• Journal of Korea Foundry Society
• /
• v.40 no.2
• /
• pp.16-24
• /
• 2020

The effect of a heat treatment on the microstructure and mechanical properties of Inconel 713C alloy vacuum investment castings were investigated. The microstructure of the as-cast state was observed, showing well-developed dendrite structures and distributed carbide particles and solidified massive precipitates in the grain or grain boundary during solidification, in this case the γ′ phase and MC particles. During a heat treatment, the γ phase matrix was reinforced by solid solution elements, carbide particles from the film morphology precipitated along the grain boundary, and many micro-precipitates of second γ′ phases 0.2 ㎛~2 ㎛ in size were newly formed in the γ phase matrix according to SEM-EDS analysis results. The tensile strength at a high temperature (850℃) decreased slightly becoming comparable with the room-temperature result, while the hardness value of the specimen after the vacuum heat treatment increased by approximately 19%, becoming similar to that of the as-cast condition. However, the impact values at room temperature and low temperature (-196℃) were approximated; this alloy was mostly not affected by an impact at a low temperature. In the observations of the fracture surface morphologies of the specimens after the tensile tests, the fractures at room temperature were a mix of brittle and ductile fractures, and an intergranular fracture in the inter-dendrite structure and some dimples in the matrix were observed, whereas the fractures at high temperatures were ductile fractures, with many dimples arising due to precipitation. It was found that a reinforced matrix and precipitates of carbide and the γ′ phase due to the heat treatment had significant effects, contributing greatly to the excellent mechanical properties.

• Journal of Welding and Joining
• /
• v.17 no.1
• /
• pp.124-132
• /
• 1999

Thermal fatigue strength of the solder joints is the most critical issue for TSOP(Thin Small Outline Package) because the leads of this package are extremely short and thermal deformation cannot be absorbed by the deflection of the lead. And the TSOP body can be subject to early fatigue failures in thermal cycle environments. This paper was discussed distribution of thermal stresses at near the joint between silicon chip and die pad and investigated their reliability of solder joints of TSOP with 42 alloy clad lead frame on printed circuit board through FEM and 3 different thermal cycling tests. It has been found that the stress concentration around the encapsulated edge structure for internal crack between the silicon chip and Cu alloy die pad. And using 42 alloy clad, The reliability of TSOP body was improved. In case of using 42 alloy clad die pad(t=0.03mm). $$\sigma$_{VMmax}$ is 69Mpa. It is showed that 15% improvement of the strength in the TSOP body in comparison with using Cu alloy die pad $($\sigma$_{VMmax}$=81MPa). In solder joint of TSOP, the maximum equivalent plastic strain and Von Mises stress concentrate on the heel of solder fillet and crack was initiated in it's region and propagated through the interface between lead and solder. Finally, the modified Manson-Coffin equation and relationship of the ratio of $N_{f}$ to nest(η) and cumulative fracture probability(f) with respect to the deviations of the 50% fracture probability life $(N_{f 50%})$ were achieved.

• Journal of Welding and Joining
• /
• v.28 no.1
• /
• pp.34-40
• /
• 2010

In Friction Stir Lap Welding(FSLW), the movement of material within the weld was more important than the microstructure, due to the interface present between the sheets. Thus, The soundness of free defect, Effective Sheet Thickness(EST) and width of joint were most important factor of mechanical properties. Specimens by lap joint types that were 'A-type' and 'R-type' were made in this study. A-type tensile specimen was loaded at advancing side and R-type tensile specimen was loaded at retreating side. Macro-, micro-structural observation and mechanical properties of FSLW A5052-H112 alloy ware investigated under varying rotating and welding speed. The results were as follows: Material hook formed decreasing after sharply increasing was appeared at the end interface of joint area in advanced side, and material hook formed decreasing after smoothly increasing was observed at that in retreated side. Tensile load had no relation with defects. As rotating speed was higher, tensile strength was increasing and EST was decreasing regardless of joint types. joint efficiency was over 70%. In a result of fractography, fracture in A-type was partially occurred by dimple in SZ, and fracture in R-type was generally occurred by dimple in HAZ.

• Journal of Welding and Joining
• /
• v.31 no.6
• /
• pp.50-57
• /
• 2013

Characterization of microstructures and cryogenic mechanical properties of electro beam (EB) welds between cast and forged Inconel 718 superalloys has been investigated. Optimal EBW condition was found in the beam current range of 36~39 mA with the constant travel speed of 12 mm/s and arc voltage of 120 kV for 10 mm-thick specimens. Electron beam current lower than 25 mA caused to occur the liquation microfissuring in cast-side heat affected zone (HAZ) of EB welds. The HAZ liquation microfissure was found on the liquated grain boundaries with resolidified ${\gamma}/Laves$ and ${\gamma}/NbC$ eutectic constituents. EBW produced welds showing a fine dendritic structure with relatively discrete Laves phase due to fast cooling rate. After post weld aging treatment, blocky Laves phase and formation of ${\gamma}^{\prime}+{\gamma}^{{\prime}{\prime}}$ strengtheners were observed. Presence of primary strengthener and coarse Laves particles in PWHT weld may cause to reduce micro-plastic zone ahead of a crack, leading to a significant decrease in Charpy impact toughness at $-196^{\circ}C$. Fracture initiation and propagation induced by Charpy impact testing were discussed in terms of the dislocation structures ahead of crack arisen from the fractured Laves phase.

