• Title/Summary/Keyword: microscopic characteristics

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Effect on the Stabilizing Heat Treatment to Weld Joint for the USC Coal Boiler Tubes(SA213 TP347H) (초초임계 석탄발전 보일러 튜브(SA213 TP347H) 용접부 안정화 열처리 효과)

  • Ahn, Jong-Seok;Park, Jin-Keun;Lee, Gil-Jae;Yoon, Jae-Yeon
    • Journal of Welding and Joining
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    • v.33 no.4
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    • pp.30-36
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    • 2015
  • Austenite stainless steel(SA213-TP347H) has widely been used for the superheater & reheater tube in USC(ultra-supercritica) coal boiler because of its high creep rupture strength and anti-oxidation. But recently, the short-term failures have happened frequently in heat affected zone for only 4,000~15,000hours of service. Many investigations have been conducted to understand the failure mechanism. The root cause of failure was comfirmed to "strain induce participation hardening crack" or "reheat cracking". This mechanism often occurred due to weld residual stress and precipitation of the Cr, Nb carbides in the stabilized stainless steel such as TP347H. This paper presents an analysis of failure tube and effect of the sample tubes that conducting stabilizing heat treatment in site after 11,380hours & 16,961hours of service. Visual inspection was performed. In addition, microscopic characteristics was identified by O.M, SEM, and hardness test was carried out to find out the heat treatment effects. Failures seem to happen because of being not conducted stabilizing heat treatment in site. And another cause is inadequate weld parameter such as pass, ampere, voltage, inter-pass temperature. Thus, this paper has the purpose to describe that how to prevent similar failures in those weld-joints.

Community characteristics of early biofilms formed on water distribution pipe materials (수도관 재질에 형성된 초기 생물막 형성 미생물의 군집 특성)

  • Kim, Yeong-Kwan;Park, Sung-Gu;Lee, Dong-Hun;Choi, Sung-Chan
    • Journal of Korean Society of Water and Wastewater
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    • v.26 no.6
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    • pp.767-777
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    • 2012
  • Annular Biofilm Reactor (ABR) equipped with coupons of three different pipe materials (STS 304, PVC, PE) was used to generate drinking water biofilm samples. The level of assimilable organic carbon (AOC) during the sample generation period was $37.3{\mu}g/L$, and this level did not seem to be low enough to limit the formation of biofilm in this study. Terminal-restriction fragment length polymorphism (T-RFLP) analyses determined T-RF profile as early as 3 h of exposure on PVC coupons. Average surface roughness ($R_a$) measured by atomic force microscopic analyses was 125.7 nm for PVC, and this value was higher than for STS (71.6 nm) and PE (74.0 nm). However, biofilm formation was faster on STS (6 h) than on PE (12 h), which indicated that surface roughness might not be the only factor that controlled the initiation of biofilm development. Upon detection of the T-RF peaks, richness (S) and diversity indices such as Shannon (H) and Simpson (1/D) demonstrated a rather slow increase until 48 h followed by rapid increase regardless of the pipe materials. Differences of microbial community structures among the biofilm samples were determined based on the cluster analysis using Jaccard coefficients (Sj). Biofilm communities could be divided into two distinct groups according to the exposure time regardless of the pipe materials. First group contained a young (< 48 h) biofilm samples (10 out of 11) but second group contained a mature (${\geq}$ 48 h) samples (11 out of 14). Results suggested that, due to the complexity of biofilm, the targeting of the first group of cluster was crucial for optimizing the management of drinking water distribution systems and controlling microbial growth.

Variation of Axial Tension-Compression Fatigue Characteristics by UNSM on Ti-6Al-4V (Ti-6Al-4V재의 UNSM처리에 의한 축인장압축피로특성변화)

  • Suh, Chang-Min;Cho, Sung-Am;Pyoun, Young-Sik;Suh, Min-Soo
    • Journal of Ocean Engineering and Technology
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    • v.25 no.6
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    • pp.42-48
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    • 2011
  • The present study makes three original contributions to nanoskinned Ti-6Al-4V materials. The nanoskins were fabricated on Ti-6Al-4V material using various surface treatments: deep rolling (DR), laser shot peening (LSP), and ultrasonic nanocrystal surface modification (UNSM). These surface treatments are newly developed techniques and are becoming more popular in industrial fields. A fatigue strength comparison at up to 106 cycles was conducted on these nanoskinned Ti-6Al-4V materials. Fatigue tests were carried out using MTS under axial loading tension-compression fatigue (R = -1, RT, 5 Hz, sinusoidal wave). The analysis of the crack initiation patterns in the nanoskinned Ti-6Al-4V materials found an interior originating crack pattern and surface originating crack type. Microscopic observation was mainly used to investigate the fatigue fractured sites. These surface modification techniques have been widely adopted, primarily because of the robust grade of their mechanical properties. These are mainly the result of the formation of a large-scale, deep, and useful compressive residual stress, the formation of nanocrystals by the severe plastic deformation (SPD) at the subsurface layer, and the increase in surface hardness.

