• Title/Summary/Keyword: microscopic characteristics

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Pharmacognostical Evaluation of Trachyspermum roxburghianum (DC) Craib Fruits

  • Verma, Nitin;Khosa, R.L.
    • Natural Product Sciences
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    • v.17 no.1
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    • pp.45-50
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    • 2011
  • Sophisticated modern research tools for evaluation of medicinal plants are available but microscopic methods are one of the simplest and cheapest methods to establish the identity of the source materials. Pharmacognostical investigation of the dried, powdered and anatomical sections of the fruits of Trachyspermum roxburghianum (DC) Craib was carried out to determine its macro and microscopical characteristics along with its physical constants. Externally, the fruits, yellowish or greenish brown in colour are elongated, elliptical, slightly curved, prominently ridged and longitudinal. As seen in transectional views of the fruits from Trachyspermum roxburghianum, the mericarp has concave sides called commissural surfaces and a convex outer side called the dorsal surface. The mericarp has three primary ridges alternating with two secondary ridges on the dorsal side. On the commissural side, there are two primary ridges which are lateral in position and two secondary ridges in the commissural side. The seed is attached to the pericarp by a short stalk called a raphe. Circular, four-lobed calcium oxalate crystals are fairly abundant in the endosperm. Phytochemical studies revealed the presence of phenolic compounds, triterpenoids, proteins and sugars. The pharmacognostical profile of the fruits will assist in standardization for quality, purity and sample identification.

Lithium Transition Metal Phosphate Cathodes for Advanced Lithium Batteries (리튬이온전지에서 새로운 양극재료를 위한 금속인산화물)

  • ;Yet Ming Chiang
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2003.11a
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    • pp.26-26
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    • 2003
  • Lithium storage electrodes for rechargeable batteries require mixed electronic-ionic conduction at the particle scale in order to deliver desired energy density and power density characteristics at the device level. Recently, lithium transition metal phosphates of olivine and Nasicon structure type have become of great interest as storage cathodes for rechargeable lithium batteries due to their high energy density, low raw materials cost, environmental friendliness, and safety. However, the transport properties of this family of compounds, and especially the electronic conductivity, have not generally been adequate for practical applications. Recent work in the model olivine LiFePO$_4$, showed that control of cation stoichiometry and aliovalent doping results in electronic conductivity exceeding 10$^{-2}$ S/cm, in contrast to ~10$^{-9}$ S/cm for high purity undoped LiFePO$_4$. The increase in conductivity combined with particle size refinement upon doping allows current rates of >6 A/g to be utilized while retaining a majority of the ion storage capacity. These properties are of much practical interest for high power applications such as hybrid electric vehicles. The defect mechanism controlling electronic conductivity, and understanding of the microscopic mechanism of lithiation and delithiation obtained from combined electrochemical and microanalytical techniques, will be discussed

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A visual inspection algorithm for detecting infinitesimal surface defects by using dominant frequency map (지배주파수도를 이용한 미소 표면 결함 추출을 위한 영상 처리 알고리듬)

  • Kim, Kim, Sang-Won;Kweon, Kweon, In-So
    • Journal of Institute of Control, Robotics and Systems
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    • v.2 no.1
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    • pp.26-34
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    • 1996
  • One of the challenging tasks in visual inspection using CCD camera is to identify surface defects in an image with complex textured backgeound. In microscopic view, the surface of real objects shows regular or random textured patterns. In this paper, we present a visual inspection algorithm to extract abnormal surface defects in an image with textured background. The algorithm uses the space and frequency information at the same time by introducing the Dominant Frequency Map(DFM) which can describe the frequency characteristics of every small local region of an input image. We demonstrate the feasibility and effectiveness of the method through a series of real experiments for a 14" TV CRT mold. The method successfully identifies a variety of infinitesimal defects, whose size is larger than $50\mu\textrm{m}$, of the mold. The experimental results show that the DFM based method is less sensitive to the environmental changes, such as illumination and defocusing, than conventional vision techniques.ques.

