• Journal of Powder Materials
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• v.10 no.5
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• pp.325-332
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• 2003

The effect of extrusion temperature on the microstructure and mechanical properties was studied in gas atomized TEX>$Al_{81}Si_{19}$ alloy powders and their extruded bars using SEM, tensile testing and wear testing. The Si particle size of He-gas atomized powder was about 200-800 nm. Each microstructure of the extruded bars with extrusion temperature (400, 450 and 50$0^{\circ}C$) showed a homogeneous distribution of primary Si and eutectic Si particles embedded in the Al matrix and the particle size varied from 0.1 to 5.5 ${\mu}m$. With increasing extrusion temperature from 40$0^{\circ}C$ to 50$0^{\circ}C$, the ultimate tensile strength (UTS) decreased from 282 to 236 ㎫ at 300 K and the specific wear increased at all sliding speeds due to the coarse microstructure. The fracture behavior of failure in tension testing and wear testing was also studied. The UTS of extrudate at 40$0^{\circ}C$ higher than that of 50$0^{\circ}C$ because more fine Si particles in Al matrix of extrudate at 40$0^{\circ}C$ prevented crack to propagate.

• Proceedings of the KWS Conference
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• 2002.10a
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• pp.217-221
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• 2002

In the coarse grain HAZ adjacent to the fusion line, most of the TiN particles in conventional Ti added steel are dissolved and austenite grain growth is easily occupied during welding process. To avoid this difficulty, thermal stability of TiN particle is improved by increasing the nitrogen content in steel. In this study, the effect of high nitrogen TiN particle on preventing austenite grain growth in HAZ was investigated. Increased thermal stability of TiN particle is helpful for preventing the austenite grain growth by pinning effect. High nitrogen TiN particle in simulated HAZ were not dissolved even at high temperature such as 1400 C and prevented the austenite grain growth in simulated HAZ. Owing to small austenite grain size in HAZ the width of coarse grain HAZ in high nitrogen TiN steel was decreased to 1/10 of conventional TiN steel. Even high heat input welding, the microstructure of coarse grain HAZ consisted of fine polygonal ferrite and pearlite and toughness of coarse grain HAZ was significantly improved.

• Journal of Power System Engineering
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• v.14 no.2
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• pp.84-89
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• 2010

The effect of forging condition on the microstructure and mechanical properties of 9Cr-1Mo heat-resisting steel was investigated. Microstructure of centrifugal casted 9Cr-1Mo heat resisting steel and forged heat resisting steel are consisted of martensite. With the increase of forging ratio, tensile strength and hardness increased, while elongation and impact value decreased. By increasing of forging starting temperature and finishing temperature, tensile strength and hardness increased, while elongation and impact value decreased. We obtained the optimum forging conditions as follow, forging ratio is 30%, forging starting temperature is $1200^{\circ}C$ and forging finishing temperature is $950^{\circ}C$.

• Transactions of Materials Processing
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• v.25 no.2
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• pp.96-101
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• 2016

The current study was conducted to elucidate the effect of cementite morphology and matrix-ferrite microstructure on sliding wear behavior in spheroidized high carbon (1wt. % C) steel. The high carbon steel was initially heat treated to obtain a full pearlite or a martensite microstructure before the spheroidization. The spheroidizing heat treatment was performed on the full pearlitic steel for 100 hours at 700℃ and tempering was performed on the martensitic steel for 3 hours at 650℃. A spheroidized cementite phase in a ferrite matrix was obtained for both the full pearlite and the martensite microstructures. Sliding wear tests were conducted using a pin-on-disk wear tester with the heat treated steel as the disk specimen. An alumina(Al₂O₃) ball was used as the pin counterpart during the test. After the spheroidizing heat treatment and the tempering, both pearlite and martensite exhibited similar microstructures of spheroidized cementite in a ferrite matrix. The spheroidized pearlite specimens had lower hardness than the tempered martensite; however, the wear resistance of the spheroidized pearlite was superior to that of the tempered martensite.

• Journal of Powder Materials
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• v.19 no.4
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• pp.278-284
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• 2012

$Al_2O_3$ foam is an important engineering material because of its exceptional high-temperature stability, low thermal conductivity, good wear resistance, and stability in hostile chemical environment. In this work, $Al_2O_3$ foams were designed to control the microstructure, porosity, and cell size by varying different parameters such as the amount of amphiphile, solid loading, and stirring speed. Particle stabilized direct foaming technique was used and the $Al_2O_3$ particles were partially hydrophobized upon the adsorption of valeric acid on particles surface. The foam stability was drastically improved when these particles were irreversibly adsorbed at the air/water interface. However, there is still considerable ambiguity with regard to the effect of process parameters on the microstructure of particle-stabilized foam. In this study, the $Al_2O_3$ foam with open and closed-cell structure, cell size ranging from $20{\mu}m$ to $300{\mu}m$ having single strut wall and porosity from 75% to 93% were successfully fabricated by sintering at $1600^{\circ}C$ for 2 h in air.

