}C$. The apparent density decreased slightly with the increasing Tm content. Regardless of the Tm content the dielectric constant $(\varepsilon_r)$ of all compositions except x=0.1 in $Bi_{(1-x)}Tm_xNbO_4$ ceramics saturated at the range of 42~44. The $Q{\times}f_0$ values of 6,000-12,000(GHz) were obtained for all compositions when the sintering temperatures were in the range of $920{\sim}960^{\circ}C$. The temperature coefficient of the resonant frequency$(\tau_f)$ can be also adjusted with increasing the amount of the doped Tm from a positive value of $+15ppm/^{\circ}C$ to a negative value of $-20ppm/^{\circ}C$. The $Bi_{(1-x)}Tm_xNbO_4$ ceramics can be possibly applied to multilayer microwave devices with low processing temperatures.

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SPATIO-SPECTRAL MAXIMUM ENTROPY METHOD: II. SOLAR MICROWAVE IMAGING SPECTROSCOPY

  • Bong, Su-Chan;Lee, Jeong-Woo;Gary Dale E.;Yun Hong-Sik;Chae Jong-Chul
    • Journal of The Korean Astronomical Society
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    • v.38 no.4
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    • pp.445-462
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    • 2005
  • In a companion paper, we have presented so-called Spatio-Spectral Maximum Entropy Method (SSMEM) particularly designed for Fourier-Transform imaging over a wide spectral range. The SSMEM allows simultaneous acquisition of both spectral and spatial information and we consider it most suitable for imaging spectroscopy of solar microwave emission. In this paper, we run the SSMEM for a realistic model of solar microwave radiation and a model array resembling the Owens Valley Solar Array in order to identify and resolve possible issues in the application of the SSMEM to solar microwave imaging spectroscopy. We mainly concern ourselves with issues as to how the frequency dependent noise in the data and frequency-dependent variations of source size and background flux will affect the result of imaging spectroscopy under the SSMEM. We also test the capability of the SSMEM against other conventional techniques, CLEAN and MEM.

Low Temperature Sintering of $Mg_{3-x}Co_x(VO_4)_2$ Microwave Dielectric Ceramics for LTCC Applications (저온소결 $Mgx_{-3}Cox(VO_4)_2$ 세라믹스의 마이크로파 유전특성)

  • Lee, Ji-Hun;Bang, Jae-Cheol
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.220-223
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    • 2005
  • We studied the effect of composition, processing, and sintering temperature on the microwave properties of $Mg_{3-x}Co_x(VO_4)_2$ system which is applicable to LTCC. When $Mg_{3-x}Co_x(VO_4)_2$ was fabricated by solid-state reaction process and sintered at the temperature range of $800\sim910^{\circ}C$, it was found that the optimum composition of x was 2 at which microwave properties of 910$^{\circ}C$-sintered one were as follows: $Q\times f_0\sim55,200GHz$ and $\varepsilon_r\sim10$. When $(MgCo_2)(VO_4)_2$ was fabricated by sol-gel process and sintered at 800$^{\circ}C$, $Q\timesf_0$was 34,400GHz which is much high compared to those fabricated by solid-state reaction process at the same sintering temperature.

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A Study on the Carbonization and Strengthening of PAN Fiber by Microwave Plasma (마이크로웨이브 플라즈마를 이용한 탄화공정 및 PAN fiber의 강도 향상에 관한 연구)

  • Choi, Ji-Sung;Joo, Jung-Hoon;Lee, Hun-Su
    • Journal of the Korean institute of surface engineering
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    • v.45 no.2
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    • pp.89-94
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    • 2012
  • A study to replace a high temperature thermal carbonization process with microwave plasma process is carried for PAN fiber as a starting material. Near atmospheric pressure microwave plasma (1 Torr~45 Torr) was used to control to get the fiber temperature up to $1,000^{\circ}C$. Even argon is an inert gas, its plasma state include high internal energy particles; ion (15.76 eV) and metastable (11.52 eV). They are very effective to lower the necessary thermal temperature for carbonization of PAN fiber and the resultant thermal budget. The carbonization process was confirmed by both EDS (energy dispersive spectroscopy) of plasma treated fibers and OES (optical emission spectroscopy) during processing step as a real time monitoring tool. The same trend of decreasing oxygen content was observed in both diagnostic methods.

