• Transactions of the Korean Society of Pressure Vessels and Piping
• /
• v.10 no.1
• /
• pp.82-89
• /
• 2014

In this study, the metallurgical analysis and mechanical property measurement have been performed to investigate the effect of long-term thermal aging on the microstructural evolution in the fusion boundary region between weld metal and low alloy steel in dissimilar metal welds. A representative dissimilar weld mock-up made of Alloy 690-Alloy 152-A533 Gr. B was fabricated and aged at $450^{\circ}C$ for 2,750 hours. The microstructural characterization was conducted mainly near in a weld root region by using optical microscopy, scanning electron microscopy, transmission electron microscopy. And the mechanical properties were measured with Vickers microhardness test and nanoindentation method. A steep gradient was shown in the chemical composition profile across the interface between A533 Gr. B and Alloy 152. Type-II boundaries were found in weld side of DMW and the hardness was the highest at the narrow zone between Type-II boundary and fusion boundary.

• Transactions of the Korean Society of Pressure Vessels and Piping
• /
• v.12 no.1
• /
• pp.41-48
• /
• 2016

To investigate the effect of long-term thermal aging on the microstructural and mechanical characteristics of weldment made of nickel base alloy and its weld metal, an accelerated heat treatment was applied to simulate the process of long-term thermal aging in the operating condition of nuclear power plant. A representative nickel-based weldment with Alloy 600 and Alloy 182 was fabricated and heat-treated at $400^{\circ}C$ for 1,713 h and 3,427 h to simulate the thermal aging for the period equivalent to 15 and 30 years in operating pressurized water reactors, respectively. The microstructural and mechanical characteristics were analyzed by using optical microscopy, scanning electron microscopy and Vickers microhardness measurement. Changes were observed in precipitation behavior and microhardness of each specimen, and these changes were mainly attributed to the change in precipitated morphology and residual stress across the weld during the thermal aging process.

• Advances in materials Research
• /
• v.9 no.3
• /
• pp.203-218
• /
• 2020

This research paper presents the outcomes in terms of mechanical and microstructural characteristics of binary and ternary concrete when exposed to elevated temperature. Three parameter were taken into account, (a) elevated temperature (i.e., 200, 400, 600 and 800℃) (b) binary concrete with cementitious material sugarcane bagasse ash (SCBA) and ground granulated blast furnace slag (GGBFS) replacement percentage (i.e., 0, 15, 20, 25 and 30%) and (c) ternary concrete with cementitious material SCBA and GGBFS replacement percentage (i.e., 0, 15, 20, 25 and 30%). A total of 285 standard cube specimens (150 mm × 150 mm × 150 mm) containing Ordinary Portland Cement (OPC), SCBA, and GGBFS were made. These specimens then exposed to several elevated temperatures for 2 h, afterword is allowed to cool at room temperature. The following basic physical, mechanical, and microstructural characteristics were then determined and discussed. (a) mass loss ratio, (b) ultrasonic pulse velocity (UPV) (c) physical behavior, (d) compressive strength, and (e) field emission scanning electron microscope (FESEM). It was found that compressive strength increases up to 400℃; beyond this temperature, it decreases. UPV value and massloss decrease with increase in temperature as well as the change in color and crack were observed at a higher temperature.

• Metals and materials international
• /
• v.24 no.6
• /
• pp.1285-1292
• /
• 2018

Microstructural properties of as-grown and annealed CoCrFeMnNi high entropy alloy (HEA) oxynitride thin films were investigated. The CoCrFeMnNi HEA oxynitride thin film was grown by magnetron sputtering method using an air gas, and annealed under the argon plus air flow for 5 h at $800^{\circ}C$. The as-grown film was homogeneous and uniform composed of nanometer-sized crystalline regions mixed with amorphous-like phase. The crystalline phase in the as-grown film was face centered cubic structure with the lattice constant of 0.4242 nm. Significant microstructural changes were observed after the annealing process. First, it was fully recrystallized and grain growth happened. Second, Ni-rich region was observed in nanometer-scale range. Third, phase change happened and it was determined to be $Fe_3O_4$ spinel structure with the lattice constant of 0.8326 nm. Hardness and Young's modulus of the as-grown film were 4.1 and 150.5 GPa, while those were 9.4 and 156.4 GPa for the annealed film, respectively.

• Korean Journal of Metals and Materials
• /
• v.46 no.12
• /
• pp.771-779
• /
• 2008

An effective way of increasing the strength and fracture toughness of reactor pressure vessel steels is to change the material specification from that of Mn-Mo-Ni low alloy steel(SA508 Gr.3) to Ni-Mo-Cr low alloy steel(SA508 Gr.4N). In this study, we evaluate the effects of alloying elements on the microstructural characteristics of Ni-Mo-Cr low alloy steel. The changes in the stable phase of the SA508 Gr.4N low alloy steel with alloying elements were evaluated by means of a thermodynamic calculation conducted with the software ThermoCalc. The changes were then compared with the observed microstructural results. The calculation of Ni-Mo-Cr low alloy steels confirms that the ferrite formation temperature decreases as the Ni content increases because of the austenite stabilization effect. Consequently, in the microscopic observation, the lath martensitic structure becomes finer as the Ni content increases. However, Ni does not affect the carbide phases such as $M_{23}C_6 $ and $M_7C_3$. When the Cr content decreases, the carbide phases become unstable and carbide coarsening can be observed. With an increase in the Mo content, the $M_2C$ phase becomes stable instead of the $M_7C_3$ phase. This behavior is also observed in TEM. From the calculation results and the observation results of the microstructure, the thermodynamic calculation can be used to predict the precipitation behavior.

• Proceedings of the Korean Society of Rheology Conference
• /
• 2002.05a
• /
• pp.17-20
• /
• 2002

• Proceedings of the Korean Powder Metallurgy Institute Conference
• /
• 1993.11a
• /
• pp.29-29
• /
• 1993

• Proceedings of the Materials Research Society of Korea Conference
• /
• 1999.05a
• /
• pp.118-118
• /
• 1999

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 1989.06a
• /
• pp.107-109
• /
• 1989

Based on the ferroelectric microstructural residual stress model, the relation between grain size and residual elastic energy was proposed. It was found that the residual elastic energy increased with decreasing grain size by modeling and DSC results. This residual elastic energy change with grain size which induce the phase transituion mode change was the cause of a diffuse phase transition in small grain size.

• Journal of Powder Materials
• /
• v.7 no.4
• /
• pp.237-243
• /
• 2000

The property and performance of the $Al_2O_3/Ni$ nanocomposites have been known to strongly depend on the structural feature of Ni nanodispersoids which affects considerably the structure of matrix. Such nanodispersoids undergo structural evolution in the process of consolidation. Thus, it is very important to understand the microstructural development of Ni nanodispersoids depending on the structure change of the matrix by consolidation. The present investigation has focused on the growth mechanism of Ni nanodispersoids in the initial stage of sintering. $Al_2O_3/Ni$ powder mixtures were prepared by wet ball milling and hydrogen reduction of $Al_2O_3$ and Ni oxide powders. Microstructural development and the growth mechanism of Ni dispersion during isothermal sintering were investigated depending on the porosity and structure of powder compacts. The growth mechanism of Ni was discussed based upon the reported kinetic mechanisms. It is found that the growth mechanism is closely related to the structural change of the compacts that affect material transport for coarsening. The result revealed that with decreasing porosity by consolidation the growth mechanism of Ni nanoparticles is changed from the migration-coalescence process to the interparticle transport mechanism.