• The Korean Journal of Ceramics
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• v.5 no.3
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• pp.224-229
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• 1999

The preparation and toughening of SiC-AIN solid solution from powder mixtures of $\beta$-SiC, AIN and $\alpha$-SiC by hot-pressing were studied in the 1870 to $2030^{\circ}C$ temperature range. The reaction of AIN and $\beta$-SiC(3C) powders causing transformation to the 2H(wurtzite) structure appeared to depend on hot-pressing temperatures and an additive of $\alpha$-SiC. For the composition of 49wt% SiC with 2 wt% $\alpha$-SiC and 47.5 wt% AIN47.5wt% SiC with 5 wt % $\alpha$-SiC at 203$0^{\circ}C$ for 1 h, th complete solid solutions with a single phase of 2H could be obtained. The appreciable amount of $\alpha$-SiC could develop the columnar inter-grains of 4H phase and the stable 2H phase with the relatively uniform composition and grain size distributions. The effect of $\alpha$-SiC on the phases present and compositional microstructures with columnar inter-grains was invetigated using X-ray diffraction, scanning electron microscopy and transmission electron microscopy. The fracture toughness and Vickers hardness of the hot-pressed solid solutions wre examined by the indentation-fracture-test method.

• Journal of the Korean Ceramic Society
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• v.53 no.2
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• pp.234-240
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• 2016

Energetically-modified material using reject fly ash (RFA), generated from thermal power plants, was manufactured to investigate the effect of the material on the physical and chemical characteristics of cement mortar. In order to modify reject fly ash, a vibration mill was used. Particle size, grain shape, and crystal structure of the ash were analyzed. Then, the compressive strength of the mortar using energetically-modified reject fly ash (ERFA) was measured. Microstructure and X-ray diffraction (XRD) patterns were also used in the analysis. As the replacement rate of ERFA increased, the value of the compressive strength tended to decrease. However, it was found that the compressive strength values of 7 and 28 days-cured specimens were higher than those of conventional ordinary Portland cement (OPC) mortar with 10 % replacement rate condition.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2003.07b
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• pp.913-917
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• 2003

In the electronic components and devices fabrication, thin film resistors with low TCR(temperature coefficient of resistance) and high precision have been used over 3 GHz microwave in recent years. Ni-Cr alloys thin films resistors is one of the most commonly used resistive materials because it has low TCR and highly stable resistance. In this work, we fabricated thin film resistors using Evanohm alloys target(72Ni-20Cr-3Al-4Mn-Si) of s-type with excellent resistors properties by RF-sputtering. Also we reported best deposited conditions of thin film resistors for microwave to observe microstructure and electronic properties of thin film according to deposited conditions(between target and substrate, power supply)

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2008.11a
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• pp.208-208
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• 2008

Micro patterning of conductor line/space on LTCC green sheet in the LTCC module is an important process for miniaturization in 3D integrated circuits. This work presented the effect of inorganic binders on the microstructure, adhesion, electrical resistivity, shrinkage and line/space resolution, which is a part of study in photoimageable conductor paste. The photoimageable conductor paste contains silver powder, polymer binder, monomer, photo-initiator, UV absorber, and solvent. The inorganic binders were furnished with varied weight percentage of anorthite, diopside and MLS-62 glass frits from 0% to 7%. The Line/space sizes thus obtained was under 25 micron.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.26 no.9
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• pp.651-655
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• 2013

$(Ba_{0.85}Ca_{0.15})(Ti_{0.9}Zr_{0.1})O_3$ + 0.04 wt% $CeO_2$ lead-free ceramics were synthesized by conventional sintering process and the effect of calcination temperature on microstructure, dielectric and piezoelectric properties were investigated. Improved piezoelectric properties have been observed at $1,125^{\circ}C$ calcination temperature which show the optimal electrical properties, $k_p$~0.457, $d_{33}$~367 pC/N, $Q_m$~158 and $T_c$~$85^{\circ}C$. These results show that the piezoelectric properties can be improved by appropriate calcination temperature.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2003.10a
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• pp.59-65
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• 2003

Four kinds of $Si_3N_4$-based ceramic cutting tools with different sintering time were fabricated to investigante the effect of sintering time on the microstructure, mechanical properties, grain sizes and the cutting performance. An endeavor was also made to determine the relation among mechanical property, Brain size and tool life. $Si_3N_4$ home made cutting tool sintered for 1 hour under $1760^{\circ}$ temperature and 25MPa pressure showed the best cutting performance among selected ceramic tools during machining both Bray cast iron and heat treated SCM440. Multiple linear regression model was used to estimate the tool lift from mechanical property, grain size and showed good result. It was also shown that hardness imposed the biggest offect on tool life.