Molecular characterization of bacterial endosymbionts of Acanthamoeba isolates from infected corneas of Korean patients

  • Xuan, Ying-Hua;Yu, Hak-Sun;Jeong, Hae-Jin;Seol, Sung-Yong;Chung, Dong-Il;Kong, Hyun-Hee
    • Parasites, Hosts and Diseases
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    • v.45 no.1 s.141
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    • pp.1-9
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    • 2007
  • The endosymbionts of 4 strains of Acanthamoeba(KA/E9, KA/E21, KA/E22, and KA/E23) isolated from the infected corneas of Korean patients were characterized via orcein stain, transmission electron microscopic examination, and 16S rDNA sequence analysis. Double membrane-bound, rod-shaped endosymbionts were distributed randomly throughout both the trophozoites and cysts of each of Acanthamoeba isolates. The endosymbionts of KA/E9, KA/E22, and KA/E23 were surrounded by electron-translucent areas. No lacunae-like structures were observed in the endosymbionts of KA/E21, the bacterial cell walls of which were studded with host ribosomes. Comparative analyses of the 16S rDNA sequences showed that the endosymbionts of KA/E9, KA/E22 and KA/E23 were closely related to Caedibacter caryophilus, whereas the KA/E21 endosymbiont was assigned to the Cytophaga-Flavobacterium-Bacteroides(CFB) phylum. In the 4 strains of Acanthamoeba, the hosts of the endosymbionts were identified as belonging to the Acanthamoeba castellanii complex, which corresponds to the T4 genotype. Acanthamoeba KA/E21 evidenced characteristics almost identical to those of KA/E6, with the exception of the existence of endosymbionts. The discovery of these endosymbionts from Acanthamoeba may prove essential to future studies focusing on interactions between the endosymbionts and the amoebic hosts.

Evaluation of Fuel Consumption Models for Eco-friendly Traffic Operations Strategies (친환경 교통운영전략을 위한 차량 연료소모량 예측모형 평가)

  • PARK, Sangjun;LEE, Jung-Beom
    • Journal of Korean Society of Transportation
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    • v.34 no.3
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    • pp.234-247
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    • 2016
  • As the necessity of the evaluation of environmentally-friendly traffic operations strategies becomes obvious, the characteristics of fuel consumption models should be comprehended in advance. This study selected three fuel consumption models developed in Korea and another three models widely used in North America, and compared their applicabilities. Specifically, the national institute of environmental research (NIER) drive modes and the VISSIM software were utilized to model various driving patterns, and their fuel consumptions were estimated using the fuel consumption models. Based on the results, all the models showed the similar results in the analysis of the most fuel efficient cruising speed. On the other hand, caution should be taken when using the KR-1 and KR-2 models in microscopic analyses because they are not sensitive to instantaneous power requirements of vehicles.

Improvement of Pedestrian Convenience and Mobility by Applying the Walking Guidance System in Subway Stations (지하철 역사내 동선 분리 시스템을 활용한 보행편의 및 이동성 증진)

  • Lee, Joo-Yong;Kim, Taewan;You, So-Young
    • Journal of Korean Society of Transportation
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    • v.33 no.2
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    • pp.204-213
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    • 2015
  • The congestion of pedestrians impedes the utilization efficiency of a subway station. Conflicts among pedestrians due to unseparated pedestrian flows not only increase the impedance of pedestrian mobility but also negatively affect on pedestrian safety. This paper analyzes the travel characteristics of bi-directional pedestrian flow based on microscopic movements, and evaluates the operation efficiency on separating the traffic line. The subway station was simulated in a 2-D grid structure by applying Discrete Element Method, and the movement is organized in each cell of the grid. As a result, the model explicates that separating the traffic line and encouraging the 'Keep right rule' would be mostly effective for the conflicting flows. Therefore, applying the 'Walking Guidance System' would be efficient to improve the pedestrian convenience and mobility.

Characteristic Analysis of Paint used in Defense Industries Equipments of Korean Conflict in The War Memorial of Korea (전쟁기념관 소장 6·25전쟁 방산장비의 도료 특성 분석)

  • Kang, Hyun Sam;Kim, Soo Chul;Park, Min Soo
    • Journal of Conservation Science
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    • v.32 no.2
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    • pp.215-221
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    • 2016
  • This study conducted analysis of paint samples from defense industries equipments of Korean Conflict in The War Memorial of Korea to identify the characteristics of the modern paint. The samples were analyzed by microscopic observation, infrared spectroscopy and SEM-EDS. Cross-section of paint samples are made up of several layers of about 9 to 20 times, and thickness of the layer is not uniform in the $10{\sim}100{\mu}m$. The putty was used for the surface treatment before painting. Inorganic analysis showed that one type of the putty consist of minium and kaolin, talc, titanium dioxide. According to the results of infrared spectroscopy, paint samples were identified as alkyd resin. Some bands such as C-H bending, C-O and C-C stretching, C-H rocking were found in spectra.

