• 한국표면공학회지
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• 제31권2호
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• pp.91-100
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• 1998

NiCrAlY/YSZ(8wt%$Y_2O_3-ZrO_2$) functionally graded thermal barrier coating (FGC) layers on a Co-base superalloy (HAYNESS 188) substrate were fabstrate were fabicated using Ar shielded single torch air plasma spraying method. Functional grading with the stepwise compositional change throughout layer thickness. Microstructural observation trvealed a successful fabrication of NiCrAlY/YSZ FGC. From the results of the curvature measurement, adhesive strength measurement and thermal shock test for the FGC, it was concluded that the optimum conditions of functionally graded coating layer thinkness and compositional pattern exit to enhance the properties of FGC, which is closely related to the internal residual stess distribution witin it.

• 한국공작기계학회논문집
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• 제10권5호
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• pp.110-117
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• 2001

In the weldments, the crack propagation rate is changed due to the residual stress. The crack propagation rate is high in the region with the residual stress. However it shows the same behavior with the base metal in the region that does not include the residual stress. The fatigue crack growth rate for the material with residual stresses can be predicted more precisely by using the effective stress ratio. The difference between experimental results and prediction results seems to be due to the redistribution of the residual stresses and microstructural change.

• 한국세라믹학회지
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• 제27권6호
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• pp.824-828
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• 1990

Zirconia gel fibers were fabricated by sol-gel processing using zirconium alkoxides and 2, 4-pentanedione. Their phase transformation and microstructural evolution were studied after heat treatments up to 150$0^{\circ}C$. Tetragonal ZrO2 began to form at 50$0^{\circ}C$ and followed by monoclinic, tetragonal phase during subsequent heat treatments at 1000, 150$0^{\circ}C$ for 1hour respectively. During cooling from 150$0^{\circ}C$, cracks were created, propagated along grain boundaries due to the volume change from tetragonal to monoclinic transformation.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1996년도 추계학술대회 논문집 학회본부
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• pp.464-467
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• 1996

The microstructural evolution during mechanical alloying of Nb and Sn powders, of average composition Nb3Sn, has been investigated by X-ray diffraction(XRD) and scanning electron microscopy(SEM). Observations by SEM showed a progressive change of milling time. From the XRD studies, the structural development with milling time depends on the ball size for a given powder/ball ratio. Using a larger ball of 9.5mm diameter, the elemental powders initially alloy mechanically to form an A15 structure phase, and then amorphised with continued milling. However, in case of milling with a smaller ball of 3.968mm diameter, an amorphous phase is first formed. These results can be understood by considering the dependence of the milling energy on the ball size. The homogeneous stoichiometric $Nb_3Sn$ phase could be easily obtained by heat treatment of a supersaturated solid solution produced by MA. Heat treatment of an amorphous phase formed by MA resulted in the mixture of the $Nb_3Sn$ and $Nb_6Sn_5$ phases.

• 한국주조공학회지
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• 제19권5호
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• pp.433-439
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• 1999

Rapidly solidified Mg-Al-Si base alloys containing Ca were obtained by melt spinning. The melt-spun ribbons were aged isochronally or isothermally to investigate age hardening phenomena and microstructural change according to the alloy composition. Age hardening occurred after aging at $200^{\circ}C$ for 1h mainly due to the precipitation of $Al_2Ca$ and $Mg_2Ca$, which have coherent interfaces with the matrix. With the increase of Ca content, the hardness values of the alloy ribbons were increased. Among the alloys, Mg-10Al-2 Si-3Ca alloy showed a good thermal stability at elevated temperature.

• Korea-Australia Rheology Journal
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• 제17권4호
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• pp.171-180
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• 2005

We present numerical results for inertialess elliptic particle suspensions in a Newtonian fluid subject to simple shear flow, using the sliding bi-periodic frame concept of Hwang et al. (2004) such that a particulate system with a small number of particles could represent a suspension system containing a large number of particles. We report the motion and configurational change of elliptic particles in simple shear flow and discuss the inter-relationship with the bulk shear stress behaviors through several example problems of a single, two-interacting and ten particle problems in a sliding bi-periodic frame. The main objective is to check the feasibility of the direct simulation method for understanding the relationship between the microstructural evolution and the bulk material behaviors.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2005년도 춘계학술대회 논문집
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• pp.291-294
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• 2005

The microstructure evolution of Alloy 718 during the direct age(DA) process was predicted using the recrystallization model and finite element analysis. The DA process of Alloy 718 was performed in two-step forging using capsulated cylindrical billets of 122mm in diameter and 180mm in height. In order to evaluate the microstructural change during the forging, a dynamic recrystallization model of Alloy 718 was implemented onto the user-subroutine of the commercial FEM code. The prediction of microstructure evolution in DA processed Alloy 718 pancake was compared with experimental results.

• Journal of Welding and Joining
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• 제5권3호
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• pp.28-37
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• 1987

To clarify the debonding phenomena of clad steel, the effect of thermal treatment (temperature, holding time) on the interfacial strength of clad steel was preliminarily investigated. From this study, it was confirmed that the interfacial strength of clad steel was deteriorated by thermal treatment and the amount of strength deteriorated, depending on the condition of thermal treatment, could be evaluated by the following equation. ${\sigma}_{ HT}/{\sigma}_{i}/=A_{0}-A\;exp(-Q/RT)log(t/t_{0})$ This equation implies that temperature has a far strong effect on strength deterioration than tiem. The deterioration of interfacial strength of clad steel after thermal treatment may be derived from the thermal stress caused by the difference in thermal expansion coefficient between component materials and microstructural change along the interface.

• Journal of Welding and Joining
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• 제1권2호
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• pp.53-60
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• 1983

COD test based on fracture mechanics concept was used in this study to evaluate the fracture toughness quantitatively. Effects of specimen sizes on critical COD value for ABS EH 36 steel and its submerged arc weldments, and the variation of critical COD value depending on metallurgical/mechanical heterogeneities caused by weld thermal cycles were investigated. Experiment was performed by using specimens made from base metal and submerged arc weldments according to BS 5762. Obtained results are summarized as follows; 1) Critical COD value for base metal decreases with increasing thickness of specimen. On hand, as the reduction ratio of critical COD decreases with increasing specimen thickness, critical COD value becomes constant above a thickness of specimen. 2) Critical COD value for weldment decreases with increasing thickness of specimen and was also affected by metallurgical states of base metal. 3) Size effects for weldment was greater at the hardened region. 4) Critical COD value was affected by microstructural change due to weld thermal cycles in weldments; that is, accicular ferrite formation is favorable for increasing of COD value.

• 한국재료학회지
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• 제15권11호
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• pp.730-734
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• 2005

Cr-Al-Si-N coatings were deposited on WC-Co substrates by a hybrid coating system of arc ion plating and DC magnet :on sputtering technique in $N_2/Ar$ mixture. The Cr-tll-Si-N coatings were synthesized with different Si contents. Their microstructure and mechanical properties were systematically investigated. The average size of crystallites largely decreases with the increase of Si content compared with Cr-Al-N. The microhardness of Cr-Al-Si-N coatings largely increases from 24 to 55 GPa. The enhanced hardness is believed to originate from the microstructural change by the fine composite microstructure of Cr-Al-N coatings with Si addition. The average friction coefficient of Cr-Al-Si-N coatings decreases from 0.84 to 0.45 with increasing Si content up to $16\;at.\%$.