• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 1997년도 고액공존금속의 성형기술 심포지엄
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• pp.183-195
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• 1997

The micorstructural characteristics, particularly $\alpha$-halo formation, in semi-solid state processed hypereutectic Al-Si alloy was investigated. The microstructural changes during reheating of wedge type mold cast ingot, hot-rolled sheet, and Si particulate reinforced Al composite was compared with those occurred during stirring of semi-solid state hypereutectic alloy. In the case of semi-solid state reheating of wedge type ingot and hot-rolled sheet, fine particles of Si as well as $\alpha$-halo formed after heat treatment. Although there seemed to be no coarsening with variations of holding time, the region of $\alpha$-halo decreased due to homogenization. Nucleation and recrystallization was accelerated with the addition of alloying elements during hot rolling resulting in primary Si particle size decrease and $\alpha$-halo formation. In the case of extruded specimens, very little morphological change of reinforcing Si particles was observed. Almost no $\alpha$-halo formed during reheating because of the oxide film formed on the reinforcing Si particles which acted as a diffusion barrier between the matrix and the primary Si particles.

• 열처리공학회지
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• 제33권2호
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• pp.72-79
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• 2020

To improve the mechanical properties of most structural materials for industrial applications, the control of microstructure is essential by heat treatment process or plastic deformation process. Since the mechanical behavior of structural materials is significantly influenced by their microstructure, it is inevitably preceded to understand the relationship between microstructure and strengthening mechanisms of materials which can be easily changed by heat treatment. In this regard, the nanoindentation test is useful technique for analyzing the influence of the localized microstructural change on small-scale mechanical behavior of various structural materials. Here, the interesting studies performed on various heat-treated materials are reviewed with focus on micromechanical properties obtained by nanoindentation, which are reported in the available literature.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2002년도 춘계학술대회 논문집
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• pp.169-172
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• 2002

Recently, the application of 3-roll mill is increasing, because of its flexibility in spread control and stand arrangements due to its compact size. But deformation characteristics and microstructural change in the process is not well known. In this study, austenite grain size (AGS) predictions were made by isothermal FE analyses and a microstructure model available in the literature. From this study, the effect of draught on the AGS characteristics was analyzed based on the divided zones of two major recrystallization behaviors.

• 소성∙가공
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• 제8권6호
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• pp.626-633
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• 1999

$Al_{85}Ni_{10}Y_5$ (at. %) amorphous alloy ribbons have been produced by rapidly solidification process and consolidated by the conventional powder metallurgy method. The grains with ∼90 nm were obtained in the Al85Ni10Y5 alloy extrudates by hot-pressing followed by hot-extusion. To investigate the effect of heat treatment on microstructural change of the extrudates, heat treatment was carried out from 200℃ to 400℃ at the step of 50℃. In addition, mechanical properties of the extrudates were analysed from torsion test at the temperature range or 400∼500℃ under a strain rates of 0.2, 0.5, and 1.0/sec. The extrudates showed a flow stress of ∼190 MPa and low elongation of ∼150% at 400℃, contributing to the enhancement of ductility and hardness for extrudates. Also, grain boundary sliding was occurred in the $Al_{85}Ni_{10}Y_5$ alloy during hot deformation.

• 한국표면공학회지
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• 제46권2호
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• pp.61-67
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• 2013

Thin film solar cells have attracted much attention due to their high cell efficiency, comparatively low process cost, and applicability to flexible substrates. In particular, CIGS solar cells have been widely studied and produced because they demonstrated the highest cell efficiency. However, the deposition process of CIGS films generally includes the selenization process conducted at elevated temperature using toxic $H_2Se$ gas. To avoid this selenization process, CIGS thin films were, in this study, deposited by RF sputtering using single composite CIGS target. In addition, the effects of sputtering bias voltage and heat treatment on the microstructural and morphological changes in deposited CIGS films were investigated and discussed.

• 한국표면공학회지
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• 제35권4호
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• pp.241-248
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• 2002

Hardfacing layers of Stellite 6 alloy with different molybdenum content are deposited on AISI 1045 carbon steel using plasma transferred arc welding (PTAW). The properties of the hardfacing layer are investigated in order to clarify the effect of molybdenum addition to the cobalt-base alloy. With an increase in molybdenum contents, the size of Cr-rich carbides in the interdendritic region is abruptly refined, but volume fraction of the carbide slightly increases. Also, with an increase of Mo, $M_{6}$ C type carbides are formed instead of Cr-rich $M_{7}$ $C_{3}$ type carbided, and this microstructural change enhanced the mechanical properties of Stellite 6 alloy.

• 한국세라믹학회지
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• 제38권10호
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• pp.876-880
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• 2001

The supported and unsupported boehmite ($\gamma$-AlOOH) membranes were prepared using a boehmite sol. The supported membrane was consisted of a porcelain support, two intermediate $\alpha-{Al_2}{O_3}$ layers, and a top boehmite membrane. XRD patterns showed that the supported top membrane had a higher $\theta-$ to $\alpha-{Al_2}{O_3}$ transformation temperature compared to the unsupported membrane. This result was also confirmed from microstructural study of the membrane. The shift in the phase transformation temperature should be explained by difference of a stress generated in the supported top membrane due to interaction between the support layers and the top membrane.

• 한국세라믹학회지
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• 제43권4호
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• pp.230-234
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• 2006

Metal-Induced Crystallization (MIC) of amorphous silicon (a-Si) using aluminum and nickel as catalysts were performed with a variation of metal thickness and temperature. Raman results showed that the crystallization of a-Si depended on the thickness of aluminum while not on nickel. Nickel that forms silicide nodules during annealing simply catalyzed the formation of crystalline silicon (c-Si) while aluminum was consumed and transferred during MIC, which resulted in more complex microstructural characteristics. Crystalline silicons after NIC had elongated shape with a twin along the long axis. Morphological change after Aluminum-Induced Crystallization (AIC) showed more equiaxial grains. The nucleation and growth mechanism of AIC was discussed.

• 한국기계연구소 소보
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• 통권19호
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• pp.43-52
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• 1989

Material damage of Unifiner Change Heater: Tube used for nearly 20 years was evaluated and Mechanical tests such as tensile tests and creep-rupture tests were conducted to predict the residual life. After the investigation, any major damage or degradation was not found except the welded zone. Microstructural observation showed that most of delta-ferrite was transformed. to sigma-phase and consequently, the ductility was very much reduced. A KLA(Knife-Line Attack) crack with 60mm in length and 2.8mm in depth was found just near the welded zone, which is believed to be caused by intergranular corrosion. Creep-rupture tests, which are very essential to predict the residual life, showed that both used base and weld metals have similar results with the reference data.

• Journal of Welding and Joining
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• 제1권1호
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• pp.47-55
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• 1983

The mechanical and microstructural properties in high heat input welds of home-made SM 50 high strength steels were investigated and compared with the manual shielded metal arc welds. Also, the fracture toughnesses of the simulated weld-bonds with various thermal cycles were quantatively examined in order to provide the basic data for further development of the high strength steels for high input welding. Main results obtained are as follows. (1) The embrittlement degree and the coarse grained region in high heat input welds appear to be extraordinarily large compared with the manual shielded metal arc welds, while the difference in change of nicrohardness is not so large in both welds. (2) The embrittleness in high heat input weld-bonds is mainly affected by the size of coarse grain rather than the microstructure. (3) The fracture toughness in high heat input weld-bonds can be improved by controlling the cooling rate from 800.deg.C to 500.deg.C rapidly.