• Proceedings of the Korean Society For Composite Materials Conference
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• 2004.10a
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• pp.39-42
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• 2004

Carbon nanofiber/Cu composite powder has been fabricated by electroless plating process. Microstructural evolution of the composite powder after heat treatment under vacuum, hydrogen and air environment was investigated. A dispersed carbon nanofiber coated by copper was produced at the as-plated condition. Carbon nanofiber is coated uniformly and densely with the plate shaped copper particles. The copper plates on the carbon nanofiber aggregate during the thermal exposure at elevated temperature in vacuum and hydrogen in order to reduce surface energy. The thermal exposure of the composite powder in air at $400^{\circ}C$ for 3 hours leads to the spherodization of the composite powder owing to oxidation of copper.

• Computers and Concrete
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• v.21 no.1
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• pp.39-46
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• 2018

With the increase in industrialization and urbanization, growing demand has enhanced rate of new constructions and old demolitions. To avoid serious environmental impacts and hazards recycled concrete aggregates (RCA) is being adopted in all over the world. This paper investigates successive recycled coarse aggregates (SRCA) in which old concrete made with RCA in form of concrete cubes was used. The cubes were crushed to prepare new concrete using aggregates from crushing of old concrete, used as SRCA. The mechanical behavior of concrete was determined containing SRCA; the properties of SRCA were evaluated and then compared with natural aggregates (NA). Replacement of NA with SRCA in ratio upto 100% by weight was studied for workability, mechanical properties and microstructural analysis. It was observed that with the increase in replacement ratio workability and compressive strength decreased but in acceptable limits so SRCA can be used in low strength concretes rather than high strength concrete structures.

• Journal of Industrial Technology
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• v.16
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• pp.169-174
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• 1996

Microstructural analyses of synthetic arsenic-containing heavy metal sludges solidified with Portland cement were performed. Heavy metal sludges containing 0.04M of cadmium, chromium, copper, lead, and arsenic were prepared by sodium hydroxide precipitation and successive vacuum filtration. The sludges mixed with cement were cured for 14 days. The solidified sample was characterized by 1) leaching test, 2) scanning electron microscopy and 3) X-ray diffractometry. Of the metals tested, only Pb concentration in the leachate exceeded the Korean regulatory limit. The level of lead in the leachate was as high as 10 times the regulatory limit. X-ray analysis suggested that the metal hydroxides might be present in complex or impure crystalline phases.

• Journal of the Korean Society for Heat Treatment
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• v.18 no.2
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• pp.83-90
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• 2005

Failure cause of the fractured engine parts was analyzed by microstructural observation. These parts were failed far earlier than the expected service life. By the stereoscope and SEM examinations of the fractured surface, the fracture modes have been identified as wear and fatigue failure. From the observation of microstructure and microhardness measurements of the failed gears, the probable cause for failures are internal oxidation during using and retained austenite and carbide networks due to heat-treatment, respectively. These defected structures at near surface contributed to the wear and fatigue failure.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1995.10a
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• pp.16-29
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• 1995

A full three-dimensional thermo-coupled rigid-viscoplastic finite element method and the currently developed microstructural evolution system which includes semi-empirical mathematical equations suggested by different research groups were used together to form an integrated system of process and microstructure simulation of hot rolling. The distribution and time history of thermomechanical variables such as temperature, strain, strain rate, and time during pass and between passes were obtained FEM analysis of multipass hot rolling processes. Then distribution of metallurgical variables were calculated successfully on the basis of instantaneous thermomechanical data. For the verification of this method the evolution of microstructure in plate rolling and shape rolling was simulated and their results were compared with the data available in literature. Consequently, this approach makes it passible to describe the realistic evolution of microstructure by avoiding the use of erroneous average value and can be used in CAE of multipass hot rolling.

• Transactions of Materials Processing
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• v.14 no.3 s.75
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• pp.215-223
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• 2005

A numerical analysis program is developed by FDM scheme for the prediction of microstructural transformation during heat treatment of steels. In this study, multi-phase model was used fur description of diffusional austenite transformations in low-alloy hypoeutectoid steels during cooling after austenitization. A fundamental property of the model consisting of coupled differential equations is that by taking into account the rate of austenite grain growth, it permits the prediction of the progress of ferrite, pearlite, and bainite transformations simultaneously during quenching and estimate the amount of martensite also by using K-M eq. In order to simulate the microstructural evolution during tempering process, another Avrami-type eq. was adopted and method for vickers hardness prediction was also proposed. To verify the developed program, the calculated results are compared with experimental ones of casting product. Based on these results, newly designed heat treatment process is proposed and it was proved to be effective for industry.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1995.06a
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• pp.81-90
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• 1995

Age hardenable aluminum alloys show high specific strength, good thermal and electrical conductivity as well as lightness, and are typical aircraft materials. High fatigue strength and good resistancy against stress corrosion cracking are also important for aircraft aluminum alloys. Al alloy 7050 has been developed to meet the above mentioned requirements and the use of this alloy as forged aircraft part becomes more important. However, forged 7050 parts showed undersirable structures such as severe local grain coarsening in surface area and unproper metal flow that is degrading mechanical properties. In this paper, microstructural aspects of die forging in the Al alloy 7050 are investigated. Also suggested are the optimal forging conditions for microstructural control of Al alloy 7050.

• Proceedings of the KWS Conference
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• 2004.05a
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• pp.156-158
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• 2004

The microstructural evolution in a 304 stainless steel weld during FSW was examined. The SZ and TMAZ showed typical dynamically recrystallized and recovered microstructures, respectively, The microstructural observation revealed that sigma phase was formed at the advancing side of the stir zone. A possibility was suggested that the rapid formation of the sigma phase is related to the transformation of austenite to delta-ferrite in the stir zone, from introduction of high strain and dynamic recrystallization during FSW.

• Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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• 2000.02a
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• pp.112-114
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• 2000

We fabricated BSCCO multifilaments superconductor tape and evaluated the effect of twisting on the microstructural evolution and critical current. Twist pitches of the tapes are in the range of 70 - 8 mm and uniformly deformed. It was observed that grain size and the degree of texture decreased as decreasing pith, probably due to the formation of the irregular interface between Ag and filaments. In addition, critical current of the tapes decreased to 6.5A with decreasing pitch to 8 mm, showing 48% of degradation compared to the untwisted tape(12.5 A). These reduction of critical current may be related to the interface irregularity, smaller grain size, worse texture and the presence of cracks due to the induced strain during twisting processing.

• Journal of Korea Foundry Society
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• v.10 no.5
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• pp.399-407
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• 1990

The effect of thermal cycling and isothermal exposure on the high temperature microstructural stability of unidirectionally solidified $Al-CuAl_2$ eutectic composite has been studied. A coarsening procedures of lamellar eutectic structures were initiated at growth fault region because of diffusion through low angle boundary at this region. It was considered that thermally induced residual stresses produced by thermal cycling were high enough to increase the dislocation density in Al-rich matrix phase. However, it was also considered that dislocations generated by these high thermal stresses were annihilated at high temperature by stress relaxation. Consequently, the thermal cycling up to 1440 cycles between 20 and $520^{\circ}C$ did not affect the microstructural stability.