• Title/Summary/Keyword: microstructure effect

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Interfacial Morphology of Glass Fiber/Polypropylene Composite (유리 섬유/폴리프로필렌 복합재료의 계면 형태구조)

  • 남주영;박수현;이광희;김준경
    • Polymer(Korea)
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    • v.27 no.4
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    • pp.299-306
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    • 2003
  • It is well known that the interaction and adhesion between the glass fiber (GF) and polymer matrix has a significant effect in determining the properties of fiber-reinforced materials. Therefore, it is one of important considerations to modify the surface of glass fiber with an appropriate sizing. We investigated the treatment method of glass fiber with coupling agent to improve the interaction of the interfacial region. The correlation between interfacial property and interphase microstructure was also examined in an attempt to realize a proper morphology at the glass fiber surfaces.

Impedance Analysis of Resistance Anomaly of $BaTiO_3$ based PTC thermistor

  • Chun, Myoung-Pyo;Myoung, Seong-Jae;Nam, Joong-Hee;Cho, Jeong-Ho
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.06a
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    • pp.182-182
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    • 2009
  • The effect of Re-oxidation on the PTCR properties of Sm-doped barium titanate ceramics was investigated by means of impedance spectroscopy. Electrical properties such as resistance vs. temperature, I-V curve were measured and microstructure was observed with SEM photography. Sample was fabricated with thick film process such as tape casting of green sheet, screen printing of electrode pattern, stacking, firing in reduced atmosphere and re-oxidation, etc. As the temperature of re-oxidation increases, resistance jump as a function of temperature enhances but resistance at room temperature increases. These behavior of resistance as a function of temperature, dependent on the re-oxidation condition, is analyzed with Cole-Cole impedance plot and is shown to be related with the degree of oxidation of grain boundary regardless of grain core during re-oxidation process of sample.

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The Mechanical Properties and Characteristics of TRIP-assisted Multiphase Steels in High Toughness for Autombile Safety (자동차의 안정성을 고려한 고인성 충격흡수 강재로서 TRIP 형 복합상강의 기계적 성질 및 그 특성)

  • 이기열
    • Transactions of the Korean Society of Automotive Engineers
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    • v.8 no.4
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    • pp.141-148
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    • 2000
  • As the steel plates used for automobile safety the TRIP-assisted multiphase steels are being introduced to automobile industry with respect to their remarkable mechanical properties for the combination of high strength and large elongation. This multiphase structure is generated by two stage heat treatment (intercritical annealing & isothermal treatment) The metastable retained austenite can be transformed to martensite when plastically deformed which results in TRIP effect. Actually the microstructure of TRIP-assisted steels consist of a fine dispersite. There present discussion deals with bainite reaction kinetics of austenite in the process o f two stage heat treatment. In relation to bainite transformation the characteristics of bainite reaction is found to be influenced by the bainite tempering temperature and also by the relative rate in which carbides precipitate within residual austenite.

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Electrical Properties of Piezoceramic PZT with $Nb_2O_5$ Dopant ($Nb_2O_5$를 첨가한 압전 세라믹 PZT의 전기적 특성)

  • Park, J.H.;Choi, H.I.;SaGong, G.
    • Proceedings of the KIEE Conference
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    • 1991.11a
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    • pp.336-338
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    • 1991
  • Effects of $Nb_2O_5$ addition ranged from 0.0 to 0.75(wt%) on the microstructure and electrical porperties of PZT ceramics have been investigated. The Pb vacancy concentration increases with increasing NbO content. However, the experimental results show the resistivity increases with increasing $Nb^{5+}$ content. This behavior can be explained as a compensation effect and $Nb^{5+}$ can serve as a donar and contribute electrons to the conduction process. According to the law of mass action, this result may reduce the total charge carrier:thus the resistivity increase with NbO content in PZT.

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Compressive Basic Creep Prediction in Early-Age Concrete (초기재령 콘크리트의 압축 기본크리프 예측)

  • 김성훈;송하원;변근수
    • Proceedings of the Korea Concrete Institute Conference
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    • 1999.10a
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    • pp.285-288
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    • 1999
  • Creep is a major parameter to represent long-term behavior of concrete structures concerning serviceability and durability. The effect of creep is recently taking account into crack resistance analysis of early-age concrete concerning durability evaluation. Since existing creep prediction models were proposed to predict creep for hardened concrete, most of them cannot consider effectively the information on microstructure formation and hydration developed in the early-age concrete. In this study, creep tests for early-age concrete made of the type I cement and the type V cement are carried out respectively and creep prediction models are evaluated for the prediction of creep behavior in early-age concrete. A creep prediction model is modified for the prediction of creep in early-age concrete and also verified by comparing prediction results with results of creep tests on early-age concrete.

