• The Korean Journal of Ceramics
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• 제5권1호
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• pp.78-81
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• 1999

Aluminium titanate is highly anisotropic in thermal expansion. As a result, thermal stresses build up in the material and intergranular cracks can develop. Both the outstanding thermal shock resistance and the low mechanical strength of aluminium titanate ceramics are a result of intergranular microcracking. The authors have previously identified a possibility of remarkably increasing fracture toughness of aluminium titanate without excessive penalty on strength. The paper shows that sintered density and porosity measurements can be used for optimizing the sintering and microstructure of aluminium titanate for an ideal balance between toughness and strength and, hence, the best thermal shock resistance.

• Advances in concrete construction
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• 제11권3호
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• pp.261-270
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• 2021

In this study, a new understanding is presented on the microcracking behavior of high strength concrete (HSC) with steel fiber addition having prior compressive loading history. Microcracking behavior at critical stress (σcr) region, using seven fiber addition volume of 0.5, 0.75, 1.0, 1.25, 1.5, 1.75, and 2.0% was evaluated, at two aspect ratios (60 and 75). The specimens were loaded up to a specified compressive stress levels (0.70fc-0.96fc), and subsequently subjected to split tensile tests. This was followed by microscopic analyses afterwards. Four compressive stress levels as percentage of fc were selected according to the linearity end point based on stress-time (σ-t) diagram under uniaxial compression. It was seen that pre-compression has an effect on the linearity end point as well as fiber addition where it lies within 85-91% of fc. Tensile strength gain was observed in some cases with respect to the 'maiden' tensile strength as oppose to tensile strength loss due to the fiber addition with teething effect. Aggregate cracking was the dominant failure mode instead of bond cracks due to improved matrix quality. The presence of the steel fiber improved the extensive failure pattern of cracks where it changes from 'macrocracks' to a branched network of microcracks especially at higher fiber dosages. The applied pre-compression resulted in hardening effect, but the cracking process is similar to that in concrete without fiber addition.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 1997년도 가을 학술발표회 논문집
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• pp.3-23
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• 1997

The growth in fast-track construction and repair has prompted major efforts to develop high-early-strength concrete mix compositions. Such mixtures rely on the use of relatively high cement contents and accelerator dosages to increase the rate of strength development. The measures, however, seem to compromise the long-term performance of concrete in applications such as full-depth patches as evidenced by occasional premature deterioration of such patches. The hypothesis successfully validated in this research was that traditional methods of increasing the early-age strength of concrete, involving the use of high cement and accelerator contents, increase the moisture and thermal movements of concrete. Restraint of such movements in actual field conditions, by external or internal restraining factors, generates tensile stresses which introduced microcracks and thus increase the permeability of concrete. This increase in permeability accelerates various processes of concrete deterioration, including freeze-thaw attack. Fiver reinforcement of concrete is an effective approach to the control of microcrack and crack development under tensile stresses. Fibers, however, have not been known of accelerating the process of strength gain in concrete. The recently developed specialty cellulose fibers, however, were found in this research to be highly effective in increasing the early-age strength of concrete. This provides a unique opportunity to increase the rate of strength gain in concrete without increasing moisture an thermal movements, which actually controlling the processes of microcracking and racking in concrete. Laboratory test results confirmed the desirable resistance of specialty cellulose fiber reinforced High-early-strength concrete to restrained shrinkage microcracking an cracking, and to different processes of deterioration under weathering effects.

• The Korean Journal of Ceramics
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• 제3권3호
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• pp.195-198
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• 1997

Post-firing process of electronic ceramic, such as electroding and encapsultion with resin, often causes damage by thermal shock. The thermal shock behavior of $BaTiO_3$ ceramics was investigated by the down-quench test, where the relative strength retained is determined after the sample is quenched from an elevated temperature into a fixed temperature bath. The critical temperature drop, $\DeltaTc$, was evaluated for three kinds of sintered $BaTiO_3$ ceramics, which were formed by extrustioin, uniaxial pressing using granules, and uniaxial pressing using powders. A drastic loss in strength caused by microcracking was observed for the specimens quenched with $\DeltaT\geq150^{\circ}C$. This concentp can be adopted as a method of the quality control by monitoring the sudden drop of the strength of capacitor products after each exposure to heat.