• Journal of the Korean Ceramic Society
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• v.40 no.1
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• pp.1-4
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• 2003

To study the effect of aggregates on the microstructure of sintered bodies, Mn-Zn ferrite powders were prepared by an alcoholic dehydration method. Aggregate powders and reground powders were used as seeds and matrices, respectively. The mixing ratios for the aggregate and reground powders were varied with the sintering temperatures. Green densities were measured with changes in forming pressure and they were related to the microstructures of the sintered bodies. The aggregates proved to be capable of acting as seeds for abnormal grain growth. When the green density difference between the aggregate and the matrix was large, the aggregate could become the seed of abnormal grain growth. As the forming pressure increased, the more aggregates became seeds of abnormal grain growth.

• Korean Journal of Materials Research
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• v.30 no.1
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• pp.44-49
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• 2020

The effect of intercritical annealing temperature on the microstructure and mechanical properties of Fe-9Mn-0.2C-3Al-0.5Si medium manganese steels containing Cu and Ni is investigated in this study. Six kinds of medium manganese steels are fabricated by varying the chemical composition and intercritical annealing temperature. Hardness and tensile tests are performed to examine the correlation of microstructure and mechanical properties for the intercritical annealed medium manganese steels containing Cu and Ni. The microstructures of all the steels are composed mostly of lath ferrite, reverted austenite and cementite, regardless of annealing temperature. The room-temperature tensile test results show that the yield and tensile strengths decrease with increasing intercritical annealing temperature due to higher volume fraction and larger thickness of reverted austenite. On the other hand, total and uniform elongations, and strain hardening exponent increase due to higher dislocation density because transformation-induced plasticity is promoted with increasing annealing temperature by reduction in reverted austenite stability.

• Journal of Power System Engineering
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• v.11 no.1
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• pp.121-126
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• 2007

This study aims at investigating the effect of heat treatment conditions on the dry sliding wear behavior of thermally sprayed Ni-based self-flux alloy coatings. Ni-based self-flux alloy powders were sprayed onto a carbon steel substrate and then heat-treated at 700, 800, 900 and $1000^{\circ}C$ for 30 minutes in a vacuum furnace. Dry sliding wear tests were performed using sliding speed of 0.4 m/s and applied load of 6 N. AISI 52100 ball(diameter 8 mm) was used as counterparts. Microstructure and wear behavior of both as-sprayed and heat-treated Ni-based self-flux alloy coatings were studied using a scanning electron microscope(SEM), energy dispersive X-ray spectroscopy(EDX), electron probe micro-analysis(EPMA) and X-ray diffraction(XRD). It was revealed that microstructure and wear behavior of thermally sprayed Ni-based self-flux alloy coatings were much influenced by heat treatment conditions.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.10a
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• pp.146-149
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• 2007

The effects of boron additions in steels have long been recognized as very important, mainly with respect to hardnability of heat treatable steels. The systematics of structure and properties of boron steels will then be illustrated in the context of low-alloy steels with carbon contents raging from 0.05 to 0.25% and boron contents 0-130 ppm. we investigated the effect of the microstructure and mechanical properties with heat treatment condition of the boron-treated(0.0013 ppm) low carbon(0.2 %C) low alloy steel. The specimens were austenitised for 5 and 10, 15 min at $880{\sim}940^{\circ}C$(with/without tempered at 150, 180 and $210^{\circ}C$ for the various periods of time from 60 min to 120 min) After heat treatment, mechanical properties were measured by tensile test and hardness test. For analysis of microstructure, Optical/SEM analysis and XRD were carried out.

• Journal of Welding and Joining
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• v.32 no.1
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• pp.22-27
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• 2014

In the past, cold crack was commonly observed in the HAZ(heat affected zone) of high-strength steels. Applying to TMCP(thermo-mechanical controlled process) and HSLA(high strength low alloy) steels, cold crack tends to increase the occurrence in the weld metal. It is generally understood that cold crack occurs when the following factors are present simultaneously : diffusible hydrogen in the weld metal, a susceptible microstructure and residual stress. In particular, many studies investigated the microstructural effect on the cold crack in HAZ and the cold crack in weld metals starts to receive the special attendance in modern times. The purpose of the study is to review the effect of weld microstructures (grain boundary ferrite, Widm$\ddot{a}$nstatten ferrite, acicular ferrite, bainite and martensite) on cold crack in the weld metals. Among various microstructures of weld metals, acicular ferrite produced the greatest resistance to the cold crack due to the fine interlocking nature and high-angle grain boundary of the microstructure.