An Electron Microscopic Study on Cartilage Canal in Thoracic Vertebra of Human Fetuses. (인태아(人胎兒) 척추(脊椎) 연골관(軟骨管)에 관(關)한 전자현미경적(電子顯微鏡的) 연구(硏究))

  • Yoon, Jae-Rhyong;Lee, Byung-Ho;Oh, Chang-Seok
    • Applied Microscopy
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    • v.23 no.1
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    • pp.91-108
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    • 1993
  • The relationship of cartilage canals to initial osteogenesis of primary ossification center of developing vertebrae in human fetuses ranging from 50mm to 260mm in crown rump length was studied by light and electron microscopy. The cartiage canals of the thoracic vertebrae were first observed at 60mm fetus. Cartilage canals were identified as vascular channels arising from perichondrium surfaces. A number of cartilage canals were observed around the primary center of ossification at 80mm fetus. At 120mm fetus, cartilage canals of the bodies of vertebra were increased. Eventually the canals were eroded from the main medullary cavity and remained at only peripheral regions of growth cartilage. Superficial, intermediate, and deep canals were identified by the characteristics of cartilage cells. Fibroblasts, undifferentiated mesenchymal cells, and vacuolated macrophages were observed adjacent to the matrix of resting cartilage cells in the superficial canal. Fibroblasts and mesenchymal cells were densely packed at the tip of canal, giving an epithelial appearance to the clustered cell in the intermediate canal. Vacuolated macrophages were in contact with matrix of hypertrophied cartilage. The thick-walled vessels in the intermediate and deep canals consisted of typical endothelial cells, but in the newly formed vessels contained mesenchymal cells and fibroblasts incorporated into the vessel wall. During lengthening of cartilage canal, the matrix of cartilage cells were invaded by newly formed capillaries and vacuolated macrophages. At the deep canal, the lateral wall of the canal terminated in matrix containing calcified cartilage. The mesenchymal cells began to differentiate into osteoblasts adjacent to the calcified matrix. The results indicate that the connective tissue cells within the cartilage canals proliferate and differentiate into osteoblasts at the site of primary ossification center.

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Risk Factors for Developing Large Emboli Following Carotid Artery Stenting

  • Kwon, Sae Min;Cheong, Jin Hwan;Lee, Sang Kook;Park, Dong Woo;Kim, Jae Min;Kim, Choong Hyun
    • Journal of Korean Neurosurgical Society
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    • v.53 no.3
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    • pp.155-160
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    • 2013
  • Objective : The introduction and development of the embolic protecting device (EPD) has resulted in a decreased rate of stroke after carotid artery stenting (CAS). The authors performed a retrospective study to investigate the risk factors for developing large emboli after CAS which can lead to ischemic events. Methods : A total of 35 consecutive patients who underwent CAS between January 2009 and March 2012 were included in this study. Patients were divided into two groups including those with small emboli (group A; grade 1, 2) and those with large emboli (group B; grade 3, 4). The size and number of emboli were assigned one of four grades (1=no clots, 2=1 or 2 small clots, 3=more than 3 small clots, 4=large clots) by microscopic observation of the EPD after CAS. We compared demographic characteristics, medical history, and angiographic findings of each group. Results : Thirty-five patients underwent CAS, and technical success was achieved in all cases. Twenty-three patients were included in group A and 12 patients in group B. Our results demonstrated that advanced age [odds ratio (OR) 1.24; 95% confidence interval (CI) 1.01-1.52; p=0.044] and smoking (OR 42.06; CI 2.828-625.65, p=0.006) were independent risk factors for developing large emboli after CAS. Conclusion : In patients with carotid artery stenosis treated with CAS, advanced age and smoking increased the number and size of emboli. Although use of an EPD is controversial, it may be useful in CAS in patients with risk factors for large emboli in order to reduce the risk of ischemic events.

Surface Composition and Molecular Diffusion on the Stability of Foams Formed from Protein/Surfactant Mixtures (단백질/계면활성제 혼합계에서 기포안정성에 대한 계면조성과 분자확산)

  • Park, Sun-Yeong;Kim, Myung-Soo;Jeong, Noh-Hee;Nam, Ki-Dae
    • Journal of the Korean Applied Science and Technology
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    • v.17 no.3
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    • pp.158-166
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    • 2000
  • A conductimetric study of foam formed from mixture of the protein, ${\beta}-lactoglobulin$, and the nonioinc surfactant, SML, revealed that their stability was reduced at concentrations of SML in the range $3{\sim}10mM$. The interaction of SML with ${\beta}-lactoglobulin$ was investigated by fluorimetry and a dissociation constant of $0.2{\mu}M$ was calculated for the complex. Surface tension studies confirmed the presence of interaction between the two components and provided evidence for the progressive displacement of ${\beta}-lactogloblin$ from the air/water interface with increasing SML concentration. Experiments using air-suspended microscopic thin liquid films revealed transitions in the chainage characteristics and thickness of the film at SML concentrations below that which resulted in destabilization of the foam. However, measurements of surface mobility of fluorescent-labeled ${\beta}-lactoglobulin$ by a photobleaching method identified that a transition to a mobile system occurred at a SML concentration which correlated with the onset of instability in the disperse phase. The results would indicate that maintenance of the viscoelastic properties of the surface is paramount importance in determining the stability of interfaces comprising mixtures of protein and surfactant.