• Title/Summary/Keyword: microstructure effect

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Tensile Properties of Hybrid Fiber-Reinforced Reactive Powder Concrete After Exposure to Elevated Temperatures

  • Li, Haiyan;Liu, Gang
    • International Journal of Concrete Structures and Materials
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    • v.10 no.1
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    • pp.29-37
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    • 2016
  • The paper presents a research project on the tensile properties of RPC mixed with both steel and polypropylene fibers after exposure to $20-900^{\circ}C$. The direct and the indirect tensile strength (in bending) were measured through tensile experiment on dog-bone specimens and bending experiment on $40{\times}40{\times}160mm$ prisms. RPC microstructure was analyzed using scanning electron microscope. The results indicate that, steel fibers can significantly improve the tensile performance of hybrid fiber-reinforced RPC, whereas polypropylene fibers have no obvious effect on the tensile performance. With increasing temperature, the flexural and axial tensile strength of hybrid fiber-reinforced RPC substantially decrease linearly, which attributes to the deteriorating microstructure. Based on the experimental results, equations are established to express the decay of the flexural and tensile strength with increasing temperature.

Effect of the Oxide Glass on the Metal Sintering Behavior in Silver Thick-Film System

  • Chung Young Sir;Kim Ho-Gi
    • Proceedings of the Korean Ceranic Society Conference
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    • 1986.12a
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    • pp.259-267
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    • 1986
  • The sintering behavior of silver-oxide glass composite thick-film has been studied with varing glass content. It is shown that during heat treatment glass became liquid phase to deeply affect the microstructure development of the silver particles and to control the physical properties of the thick-films. As glass content increased, the initial repacking of silver particles took place rapidly but the homogeneities of the microstructure showed different features. When the glass content was over some range, the silver particles exuded glass to decrease net energy and glass formed liquid pools separated from the solid skeletons. Finally the relations between the microstructures and electrical properties of the thick-film were discussed.

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Effect of Microstructure on the Properties of High Strength Grouts (고강도 그라우트재의 특성에 미치는 미세구조의 영향)

  • 정민철;남기웅;정윤중
    • Journal of the Korean Ceramic Society
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    • v.31 no.6
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    • pp.609-616
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    • 1994
  • Investigation for the high strength grouts using ordinary cement mortar, melamine formaldehyde condensate (MFC) with various admixtures was carried out. The physical properties of the grouts were investigated through the observation of the microstructure and the application of fracture mechanics. When the lime stone and fly ash was added with 6 wt% to the grouts, the compressive strength was about 72 MPa, 69 MPa respectively, and the flexural strength was about 11.9 MPa, 11.4 MPa respectively, the Young's modulus was about 4.3 GPa, 3.9 GPa, and the critical stress intensity was about 7.3 ×10-1MNm-1.5, 6.8×10-1MNm-1.5 respectively. When the silica fume was added with 6 wt% to the grouts, the compressive strength and the flexural strength were 81 MPa, 12.3 MPa, Young's modulus was 4.8 GPa and the critical stress intensity was about 8.4×10-1MNm-1.5.

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Effect of $Mo_2C$ Content on the Microstructure and Properties of Ti(CN)-$Mo_2C$ Ceramics

  • Park, Dong-Soo;Lee, Yang-Doo;Taejoo Jung
    • The Korean Journal of Ceramics
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    • v.5 no.3
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    • pp.230-234
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    • 1999
  • Ti(CN)-0.3mole% $Mo_2C$ ceramics were prepared by pressureless sintering. $Mo_2C$ dissolved in Ti(CN) more easily in a nitrogen environment than in the other environment because nitrogen forced Mo to form a solid solution, (Ti, No)(C, N). A "core-rim" structure developed within the grains. The boundary between the "core" and the rim was delineated by thermal etching in the sample with more than 2 mole% $Mo_2C$. The rim thickness and the grain size decreased as the $Mo_2C$ content increased. The hardness and the flexural strength showed maxima of 18.2 GPa and 1.23 GPa, respectively when the $Mo_2C$ content was 2 mole%. The post-sintering heat treatments improved the properties.oved the properties.

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Effect of Si Addition on the Microstructure of AI-Cu-Si Alloy for Thin Film Metallization (반도체 metallization용 Al-Cu 합금의 미세구조 천이에 미치는 Si 첨가영향)

  • Park, Min-Woo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.05b
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    • pp.237-241
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    • 2000
  • The effects of Si addition on the precipitation processes of in Al-Cu-Si alloy films were studied by the transmission electron microscopy. Deposition of an Al-1.5Cu-1.5Si (wt. %) film at $305^{\circ}C$ resulted in formation of fine, uniformly distributed spherical $\theta$-phase particles due to the precipitation of the $\theta$ and Si phase particles during deposition. For deposition at $435^{\circ}C$, fine $\theta$-phase particles precipitated during wafer cooldown, while coarse Si nodules formed at the sublayer interface during deposition. The film susceptibility to corrosion is discussed in relation to the film microstructure and deposition temperature.

