• Journal of Korea Foundry Society
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• v.22 no.5
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• pp.238-244
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• 2002

Water and oil were completely synthesised with ultrasonic vibration energy irradiation. Pure Pb were added into Al melt during irradiated the ultrasonic vibration energy in 750. And the ultrasonic vibration energy was applied to Al-Pb melt to enhance the miscibility. Microstructural analysis, thermal analysis and X-ray diffraction analysis were carried out to evaluate the effect of the ultrasonic vibration energy on the castability and microstructural reliability. (1) Using the ultrasonic vibration energy irradiation, the complete mixing of water and oil was obtained. (2) The microstructure was refined by the application of ultrasonic vibration energy in Al-Pb alloys. (3) Relatively large Pb particles, $5{\mu}m$ were most distributed alone the grain boundaries with fine Pb particles evenly distributed in the matrix. (4) The solubility of Ph in Al-Pb alloys was increases up to 5% with the application of ultrasonic vibration energy.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.8 no.4
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• pp.123-129
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• 1999

Although type 316 stainless steel is widely used such as in reactors of petrochemical plants and pipes of steam power plants and s attracting attention as potential basic material for the fast breeder reactor structure alloys in nuclear power plants and is attracting attention as potential basic material for the fast breeder reactor structure alloys in nuclear power plants the effect of precipitates which form during the long term exposure at service temperature on creep properties is not known sufficiently. In this study to investigate the creep properties and the influence of prior aging on the microstructure to form precipitates specimens were first solutionized at 113$0^{\circ}C$ for 20 minutes and then aged for different times of 0 hr, 100 hrs, 1000 hrs and 2200 hrs at 75$0^{\circ}C$ After heat treatments tensile tests both at room temperature and $650^{\circ}C$ and constant load creep ruptuere tests were carried out.

• Korean Journal of Materials Research
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• v.14 no.1
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• pp.1-8
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• 2004

Laser weldability of aluminized steels for deep drawing application has been investigated. Test coupons for Nd:YAG laser welding and $CO_2$ laser welding were prepared trom the commercial steels. According to the test results, total penetration and back bead width of aluminized steels were sensitive to the welding conditions. Bead width at the half thickness of the overlap joint, however, was rather constant. Laser weldability of aluminized steels was superior to that of zinc coated steel. Weld microstructure revealed that overlap zone adjacent to the fusion line was filled with coated materials, which was thought to be desirable to protect weld from crevice corrosion. The aluminum coated materials was also found in the weld metal. Practically no spattering was observed in the laser welding of aluminized steels even when the welding was performed without joint gap. In the welding of zinc coated steel, however, spattering was so severe that it was difficult to get the acceptable weld. Bead quality of aluminized steel laser weld was smooth and stable.

• Proceedings of the Korea Association of Crystal Growth Conference
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• 2000.06a
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• pp.243-248
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• 2000

Effect of NiO addition on microstructure, stability of tetragonal phase and mechanical properties was investigated. (Y, Ni)-TZP solid solution was obtained by pressureless sintering. The fracture toughness was increased by solid solution of NiO. Neither reaction phase nor glassy phase was observed at the grain boundaries. From these results, it was determined that solid solution of NiO was destabilized tetragonal phase of Y-TZP. Y-TZP/Ni nanocomposite that contained nano-sized Ni particles was also fabricated by internal reduction method. Some evaluations and discussions were carried out for both (Y, Ni)-TZP solid solution and Y-TZP/Ni nanocomposite.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.10a
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• pp.139-141
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• 2009

This study analyzed the effect of the microstructure and alloying element on hydrogen-induced delayed fracture properties for the Energy Saving Wire (ESW) developed recently. Specimens were produced with a diameter 6.5mm post to the deformation (0, 10, 20 and 30%), followed by injecting the hydrogen. The experimental results by using GAS chromatography showed that the more hydrogen was emitted for high-carbon steel (0.45%C steel and 0.35%C steel) than low-carbon steel(0.2%C-Cr steel and 0.2%C-Cr-Mo steel). And, 0.45%C steel, 0.35%C steel and 0.2%C-Cr-Mo steel exhibited the crack for 30% deformed specimen. The hydrogen emitted was analyzed with the amount, the spheroidization, and the size of the carbides.