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A Study on Microscopic Damage Behavior of Carbon Fiber Sheet Reinforced Concrete using Acoustic Emission Technique (음향방출 기법을 이용한 탄소섬유시트강화 콘크리트의 미시적 손상 거동에 관한 연구)

  • 이진경;이준현;정성륜
    • Composites Research
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    • v.12 no.4
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    • pp.62-70
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    • 1999
  • It was well recognized that damages associated mainly with the aging of civil infrastructrues were one of very serious problems for assurance of safety and reliability. In recent, carbon fiber sheet(CFS) has been widely used for reinforcement and rehabitation of damaged concrete beam. However, the fundamental mechanism of load transfer and its load-resistant for carbon fiber sheet reinforced concrete are not fully understood. In this study, three point bend test has been carried out to understand the damage progress and micro-failure mechanism of CFS reinforced concretes. For these purposes, four kinds of specimens are used, that is, concrete, respectively. Acoustic Emission(AE) technique was used to evaluate the characteristics of damage progress and failure mechanism of specimens. In addititon, two-dimensional AE source location was also performed to monitor crack initiation and propagation processes for four types of these specimens.

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A Study on Shear Fracture Behavior of Metal in Micro Hole Punching Process (금속 소재의 미세 홀 펀칭 시 전단 파괴 거동 연구)

  • 유준환;임성한;주병윤;오수익
    • Transactions of Materials Processing
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    • v.12 no.4
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    • pp.314-319
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    • 2003
  • In the micro hole punching, the size and shape of burr and burnish zone are very important factors to evaluate quality of micro holes which depend on punch-die clearance, strain rate, workpiece material and etc. To get micro holes with small burr and wide burnish zone for industrial demands, not only the parametric study but also a study on fracture behavior in shear band are necessary. In this study, 100 $\mu$m, 25 $\mu$m micro holes in diameter were fabricated on brass (Cu63/Zn37) and SUS 316 foils as aspect ratio 1:1, and the characteristics of micro holes was investigated comparing with those of macro holes over several mm by scanning electron microscopic views and section views. Like macro hole, micro hole is also composed of 4 portions, rollover. burnish zone, fracture zone and burr, and it shows similar fracture behavior in shear band. But by high strain rate (10$^2$∼10$^3$s$^{-1}$ ) condition unlike that of macro hole fabrication and by the increment of relative grain size in the direction of the workpiece thickness, fracture zone is not observed.

Review of Metal Oxide-based Formaldehyde Gas Sensor to Measure Indoor Air Quality (실내 대기질 진단을 위한 금속산화물 기반 폼알데하이드 가스센서 연구 동향)

  • Kim, Yoon Hwa;Koo, Won-Tae;Jang, Ji-Soo;Kim, Il-Doo
    • Journal of Sensor Science and Technology
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    • v.28 no.6
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    • pp.377-384
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    • 2019
  • People currently spend more than 80% of their time indoors; therefore, the management of indoor air quality has become an important issue. The contamination of indoor air can cause sick house syndrome and various environmental diseases such as atopy and nephropathy. Formaldehyde gas, which is the main contaminant of indoor air, is lethal even with microscopic exposure; however, it is commonly used as an adhesive and waterproofing agent for indoor building materials. Therefore, there is a need for a gas sensor capable of detecting trace amounts of formaldehyde gas. In this review, we summarize recent studies on metal oxide-based semiconductor gas sensors for formaldehyde gas detection, methods to improve the gas-sensing properties of metal oxides of various dimensions, and the effects of catalysts for the detection of parts-per-billion level gases. Through this, we discuss the necessary characteristics of the metal oxidebased semiconductors for gas sensors for the development of next-generation sensors.

Experimental Study on Congenital Malformations of the Heart and Great Vessels in Rat Fetuses Induced by Nitrofen (임신랫트 태자에서 Nitrofen에 의해 유발된 선천성 심혈관 기형에 관한 실험연구)

  • 김원곤
    • Journal of Chest Surgery
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    • v.20 no.4
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    • pp.659-672
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    • 1987
  • Nitrofen [2,4-dichlorophenyl-P-nitrophenyl ether] is a diphenyl ether herbicide used for pre and post-emergent control of broad leafed weeds. This chemical was known to induce a variety of congenital cardiovascular anomalies with diaphragmatic hernia and hydronephrosis in the rate fetuses. The present study was conducted to produce congenital cardiovascular anomalies in the rat fetuses by oral nitrofen administration at the indicated doses and days of gestation, and to find the characteristics of nitrofen-induced cardiovascular anomalies. All the observed fetuses were removed from the pregnant Sprague-Dawley rats sacrificed on the twenty-first day of gestation. They were preserved in 10 per cent formalin and dissection for examination were carried out under a dissecting microscope using forceps and scissors. Following results and conclusion were based on dissecting microscopic findings on 482 offsprings. 1. The eleventh day of gestation was the most sensitive day for nitrofen induction of congenital cardiovascular anomalies in the rat. This incidence was dose-related in rats exposed on the eleventh day of gestation. 2. Ventricular septal defect was the most common single anomaly that represented more than half of the total cardiovascular anomalies, followed by aortic arch anomalies and tetralogy of Fallot. 3. Cardiac anomalies derived from infundibular maldevelopment such as tetralogy of Fallot and pulmonary atresia with ventricular septal defect were only observed in the eleventh gestation day treated group. 4. Aortic arch anomalies were found in high frequency and the great majority were characteristically anomalous right subclavian artery with left aortic arch. Key words; nitrofen, congenital cardiovascular anomalies.

