• Journal of Advanced Marine Engineering and Technology
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• v.27 no.6
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• pp.704-713
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• 2003

The effect of partial substitution of tungsten for molybdenum on the microstructure and corrosion resistance in 22Cr-5Ni-3Mo duplex stainless steel(DSS) aging heat treated in a temperature range of 600~$1000^{\circ}C$ has been investigated. Electrochemical tests were carried out for the evaluation of corrosion resistance. Aging treatment had hardly influenced the general corrosion resistance. With the increase of aging time, the pitting corrosion resistance of the DSS had decreased, After aging for 2min at 700~$900^{\circ}C$, the pitting potential of the 3Mo steel decreased remarkably, while that of the W-substituted steel hardly changed. During aging. the intermetallic $\sigma$ and secondary austenite ($\gamma_2$) phases were precipitated. and the pitting corrosion and intergranular corrosion resistance were significantly decreased after aging at 700~$750^{\circ}C$ for 10 h, which could be caused by the $\gamma_2$ formation. The ${\gamma}$$_2$ phase could affect the depletion of molybdenum and chromium in the $\gamma_2/\alpha and \gamma_2/\sigma$ boundaries.

• Proceedings of the KSME Conference
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• 2007.05a
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• pp.409-414
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• 2007

Wettability of solid surfaces with liquids is governed by the chemical properties and the microstructure of the surfaces. We report on the preparation of liquid-repellent surfaces using surface-attached monolayers of perfluorinated polymer molecules on porous silica substrates. A covalent attachment of the polymer molecules to the substrate is achieved by generation of the polymer chains through starting a surface-initiated radical-chain polymerization of a fluorinated monomer. To this, self-assembled monolayers of azo initiators are attached to silica substrates, which are used to kick off the polymerization reaction in situ. The growth of the fluorinated polymer films and the characterization of the obtained surfaces by surface plasmon spectroscopy, XPS, and contact angle measurements is described. It is shown that perfluorinated polymer films can be grown with controlled thicknesses on flat and even on porous silica surfaces, essentially without changing the surface roughness. The combination of the low surface energy coating and the surface porosity allows generation of materials which are both water and oil repellent.

• Journal of Powder Materials
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• v.11 no.1
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• pp.34-42
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• 2004

The effect of extrusion temperature on the microstructure and mechanical properties were studied in He-gas atomized $Al_{81-(x＋y)}Si_{19}Ni_xCe_y$ alloy powders and their extruded bars using SEM, tensile testing and thermal expansion testing. The extruded bar of $Al_{73}Si_{19}Ni_7Ce_1$ alloy consists of a mixed structure in which fine Si particles with a particle size below 20∼500nm and very fine $Al_3Ni,\;Al_3Ce$ compounds with a particle size below 200nm are homogeneously dispersed in Al martix with a grain size below 500nm. With increasing extrusion temperature, the microstructural scale was decreased. The ultimate tensile strength of the alloy bars has incresed with decreasing extrusion temperature from 500 to 35$0^{\circ}C$ and $Al_{73}Si_{19}Ni_7Ce_1$ alloy extreded at 35$0^{\circ}C$ shows a highest tensile strength of 810 MPa due to the fine namostructure. The addition of Ni and Ce decreased the coefficients of thermal expansion and the effects of extression temperature on the thermal expansion were not significant.

• Computers and Concrete
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• v.17 no.4
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• pp.553-566
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• 2016

Fracture energy is one of the key parameters reveal cracking resistance and fracture toughness of concrete. The main purpose of this study is to determine fracture behavior, mechanical properties and microstructural analysis of high strength basalt fiber reinforced concrete (HSFRC). For this purpose, three-point bending tests were performed on notched beams produced using HSFRCs with 12 mm and 24mm fiber length and 1, 2 and $3kg/m^3$ fiber content in order to determine the value of fracture energy. Fracture energies of the notched beam specimens were calculated by analyzing load versus crack mouth opining displacement curves by the help of RILEM proposal. The results show that the effects of basalt fiber content and fiber length on fracture energy are very significant. The splitting tensile and flexural strength of HSFRC increased with increasing fiber content whereas a slight drop in flexural strength was observed for the mixture with 24mm fiber length and $3kg/m^3$ fiber content. On the other hand, there was no significant effect of fiber addition on the compressive strength and modulus of elasticity of the mixtures. In addition, microstructural analysis of the three components; cement paste, aggregate and basalt fiber were performed based on the Scanning Electron Microscopy and Energy-Dispersive X-ray Spectroscopy examinations.

• Journal of Powder Materials
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• v.20 no.1
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• pp.24-32
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• 2013

The effect of carrier gases (He, $N_2$) on the properties of Ti coating layers were investigated to manufacture high-density Ti coating layers. Cold spray coating layers manufactured using He gas had denser and more homogenous structures than those using $N_2$ gas. The He gas coating layers showed porosity value of 0.02% and hardness value of Hv 229.1, indicating more excellent properties than the porosity and hardness of $N_2$ gas coating layers. Bond strengths were examined, and coating layers manufactured using He recorded a value of 74.3 MPa; those manufactured using $N_2$ gas had a value of 64.6 MPa. The aforementioned results were associated with the fact that, when coating layers were manufactured using He gas, the powder could be easily deposited because of its high particle impact velocity. When Ti coating layers were manufactured by the cold spray process, He carrier gas was more suitable than $N_2$ gas for manufacturing excellent coating layers.