• Journal of the Korean Society for Heat Treatment
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• v.22 no.2
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• pp.80-87
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• 2009

Effects of retained austenite contents on ductility of medium carbon spring steels according to steel alloy compositions and heat treatment conditions were studied. Contents of retained austenite varied with steel compositions and heat treatment conditions, and some retained austenite were found to transform to martensite on stress. Reduction of area (RA) increased with contents of retained austenite, then saturated through its maximum, and subsequently decreased. Increase in RA with retained austenite contents could be due to crack blunting effect by retained austenite on stress, however, more contents of martensite transformed from retained austenite in its higher contents could cause decrease in RA.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.26 no.12
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• pp.867-871
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• 2013

The Ti adhesion layers were deposited onto the glass substrate for transparent capacitors using $Bi_2Mg_{2/3}Nb_{4/3}O_7$ (BMNO) dielectric thin films. Graphene was transferred onto the Ti/glass substrate after growing onto the Ni/$SiO_2$/Si using rapid-thermal pulse CVD (RTPCVD). The BMNO dielectric thin films were investigated for the microstructure, dielectric and leakage properties in the case of capacitors with and without Ti adhesion layers. Leakage current and dielectric properties were strongly dependent on the Ti adhesion layers grown for graphene bottom electrode.

• Bulletin of the Korean Chemical Society
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• v.35 no.9
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• pp.2689-2693
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• 2014

The control over microstructure in block copolymer thin films using external electric fields has become an interesting research topic. In this article, the effect of nanoparticle on the microdomain alignments in block copolymer (polystyrene-b-poly(2-vinylpyridine)/nanoparticle (Au) thin films under electric fields has been examined with transmission electron microscopy. The homogeneous dispersion of Au nanoparticles into the block copolymer matrix was achieved by surface modification of nanoparticles with compatible ligands. Compared with the phenomenon seen in the pristine block copolymer thin films, a peculiar alignment behavior was observed in the block copolymer/nanoparticle hybrid thin films under electric fields. In addition, the different pathways observed in the pristine and nanoparticle incorporated block copolymer thin films were also monitored as a function of exposure time. This work can provide the fundamental information for understanding microdomain alignment in block copolymer/nanoparticle thin films under external electric fields.

• Applied Microscopy
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• v.45 no.4
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• pp.189-194
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• 2015

Backside Ar ion milling technique for the preparation of cross-sectional transmission electron microscopy (TEM) specimens, and backside-ion milling combined with focused ion beam (FIB) operation for electron holography were introduced in this paper. The backside Ar ion milling technique offers advantages in preparing cross-sectional specimens having thin, smooth and uniform surfaces with low surface damages. The back-side ion milling combined with the FIB technique could be used to observe the two-dimensional p-n junction profiles in semiconductors with the sample quality sufficient for an electron holography study. These techniques have useful applications for accurate TEM analysis of the microstructure of materials or electronic devices such as arrayed hole patterns, three-dimensional integrated circuits, and also relatively thick layers (> $1{\mu}m$).

• Transactions of the Korean Society of Mechanical Engineers
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• v.8 no.1
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• pp.34-40
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• 1984

In this study, martensite-ferrite dual phase steel composed of martensite in hard phase and ferrite in soft phase is made as model material, and the difference of fatigue crack propagation behavior resulted from the structural size is investigated by fracture mechanics and microstructural method. The main results obtained are as follows; 1)Fatigue crack propagation rate is influenced by ferrite grain size. In other words, in the low .DELTA. K region fatigue crack propagation rate is decreased with decreasing of grain size but the difference of propagation rate resulted from the structural size is decreased as .DELTA.K is increased. 2)The above result is explained by the degree of crack arrest effect of second phase for fatigue crack propagation depending on the ratio of reversed plastic zone size to ferrite grain size.