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A Study on the Microstructural Control of LAS Ceramics (II): Influence of L$Li_2O{cdot}4B_2O_3$ Frit Addition on the Microstructure and Thermal Expansion of ${\beta}$-Spodumene (LAS계 내열충격성 재료의 미세구조 제어(II): $Li_2O{cdot}4B_2O_3$ 프릿트 첨가가 ${\beta}$-Spodumene의 미세구조 및 열팽창특성에 미치는 영향)

  • 박정현;김현민;이화선
    • Journal of the Korean Ceramic Society
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    • v.29 no.7
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    • pp.533-538
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    • 1992
  • Effect of Li2O.4B2O frit on the microstructural and thermal expansion behaviour of $\beta$-spodumene ceramics was investigated. With 4.0~8.0 wt.% frit addition, sintering temperature range was enlarged and densification was enhanced through liquid phase sintering. As the amount of frit addition was increased, thermal expansion coefficient was increased to 1.72$\times$10-6$^{\circ}C$-1 of its highest value, which indicated that the increment of thermal expansion coefficient due to the second phase was constrained.

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Thermoelectric Property and p-n Transition Mechanism of Hot Pressed Bi4/3Sb2/3Te3 ($Bi_{4/3}Sb_{2/3}Te_3$ 가압소결체의 열전특성과 p-n 전이기구)

  • 박태호;유한일;심재동
    • Journal of the Korean Ceramic Society
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    • v.29 no.11
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    • pp.855-862
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    • 1992
  • Thermoelectric power, electrical conductivity and Hall effect were measured, as functions of temperature in the range of 100 to 600 K, on polycrystalline Bi4/3Sb2/3Te3 which had been prepared via uniaxial hot-pressing at different temperatures in the range of 373 K to 773 K, aiming at searching a profitable processing route to a polycrystalline thermoelectric material, a promising, viable alternative to a single crystalline one. It was found that, with increasing temperature of pressing under a fixed pressure, the material, normally a p-type prior to being hot-pressed, underwent a transition to n-type. This transition was confirmed to be due to plastic deformation during hot-pressing and interpreted as being attributed to the change of the major ionic defect BiTe' into TeBi˙at temperature high enough for structure elements mobility. Thermoelectric figure-of-merit of the hot-pressed material was discussed in connection with the p-n transition in addition to microstructure.

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Effect of Aging on the Microstructure and Mechanical Properties in Super Duplex Stainless Steel (슈퍼 2상 스테인리스강의 미세조직 및 기계적 성질에 미치는 시효의 영향)

  • Kim, Su-Chun;Kang, Chang-Yong
    • Journal of Ocean Engineering and Technology
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    • v.23 no.3
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    • pp.40-45
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    • 2009
  • With the increase in the annealing temperature, the volume fraction of austenite phase increased and the volume fraction of ferrite phase decreased. In compliance with the addition of N, not only the volume fraction of austenite phase was increased but also the austenite structure was made larger. Volume fraction of ${\sigma}$ phase was increased by decreasing of the volume fraction of ferrite phase, with the increase in the aging time and in compliance with the addition of N. As increasing in volume fraction of ${\sigma}$ phase, tensile strength and hardness increased, while elongation and impact value decreased. Elongation slowly decreased and impact value rapidly decreased at the early stage of aging. By the added N, tensile strength, elongation, hardness and impact value was increased.

Dispersion and Forming of Alumina Powders via Crosslinkable Organic Molecules (가교가능한 유기화합물을 이용한 알루미나의 분산과 성형)

  • 김봉호;신평우;백운규;정연길;최성철;박철원
    • Journal of the Korean Ceramic Society
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    • v.32 no.2
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    • pp.217-226
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    • 1995
  • Alumina powders were dispersed using crosslinkable organic molecules by electrosteric stabilization and then consolidated by crosslinking of organic molecules. The effect of processing variables such as the physicochemical properties of both solvent media and organic molecules, the proportions of mixed organic media, etc. were studied. FT-IR was used todeduce the mechanism of organic molecules adsorption on the alumina particle surfaces. The adsorption characteristics and the electrokinetic behavior of alumina suspensions were correlated with the stability of particle in alumina suspension using rheological measurements. The green body of alumina consolidated by the chemical crosslinking of the adsorbed organic molecules after the alumina suspension had been stabilized was tough enough for green machining and the sintered alumina fabricated by this proposed process also showed a high bending strength and a homogeneous microstructure.

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Analysis of Tube Expansion by Hydroforming (하이드로포밍에 의한 튜브 확관에 대한 해석)

  • Lee, Jae-Won;Park, Jong-Jin
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.11
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    • pp.2253-2261
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    • 2002
  • Recently the hydroforming technology has drawn a lot of attention because of its capability to produce high quality and light weight parts. In the present study, the tube expansion - one of the simplest hydroforming processes, has been investigated in order to understand fundamental phenomena such as deformation characteristics and effect of process parameters. As a result, the most important process parameters, which determine the state of stress at the expanded zone, were found to be pressure and die displacement. If the stress becomes equi-axial tension at the zone, necking occurs at some distance from the weld line and develops into a crack along the axial direction. Some aspects of mechanical property measurements as well as distributions of hardness and microstructure are also discussed in this paper.