• Journal of Korea Foundry Society
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• v.21 no.2
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• pp.127-134
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• 2001

Misch metal (rare earth element, Ce, La, Nd, Pr) which has large influence on high-temperature stability and toughness was added to the Al-5%Ni-5%Mg alloy, and squeeze casting was used for Al-5%Ni-5%Mg-(Mm) alloys. The effect of applied pressure and misch metal additions on mechanical properties in Al-5%Ni-5%Mg alloy by direct squeeze casting has been investigated. The applied pressure were 0 MPa(gravity casting), 25, 50 and 75 MPa. Squeeze-cast Al-5%Ni-5%Mg-(Mm) alloys had better mechanical properties than those of non-pressurized cast alloys because of the increased cooling rate by the application of pressure during solidification. By the addition of misch metal in Al-5%Ni-5%Mg alloy, better combination of strength and elongation was obtained. The addition of 0.3%Mm in Al-5%Ni-5%Mg alloy improved the heat resistant property due to the formation of fine eutectic phases.

• Journal of Welding and Joining
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• v.24 no.2
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• pp.48-56
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• 2006

The fatigue strength of the welds is affected by such factors as the weld geometry, microstructures, tensile properties and residual stresses caused by fabrication. It is very important to evaluate the structural integrity of the welds in nuclear power plant because the weldment undergoes the most of damage and failure mechanisms. In this study, the fatigue assessments for a reactor vessel outlet nozzle with the weldment to the piping system are performed considering the welding residual stresses as well as the effect of local brittle zone in the vicinity of the weld fusion line. The analytical approaches employed are the microstructure and mechanical properties prediction by semi-analytical method, the thermal and stress analysis including the welding residual stress analysis by finite element method, the fatigue life assessment by following the ASME Code rules. The calculated results of cumulative usage factors(CUF) are compared for cases of the elastic and elasto-plastic analysis, and with or without residual stress and local brittle zone effects, respectively. Finally, the fatigue life of reactor vessel outlet nozzle weld is slightly affected by the local brittle zone and welding residual stresses.

• Proceedings of the KWS Conference
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• 2006.10a
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• pp.63-65
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• 2006

The paper deals with the effect of hydrogen or helium in argon as a shielding gas on GTA welding of austenitic stainless steel. The studies were carried out in GTA(Gas Tungsten Arc) welding with a non-consumable electrode in case with different volume additions of hydrogen or helium to the argon shielding gas, i.e $5%H_2,\;10%H_2$, 30%He and 67%He. The penetration, welding voltage, microstructure and mechanical property were examined. The deepest penetration was obtained from the sample which was welded under shielding gas of $10%H_2$. The studies showed that hydrogen or helium addition to argon changes the static characteristic of the welding arc. The hydrogen or helium addition to argon increases arc power and the quantity of the material melted. The weld metal penetration depth and its width increased with increasing hydrogen or helium content. Additionally, welding voltage increased with increasing hydrogen or helium content.

• Journal of Welding and Joining
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• v.27 no.3
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• pp.52-59
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• 2009

Flash butt welding is applied in many industries. New technology was developed recently for joining billets which called "EBROS (Endless Bar Rolling System)". After reheating billets in furnace, two billets were joined using flash butt welding. The objective of this study was to investigate the effect of alloying elements on mechanical properties of flash butt welded zone of hot rolled steel bar. The tensile properties on welded zone of Fe-Mn steel and Fe-Mn-V steel were dropped as compared with non-welded zone. Fe-Mn-Nb steel was opposed to the former. It was found that the white band at the welded zone had high ferrite volume fraction and large ferrite grain size. The vertical white band between flash butt welded billets was transformed into an arrowhead it of steel bar. According to this band, softening has been appeared. There was a interesting phenomenon with HAZ of Fe-Mn-Nb Steel, 40nm scale of particles were observed and hardness of HAZ was higher than non-welded zone.

• Transactions of Materials Processing
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• v.22 no.3
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• pp.158-164
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• 2013

The spheroidization behavior of cementite in a SK85 high carbon steel was investigated in this study. Fine and coarse pearlite microstructures were obtained by appropriate heat treatments according to the TTT diagram of SK85 high carbon steel. Hot rolled plates of SK85 steel were austenitized at $800^{\circ}C$ for 2 hrs and then put directly into a salt bath at either $570^{\circ}C$ or $670^{\circ}C$ to obtain a fine pearlite (FP) structure and a coarse pearlite (CP) structure, respectively. Cold rolling was subsequently conducted on those specimens with reduction ratios from 0.2 to 0.4. Spheroidization heat treatments were conducted at the subcritical temperatures of 600 and $720^{\circ}C$ for 1 to 32 hrs to elucidate the effect of initial microstructures, heat treatment temperature, and cold reduction ratios on the cementite spheroidization rate. Spheroidization proceeded with fragmentation of cementite plates, spheroidization of the cementite platelets, and coarsening consecutively. Mechanical fragmentation of cementite by cold rolling expedited the rate of spheroidization. The spheroidization rate of FP was much more rapid than that of CP and the spheriodization rate increased with increases in the cold reduction ratio.