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Effect of the Mold Temperatures on the Microstructure and Mechanical Properties of Low Pressure Die-Cast Product (저압주조품의 미세조직과 기계적성질에 미치는 금형온도의 영향)

  • Lee, Jeong-Keun;Park, Chong-Sung;Kim, Myung-Ho
    • Journal of Korea Foundry Society
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    • v.18 no.3
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    • pp.254-261
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    • 1998
  • Microstructure and mechanical properties of the low pressure die-cast Al wheels were investigated by microscope, image analyzer, NDT (non-destructive test), and tensile test. The variation of SDAS (secondary dendrite arm spacing), porosity per unit area, quality grade, and tensile properties with the mold temperatures were examined. SDAS was gradually decreased with a decrease in temperature. However, the lowest value of porosity per unit area was observed at the mold temperature of $405^{\circ}C$ and the optimum mold temperature was found to be $405^{\circ}C$. Besides, from the observation of pore morphology, it was also found that the pore formation was mainly caused by shrinkage during solidification. The tensile strength, elongation, and impact toughness were markedly decreased, however the yield strength was nearly constant. The decrease of mechanical properties is attributed to the increase of porosity.

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A Numerical Study of the Effect of Casting Temperature and Rotational Frequency of Mold on the Functionally Graded Microstructure in Centrifugal Casting of Hyper-eutectic Al-Si Alloy (과공정 Al-Si합금의 원심주조시 용탕온도와 금형회전수가 경사기능 조직에 미치는 영향에 대한 해석적 고찰)

  • Park, Jeong-Wook;Kim, Heon-Joo
    • Journal of Korea Foundry Society
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    • v.29 no.2
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    • pp.78-85
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    • 2009
  • Functionally graded microstructure of centrifugal cast Al-Si alloy, especially distribution of primary Si particles according to the changes of melt pouring temperature and rotation frequency was investigated by numerical simulation. Moving velocity of Si particles increased as the melt pouring temperature and rotational frequency of mold increased. Therefore, segregation tendency of primary Si particles toward inner side of cylindrical sample increased as the melt pouring temperature and rotational frequency of mold increased. Rich distribution region of particles was located at 0.9, 0.7, 0.4 mm from inner surface of cylindrical sample under the centrifugal cast condition of $750^{\circ}C$ melt pouring temperature and 1500, 2000 and 2500 rpm mold rotational frequencies, respectively, by numerical simulation.

Effect of elevated temperature on physico-mechanical properties of metakaolin blended cement mortar

  • Morsy, M.S.;Rashad, A.M.;El-Nouhy, H.A.
    • Structural Engineering and Mechanics
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    • v.31 no.1
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    • pp.1-10
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    • 2009
  • An experimental investigation was conducted to evaluate the performance of mortars with and without Metakaolin (MK) exposed to elevated temperatures $200^{\circ}C$, $400^{\circ}C$, $600^{\circ}C$ and $800^{\circ}C$ for two hours. The binder to sand ratio was kept constant (1:5.23). The ordinary Portland cement (OPC) was replaced with MK at 0%, 5%, 10% 20% and 30%. All mixtures were designed to have a flow of $94{\pm}5%$. The compressive strength of mortars before and after exposure to elevated temperature was determined. The formation of various decomposition phases were identified using X-ray diffractometry (XRD) and differential thermal analysis (DTA). The microstructure of the mortars was examined using scanning electron microscope (SEM). Test results indicated that MK improves the compressive strength before and after exposure to elevated temperature and that the 20% cement replacement of MK is the optimum percentage.

Physical Properties of Thin Metal Films -II (-Effect of Oxygen on Thin Metal Film Formation and Physical Properties- (금속박막의 물리적 성질 -II- -금속박막형성과 물성에 미치는 산소의 영향-=)

  • 이세경;박수현
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.25 no.7
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    • pp.791-798
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    • 1988
  • Films of Cr, Cu, and Al were deposited by the evaporation technique at the high vacuum level-high evaporation rate and the low vacuum level-low evaporation rate. We measured sheet resistance and light transmittance, and observed microstructure and diffraction pattern by TEM, and investigated oxygen content in thin film by AES. We discussed the relations among microstructure, sheet resistance, and light transmittance with AES data. We found that the films deposited at the high vacuum level-high evaporation rate have small oxygen content in thin film comparing to the films deposited at the low vacuum level-low vacuum level-low evaporation rate, and that the films having crystalline structure and larger grain size were formed in the case of the high vacuum level-high evaporation rate and they showed lower sheet resistance and lower light transmittance.

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Effect of Annealing and Co contents on the Structural and Physical Properties in AlN Thin Films

  • Han, Chang-Suk;Han, Seung-Oh
    • Journal of the Korean Society for Heat Treatment
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    • v.23 no.6
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    • pp.331-337
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    • 2010
  • Aluminum nitride (AlN) thin films containing various amounts of Co content have been deposited by using a two-facing targets type sputtering (TFTS) system. The deposited films were also annealed successively and isothermally at different temperatures. Annealing treatment can control the physical properties as well as the microstructure of AlN films with Co particles. High magnetization and high resistivity are obtainable in AlN films containing dispersed Co particles. The coercivity of the films does not depend on annealing time, but it increases with increasing annealing temperature due to the increase of the grain size. A high saturation magnetization of 46 kG and resistivity of 2200 ${\mu}{\Omega}$-cm was obtained for AlN films containing 25 at% Co.