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Production of 3-Hydroxypropionic Acid from Acrylic Acid by Newly Isolated Rhodococcus erythropolis LG12

  • Lee, Sang-Hyun;Park, Si-Jae;Park, Oh-Jin;Cho, Jun-Hyeong;Rhee, Joo-Won
    • Journal of Microbiology and Biotechnology
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    • v.19 no.5
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    • pp.474-481
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    • 2009
  • A novel microorganism, designated as LG12, was isolated from soil based on its ability to use acrylic acid as the sole carbon source. An electron microscopic analysis of its morphological characteristics and phylogenetic classification by 16S rRNA homology showed that the LG12 strain belongs to Rhodococcus erythropolis. R. erythropolis LG12 was able to metabolize a high concentration of acrylic acid (up to 40 g/l). In addition, R. erythropolis LG12 exhibited the highest acrylic acid-degrading activity among the tested microorganisms, including R. rhodochrous, R. equi, R. rubber, Candida rugosa, and Bacillus cereus. The effect of the culture conditions of R. erythropo/is LG12 on the production of 3-hydroxypropionic acid (3HP) from acrylic acid was also examined. To enhance the production of 3HP, acrylic acid-assimilating activity was induced by adding 1 mM acrylic acid to the culture medium when the cell density reached an $OD_{600}$ of 5. Further cultivation of R. erythropo/is LG 12 with 40 g/l of acrylic acid resulted in the production of 17.5 g/l of 3HP with a molar conversion yield of 44% and productivity of 0.22 g/l/h at $30^{\circ}C$ after 72 h.

CHARACTERISTICS OF WALL IMPINGEMENT AT ELEVATED TEMPERATURE CONDITIONS ON GDI SPRAY

  • Park, J.;Im, K.S.;Kim, H.;Lai, M.C.
    • International Journal of Automotive Technology
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    • v.5 no.3
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    • pp.155-164
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    • 2004
  • The direct injection gasoline spray-wall interaction was characterized inside a heated pressurized chamber using various visualization techniques, including high-speed laser-sheet macroscopic and microscopic movies up to 25,000 frames per second, shadowgraph, and double-spark particle image velocimetry. Two hollow cone high-pressure swirl injectors having different cone angles were used to inject gasoline onto a heated plate at two different impingement angles. Based on the visualization results, the overall transient spray impingement structure, fuel film formation, and preliminary droplet size and velocity were analyzed. The results show that upward spray vortex inside the spray is more obvious at elevated temperature condition, particularly for the wide-cone-angle injector, due to the vaporization of small droplets and decreased air density. Film build-up on the surface is clearly observed at both ambient and elevated temperature, especially for narrow cone spray. Vapor phase appears at both ambient and elevated temperature conditions, particularly in the toroidal vortex and impingement plume. More rapid impingement and faster horizontal spread after impingement are observed for elevated temperature conditions. Droplet rebounding and film break-up are clearly observed. Post-impingement droplets are significantly smaller than pre-impingement droplets with a more horizontal velocity component regardless of the wall temperature and impingement angle condition.

Water-flow Test/Performance Evaluation of Nonimpinging-type Injector used in the Hydrazine Thruster of Medium-level Thrust (중형급 하이드라진 추력기에 장착되는 비충돌형 인젝터의 수류시험 및 성능평가)

  • Jung, Hun;Kim, Jong-Hyun;Kim, Jeong-Soo;Kim, In-Tae
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2011.11a
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    • pp.139-142
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    • 2011
  • A water-flow test for acceptance verification is carried out for a nonimpinging-type injector prior to the design-performance verification of hydrazine thruster under development. The injector used in the experiment is to be equipped on the hydrazine thruster producing 70 N of nominal thrust at an inlet pressure of 24.6 $kg_f/cm^2$. It is observed that there exist varying characteristics of atomization among the injector-nozzle orifices caused by a fabrication error which can be judged from a microscopic standpoint. On the other hand, all of the injector orifices are placed within the design criteria in an injection-angle performance.

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