• Journal of Korea Foundry Society
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• v.15 no.6
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• pp.604-615
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• 1995

Austenitic stainless steel castings using expandable polystylene(referred to hereafter as EPS) patterns are often affected by distinctive defects associated with incomplete decomposition of the EPS as the molds are filled with metal. The quality of the castings, with particular reference to carbon pick-up in austenitic stainless steel is further influenced to a significant extent by such factors as reduced pressure, the additive by adding $Na_2CO_3$ in coating. The steel composition and microstructure were examined at the surface layer of castings, at depths of 1mm, by taking successive layers of swarf and analysis. In experiments, the carburizing atmosphere was neutralized, showing that the coating performed efficiently by decomposing almost instantly on heating and liberating $CO_2$. The upper parts of castings obtained using EPS patterns were slightly higher in carbon pick-up than other parts. Comparing the 316L and 304 stainless steel castings, qualitative and quantative differences could be found between the carbon pick-up behaviours as influence of the carbon content and alloying elements. Carbide former such as Cr makes carbon more soluble in the steel. This must make carbon pick-up in the surface layer but at the same time richer in carbon especially in the 304 stainless steel castings.

• Journal of Korea Foundry Society
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• v.13 no.3
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• pp.259-267
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• 1993

The effects of casting processes-direct and indirect squeeze casting, permanent mold casting and die casting on the microstructure and mechanical properties were studied for the hypereutectic B390 aluminium alloy. The effects of T5 and T6 heat treatment were also examined. The direct and indirect squeeze casting showed no casting defects such as porosity and shrinkage were observed in permanent mold castings and die castings. The primary silicon phase was refined and homogeneously distributed in the order of indirect squeeze casting, diecasting, direct squeeze casting and permanent mold casting. Depletion of primary silicon phase in die casting surface was disappeared in indirect squeeze casting. Tensile strength of cast and heat treated specimens were increased in the order of direct squeeze casting, permanent mold casting, indirect squeeze casting and die casting. Hardness of indirect squeeze castings was larger than that of other castings. As indirect squeeze casting of B390 aluminium alloy, the time of T6 heat treatment to achieve high strength can be reduced.

• Journal of Korea Foundry Society
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• v.17 no.2
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• pp.195-206
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• 1997

AC8A matrix composites reinforced with Ni-aluminide were fabricated by squeeze casting process, and the characteristics and nature of the growth of Ni-aluminide phases at the interface between nickel and aluminurn were investigated. In the as-cast composites, the reaction layer between Ni skeleton and aluminum matrix was found to be $NiAl_3$, regardless of the casting temperatures and the kinds of preforms. During high temperature solution treatment the $NiAl_3$ layer grew and formed new $Ni_2Al_3$ layer. Because of presence of the porosity formed by Kirkendall effect at the interface between $NiAl_3$ and aluminum matrix, the tensile strength of composites was inferior to that of AC8A matrix alloy. However, the composites exhibited superior wear resistance due to the formation Ni-aluminide intermetallic phases. Composite A, of which Ni skeleton was fully transformed into Ni-aluminide, shows better wear resistance than that of composite B which still possessed some unreacted Ni skeleton.

• Journal of Korea Foundry Society
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• v.31 no.6
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• pp.354-361
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• 2011

The liquid metal shearing device was constructed and assembled with a commercial high-pressure die-caster in order to induce intensive turbulent shearing force on molten aluminum alloys. The effect of the liquid metal shearing on the microstructure and tensile properties of A356 alloys was investigated with the variation of iron content. The experimental results show that dendritic primary ${\alpha}$-Al phase was effectively modified into a equiaxed form by the liquid metal shearing. It was also found that the needle-like ${\beta}$-AlFeSi phase in a Fe containing A356 alloy was changed into a blocky shape resulting in the improved mechanical properties. Based on the mechanical properties, it was suggested that the iron content in A356 alloy could be more widely tolerated by utilizing the liquid metal shearing HPDC process.