• Title/Summary/Keyword: microstructure effect

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Mechanical Properties and Ultrasonic Characteristic of SS400 and STS304 by Simulated Heats (열재현에 의한 SS300 및 STS304의 기계적 성질 및 초음파 특성)

  • Jeong, Jeong-Hwan;Ahn, Seok-Hwan;Park, In-Duck;Nam, Ki-Woo
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2003.10a
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    • pp.127-132
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    • 2003
  • In a today industry, the welding is doing a many portion in structure manufacture. This study is simulated heat of heat-effected zone and researched a mechanical properties and ultrasonic characteristic in used the SS400 and the STS304. As the result mechanical properties of steel that become drawing decreased because of remaining stress by strain gardening according as simulated heat temperature rises, but according as temperature rises in material that do simulated heat after have done annealing, mechanical propensity was improved. The velocity and attenuation become different by effect of remaining stress than effect of material internal microstructure in ultrasonic wave test. In the case of STS304, there was change in mechanical properties by effect that is by strain hardening, but there was no change in material that simulated heat after annealing. When become drawing in ultrasonic waves test, according as simulated heat temperatures rise, change of attenuation coefficient is looked, but material that simulated heat after annealing was no change almost both the volocity and attenuation.

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A Study on the Surface Modification of Graphite by CVD SiC -Growth Characteristics of SiC in a Horizontal CVD Reactor- (화학증착 탄화규소에 의한 흑연의 표면개질 연구 -수평형 화학증착반응관에서 탄화규소 성장특성-)

  • 김동주;최두진;김영욱;박상환
    • Journal of the Korean Ceramic Society
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    • v.32 no.4
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    • pp.419-428
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    • 1995
  • Polycrystalline silicon carbide (SiC) thick films were depostied by low pressure chemical vapor deposition (LPCVD) using CH3SiCl3 (MTS) and H2 gaseous mixture onto isotropic graphite substrate. Effects of deposition variables on the SiC film were investigated. Deposition rate had been found to be surface-reaction controlled below reactor temperature of 120$0^{\circ}C$ and mass-transport controlled over 125$0^{\circ}C$. Apparent activation energy value decreased below 120$0^{\circ}C$ and deposition rate decreased above 125$0^{\circ}C$ by depletion effect of the reactant gas in the direction of flow in a horizontal hot wall reactor. Microstructure of the as-deposited SiC films was strongly influenced by deposition temperature and position. Microstructural change occurred greater in the mass transport controlled region than surface reaction controlled region. The as-deposited SiC layers in this experiment showed stoichiometric composition and there were no polytype except for $\beta$-SiC. The preferred orientation plane of the polycrystalline SiC layers was (220) plane at a high reactant gas concentration in the mass transfer controlled region. As depletion effect of reactant concentration was increased, SiC films preferentially grow as (111) plane.

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Effect of Cu Content on Microstructural and Magnetic Properties of a Nd-Fe-B Strip Cast (Cu 첨가에 따른 Nd-Fe-B strip cast의 미세조직과 자기적 특성의 상관관계)

  • Park, Song-E;Kim, Tae-Hoon;Lee, Seong-Rae;Kim, Dong-Hwan;NamKung, Seok;Jang, Tae-Suk
    • Journal of Powder Materials
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    • v.18 no.1
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    • pp.24-28
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    • 2011
  • Effect of Cu content on microstructural and magnetic properties of a $(Nd_{26.06},Dy_{6.51})Fe_{bal.}$ $Cu_xB_{0.97}$(wt.%), (x = 0.2, 0.3, 0.4, 0.5) strip-cast was studied. The average inter-lamellar spacing in the free surface and wheel side of the strip cast increased as the Cu content increases. The grain uniformity, the grain alignment, and (00L) texture of the strip cast increased with Cu contents up to 0.4 wt.%. These microstructural changes were attributed to the decrease of the effective cooling rate of the melted alloy caused by the decrease of the melting temperature of resulting from Cu addition. Coercivity and remanence were increased because of the grain alignment and (00L) texture improvement with Cu contents up to 0.4 wt.%.