Microwave Dielectric Properties of Low-temperature Sintered $MgCo_2(VO_4)_2$ Ceramics Synthesized by Sol-Gel process (졸-겔 공정에 의해 제조된 저온소결 $MgCo_2(VO_4)_2$ 세라믹스의 마이크로파 유전특성)

  • Lee, Ji-Hun;Bang, Jae-Cheol
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.288-289
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    • 2006
  • We studied the effect of sol-gel processing and sintering temperature on the microwave properties of $MgCo_2(VO_4)_2$ system(MCV) which is applicable to LTCC(low-temperature cofired ceramics). The MCV was synthesized by sol-gel process using solution that contains precursor molecules for Mg, Co, and V. SEM analysis shows that the average particle size is ${\sim}1{\mu}m$ and size distribution is very uniform compared to the one prepared by conventional solid-state reaction process. Highly dense samples were obtained at the sintering temperature range of $750^{\circ}C{\sim}930^{\circ}C$. The maximum $Q{\times}f_0$ value of 55,700GHz, dielectric constant(${\varepsilon}_r$) of 10.41 and temperature coefficient(${\tau}_f$) of $-85ppm/^{\circ}C$ was obtained at the sintering temperature of $930^{\circ}C$. The superior microwave properties of sol-gel processed MCV relative to conventional solid-state reaction processed one is remarkable especially at lower sintering temperatures such as $750^{\circ}C$ and $800^{\circ}C$.

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Pre-establishment of Microwave-Assisted Extraction Under Atmospheric Pressure Condition for Ginseng Components (상압조건의 마이크로웨이브 공정을 위한 인삼성분의 추출조건 설정)

  • Kim, Kyung-Eun;Lee, Gee-Dong;Kwon, Joong-Ho
    • Korean Journal of Food Science and Technology
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    • v.32 no.2
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    • pp.323-327
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    • 2000
  • Microwave-assisted process (2,450MHz), which is known as a more environmental-friendly process with economic advantages than the current extraction methods, was investigated to pre-establish the extraction conditions for soluble ginseng components used for the processing of ginseng products. The extractions of soluble ginseng components showed optimum conditions, such as 60 mesh in particle size, 1 : 10 (g/mL) in the sample to solvent ratio, and less than 100 watts in energy efficiency. Under these conditions using along with 60% ethanol for 5 min, the overall yield of ginseng extracts was about 83%. Most soluble components including saponins were extracted by repeating five times of microwave-assisted extraction.

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A Study on Treatment of a Contaminated Soil by Oil using Continuous System of High Temperature Heating Element and Microwave (마이크로웨이브와 고온발열체를 이용한 연속식 공정의 유류오염토양 처리에 관한 연구)

  • Ha, Sang-An;You, Mi-Young
    • Journal of Soil and Groundwater Environment
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    • v.17 no.1
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    • pp.8-12
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    • 2012
  • This study is maintains the condition of high temperature (above $600^{\circ}C$) within a short time using on microwave and high temperature heating elements. And removal characteristics according to changes in soil moisture, microwave power and temperature through the decomposition of the contaminated soil by oil. The difficulty resolvability material was sort of lubricating oil having long carbocyclic (C18-C50) and TPH removal rate reached 85.2% at 6 kW and $700^{\circ}C$ and thus the contaminant was removed 1,788 mg/kg within a process time of 40 minutes. In the case of light oil, gasoline contaminated soil, the removal amount showed 567 mg/kg and the treatment rate reached 98.4% at 6 kW, $500^{\circ}C$ and 20 minute. In the case of non-resolvability reached TPH concentrations on 2,000 mg/kg of worrisome level of soil contamination in the 3 zones at 6 kW, $700^{\circ}C$ and 30 minute. At the time, showed up processing costs 8,173 won per ton.