• The Korean Journal of Ceramics
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• 제2권4호
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• pp.246-250
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• 1996

The thermomechanical properties of materials from the system Al2O3-SiO2-TiO2(Tialite-Mullite) were investigated by correlating the thermal expansion anisotroypy, flexural strength and Young's modulus with grain size and atructural microcracking during cooling. Microcracking temperatures were determined by measuring the hysteresis of the thermal expansion anisotropy with dilatometry. Single phase Aluminium Titanate is a low strength material, while composites with more than 10 vol% mullite as second phase enhance the Young's modulus, thermal expansion coefficient and room temperature strength.

• 한국초전도저온공학회:학술대회논문집
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• 한국초전도저온공학회 2003년도 학술대회 논문집
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• pp.146-148
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• 2003

SrZrO$_3$ resistive oxide barriers on Ag sheathed Bi2223 monocore tapes were prepared by the sol-gel and dip coating method to reduce AC coupling loss. The performance of the dip-coated SrZrO$_3$ thin films was evaluated in terms of bond strength and surface microstructure by varying the amount of PVP (polyvinylpyrrolidone) binder. Although bond strength and coating thickness increased as the PVP content rose, surface microcracking was more severe for the specimen containing higher content of PVP binder. It suggests that coating thickness and microcracking of the SrZrO$_3$ films on Bi2223 tapes was governed primarily by the amount of PVP binder.

• 한국세라믹학회지
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• 제35권6호
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• pp.551-558
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• 1998

Detection of microcrack in {{{{ {Al }_{2 } {O }_{3 } }} ceramics were studided by AE(acoustic emission) technique with 4-point bending test in order to evaluate the fracture process and formation of microcrack. Fully-dense alu-mina ceramics having a different grain size were fabricated by varing the hot-pressing temperature. The grain size of alumina increased with increasing the hot-pressing temperature whereas the bending strength decreasd. The microcracks were observed by SEM and TEM. The generation of AE event increased with increasing the applied load and many AE event was generated at maximum applied load. Alumina with smaller grain size shows the generation of many AE event resulting in an increase of microcrack formation. An intergranular fracture is predominantly observed in fine-grained alumina whereas intragranular fracture occurs predominantly in coarse-grained alumina,. Analysis of micorstructure and AE prove that primary mi-crocracks occur within grain-boundaries of alumina. The larger microcracking were formed by the growth and/or coalesence of primary microcracks. Then the materials become to fracuture by main crack gen-eration at the maximum applied load.

• 한국농공학회지
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• 제43권5호
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• pp.124-131
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• 2001

The shrinkage properties of high early strength concrete were investigated. One of the method to control microcrack and crack development due to restrained shrinkage is to reinforce concrete with randomly distributed fibers. Regulated-set cement and two different types of fiber were adopted. The experiments for heat of hydration, drying and autogenous shrinkage were conducted. The desirable resistance of high early strength fiber reinforced concrete to restrained shrinkage microcracking was achieved. These results indicate that use of fiber in high early strength concrete plays an important role in control of crack development due to restrained shrinkage.

• 한국분말재료학회지
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• 제2권3호
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• pp.216-222
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• 1995

$SiC/TiB_2$ composites of varying $TiB_2$ content from 0 to 52 vol.% were prepared by pressureless sintering. When these composites were sintered at $2150^{\circ}C$ the mechanical properties such as elastic modulus, strength and toughness increased with increasing $TiB_2$ content. On the other hand, at a sintering temperature of $2200^{\circ}C$, the mechanical properties reduced gradually with increasing $TiB_2$ content. The main reason was deduced from the onset of spontaneous microcracking and the critical particle size for microcracking was calculated approximately 5.6 $\mu\textrm{m}$.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2004년도 추계 학술발표회 제16권2호
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• pp.445-448
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• 2004

Recently, bridge deck overlay with latex modified concrete is widely applied in domestic. the capacity of bridge deck overlay depends on bond state on the surface. factors that have an effect on bond state are clean condition on the surface, absence of surface microcracking, absence of laitance, overlay curing. In this study, it is researched that characteristic of bond strength according to moisture condition on the surface and the removal method of concrete. As a result, it shows high bond strength in dry condition when w/c is $31\%$ and in moisture condition when w/c is $38\%$ respectively. characteristic of bond strength according to the removal method of concrete shows high bond strength when using water-jets rather than jackhammers.