Effect of Prior Deformation and Cyclic Transformation on the Mechanical Properties in Fe-30 Ni-0.24C Alloy (Fe-30 Ni-0.24C합금에서 역변태 오스테나이트의 기계적 성질에 미치는 이전가공도 및 역변태 Cycle수의 영향)

  • Kim, H.S.;Lee, K.B.;Hong, S.K.
    • Journal of the Korean Society for Heat Treatment
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    • v.3 no.4
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    • pp.1-9
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    • 1990
  • In this study, the ausformed martensite cooled to $-196^{\circ}C$ with various deformation degrees in Fe-30%Ni-0.24%C alloy was transformed to reversed austenite at $500^{\circ}C$ by cyclic reverse martensitic transformation. The effects of prior deformation and the number of cyclic reverse transformation on the microstructure and the mechanical properities of reversed anstensite were investigated. Experimental results showed that the strength of reversed austenite was higher than that of original austenite. This is due to higher dislocation density and grain refining. The reversed austenite formed from ausformed martensite was highly strengthened by prior deformation. This strengthening effect of reversed austenite is attributed to higher dislocation density than grain fefining. The yield strength of reversed austenite below 30% prior deformation, but above 30% prior deformation the strength of reversed austenite is lower than that of deformed austenite. This is due to partly disappearance of strain hardening effect at higher deformation degree by reverse transformation. The strength of reversed austenite is increased with the number of cyclic transformation. Especially, it is principally strengthened by the first cyclic transformation and shows higher increase in yield strength than that of ultimate tensile strength.

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The Effect of Additives on Twins in ZnO Varistors (ZnO 바리스터에서 첨가물이 쌍정에 미치는 영향)

  • 한세원;조한구;강형부
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.1057-1060
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    • 2001
  • By comparison of the experimental results in two systems of ZnO varistors, its appear that Sb$_2$O$_3$is the indispensable element for twinning in ZnO varistors, and the Zn$_{7}$Sb$_2$O$_{12}$ spinel acts as the nucleus to form twins. A1$_2$O$_3$is not the origin of twinning in ZnO varistor, but it was found that A1$_2$O$_3$could strengthen the twinning and form a deformation twinning by ZnA$_{12}$O$_4$-dragging and pinning effect. The inhibition ratios of grain growth and nonuniformity of two systems ZnO varistors increase with the increase of A1$_2$O$_3$content. The twins affect the inhibition of grain growth, the mechanism could be explained follow as : twins increase the mobility viscosity of ZnO grain and grain boundary, and drag ZnO grain and liquid grain boundary during the sintering, then the grain growth is inhibited, and the microstructure becomes more uniform.orm.m.

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Effect of SiO2, Al2O3, and Clay Additions on the Sintering Characteristics of Zircon (Silica, Alumnia, Clay를 첨가한 지르콘의 소결특성에 미치는 영향)

  • Lee, Keun-Bong;Jung, Seung-Hwa;Lee, Ju-Sung;Hong, Gyung-Pyo;Jo, Bum-Rae;Moon, Jong-Su;Kang, Jong-Bong
    • Korean Journal of Materials Research
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    • v.18 no.7
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    • pp.352-356
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    • 2008
  • Effect The effect of sintering additives ($SiO_2$, $Al_2O_3$, Clay) on the mechanical characteristics of sintered zircon was investigated. 1 vol% of additives in zircon powder was was sintered at $120{\sim}1500^{\circ}C$, the mechanical characteristics were measured, and microstructure analysis were was conducted. $Al_2O_3$ and clay additions increase the formation of monoclinic and tetragonal-$ZrO_2$ formation. An addition of SiO2 addition suppressed the formation of tetragonal-$ZrO_2$ formation., The A specimen sintered at $1400^{\circ}C$ showed the a density of $4.05\;g/cm^3$ and the a microhardness of 1120 HV, respectively.

Effect of Micro-Alloying Elements on Recrystallization Behavior of Carbon Steels at Different Strain Rates (변형률 속도에 따른 탄소강의 재결정 거동에 미치는 미량 합금 원소의 영향)

  • Lee, Sang-In;Lim, Hyeon-Seok;Hwang, Byoungchul
    • Korean Journal of Materials Research
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    • v.26 no.10
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    • pp.535-541
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    • 2016
  • The present study deals with the effects of micro-alloying elements such as Ni, V, and Ti on the recrystallization behavior of carbon steels at different strain rates. Eight steel specimens were fabricated by varying the chemical composition and reheating temperature; then, a high-temperature compressive deformation test was conducted in order to investigate the relationship of the microstructure and the recrystallization behavior. The specimens containing micro-alloying elements had smaller prior austenite grain sizes than those of the other specimens, presumably due to the pinning effect of the formation of carbonitrides and AlN precipitates at the austenite grain boundaries. The high-temperature compressive deformation test results indicate that dynamic recrystallization behavior was suppressed in the specimens with micro-alloying elements, particularly at increased strain rate, because of the pinning effect of precipitates, grain boundary dragging and lattice misfit effects of solute atoms, although the strength increased with increasing strain rate.

Effects of Titanium, Hafnium and Zircornium Alloying Elements on Microstructures and $D0_3{\leftrightarrow}B2$ Transition Temperature of Fe-30Al-5Cr Alloys (Fe-30Al-5Cr 합금의 미세조직 및 $D0_3{\leftrightarrow}B2$ 천이온도에 미치는 Ti, Hf 및 Zr의 첨가효과)

  • Kim, Sung-Su;Joo, Sung-Min;Oh, Seon-Hun;Kim, Kwan-Hyu;Choi, Dap-Chun
    • Journal of Korea Foundry Society
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    • v.21 no.1
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    • pp.15-23
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    • 2001
  • The changes in the microstructures and $D0_3{\leftrightarrow}B2$ transition temperature were investigated for Fe-30at.%AI-5at.%Cr alloy with the ordered $D0_3$, structure when Ti, Hf and Zr were added respectively. The addition of Cr has no effect on the microstructure. However, as the amount of Ti addition increased, the grain size became smaller. Addition of Ti+Hf, Ti+Zr and Ti+Hf+Zr also showed the similar effect. When 20at.% of Ti was added, the second phase precipitates on the substrate. The addition of Cr, Hf and Zr alone has no effect on $D0_3{\leftrightarrow}B2$ transition temperature. However, as the amount of Ti addition increased by 5, 10, 15 and 20at.%, the transition temperatures showed 929, 930, 960 and $930^{\circ}C$ respectively.

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The Study on the Unidrectionally Solidified $AI-CuAl_2$ Eutectic Composites(1) (Effect of Solidification Condition and Vibration on the Microstructure) (일방향 응고한 $AI-CuAl_2$공정복합재료에 관한 연구(1)(미세조직에 미치는 응고조건과 진동의 영향))

  • Lee, Hyeon-Gyu;Hong, Jong-Hwi
    • Korean Journal of Materials Research
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    • v.4 no.2
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    • pp.177-186
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    • 1994
  • The effect of solidification condition and vibration on structure refinement was investigatedfor unidirectionally solidified $AI-CuAI_{2}$ eutectic composites. Eutectic composites were unidirectionally solidifiedunder vibration with variation of growth rates (R) and thermal gradient((G), $32^{\circ}C$/cm, and 35$^{\circ}C$/cm. The lamellar structure was varied according to growth condition(G/R ratio). For the structure refinementthe effect of G/R was found out to be greater rather than that of vibration. The interlamellarspacing(l) in this materials was varied with the growth rates(R) by "$\lambda^{2}R$=Constant" relationshipquot; relationship

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Effect of Chemical Composition on Tensile Property in TRIP-assisted Multiphase Steel for Automobile Structure (차량구조용 변태유기소성(TRIP)형 복합조직강의 인장성질에 미치는 화학조성의 영향)

  • Lee, Ki-Yeol;Bang, Il-Hwan;Ma, Ah-Ram;Kim, Young-Sun
    • Transactions of the Korean Society of Automotive Engineers
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    • v.15 no.3
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    • pp.106-113
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    • 2007
  • The effect of chemical composition on the microstructural change and tensile property in TRIP-assisted steels with different chemical composition was investigated by using SEM, TEM, XRD and UTM. As a result of microscopic observation, the morphology of retained austenite could be identified as two types : a granular type in a steel containing higher sillicon and a film type in a steel having higher carbon. For the case of higher carbon-containing steel with a tensile strength of 860 MPa and a total elongation of 38%, film-typed retained austenite could be observed between lath bainitic ferrite. Actually, metastable retained austenite was a requisite for the good formability, which means that chemical composition plays a significant role in the microstructure and tensile property of TRIP-assisted steels. With respect to tensile property, the steels containing suitable silicon and manganese, respectively, showed a typical TRIP effect in stress-strain curve, while a steel containing higher manganese content exhibited the assimilar behavior shown in dual phase steel.