• Anatomy and Cell Biology
• /
• v.57 no.2
• /
• pp.294-304
• /
• 2024

Type 2 diabetes mellitus is increasingly becoming more prevalent worldwide together with hospital care costs from secondary complications such as bone fractures. Femoral fracture risk is higher in diabetes. Therefore, this study aimed to assess the osteometric and microarchitecture of the femur of Zucker Diabetic Sprague-Dawley (ZDSD) femur. Ten-week-old male rats (n=38) consisting of 16 control Sprague-Dawley (SD) and 22 ZDSD rats were used. The rats were terminated at 20 weeks and others at 28 weeks of age to assess age, diabetes duration effects and its severity. Bilateral femora were taken for osteometry, bone mass measurements and micro-focus X-ray computed tomography scanning to assess the trabecular number (TbN), thickness (TbTh), spaces (TbSp), bone tissue volume to total volume (BV/TV) and volume (BV). Diabetic rats had shorter (except for 20-weeks-old), lighter, narrower, and less robust bones than SD controls that wered more robust. Although cortical area was similar in all diabatic and control rats, medullary canal area was the largest in ZDSD rats. This means that the diabetic rats bones were short, light and hollow. Diabetic rats aged 20 weeks had reduced BV, BV/TV, TbN with more spacing (TbSp). In contrast, the 28 weeks old diabetic rats only showed reduced BV and TbN. Discriminant function analysis revealed, for the first time, that osteometric parameters and TbTh, TbN, and TbSp were affected by diabetes. This knowledge is valuable in the management of diabetic complications.

• Journal of Mechanical Science and Technology
• /
• v.16 no.7
• /
• pp.919-926
• /
• 2002

In this study, the numerical prediction of the thermal fatigue lie? of a $\mu$BGA (Micro Ball Grid Array) solder joint was focused. Numerical method was performed using the three-dimensional finite element analysis for various solder alloys such as Sn-37%Pb, Sn-3.5%Ag, Sn-3.5%Ag-0.7%Cu and Sn-3.5%Ag-3%In-0.5%Bi during a given thermal cycling. Strain values obtained by the result of mechanical fatigue tests for solder alloys, were used to predict the solder joint fatigue life using the Coffin-Manson equation. The numerical results showed that Sn-3.5%Ag with the 50-degree ball shape geometry had the longest thermal fatigue life in low cycle fatigue. A practical correlation for the prediction of the thermal fatigue life was also suggested by using the dimensionless variable γ. Additionally Sn-3.5Ag-0.75Cu and Sn-2.0Ag-0.5Cu-2.0Bi were applied to 6$\times$8$\mu$BGA obtained from the 63Sn-37Pb Solder. This 6$\times$8$\mu$BGA were tested at different aging conditions at 130$\^{C}$, 150$\^{C}$, 170$\^{C}$ for 300, 600 and 900 hours. Thickness of the intermetallic compound layer was measured thor each condition and the activation energy thor their growth was computed. The fracture surfaces were analyzed using SEM (Scanning Electron Microscope) with EDS ( Energy Dispersive Spectroscopy).

• Journal of Biomedical Engineering Research
• /
• v.30 no.5
• /
• pp.444-451
• /
• 2009

Purpose: The aim of present study is to detect longitudinal alterations of mechanical characteristic determined by bone quality (microarchitecture and degree of mineralization) on femur trabecular bone due to metastatic bone tumor Materials and Methods: Each 6 female SD rats (12 weeks old, approximate 250g) were allocated in SHAM and TUMOR Group. W256 (Walker carcinosarcoma 256 malignant breast cancer cell) was injected into the right femur (intraosseous injection) in TUMOR Group, whereas 0.9% NaCl (saline solution) was injected in SHAM Group. The right hind limbs of all rats were scanned by in-vivo micro-CT to acquire structural parameters, bone mineral density, X-ray attenuation and bone mineralization distribution at 0 week and 4 weeks after surgery. Results: BMD, BV/TV and Tb.N of trabecular bone in TUMOR group were markedly decreased (26%, 11% and 23%) while those in SHAM group were significantly increased (34%, 48% and 11%) (p<0.05). BS/BV, Tb.Sp and SMI in TUMOR group were significantly increased (-16%, 38% and 2%) compared with those in SHAM group (-33%, 12% and -16%) (p<0.05). Additionally, bone mineralization in TUMOR group significantly decreased while those in SHAM group was significantly increased (p<0.05). Conclusion: It is identified that how much bone microarchitecture and mineralization are diminished due to the metastatic bone tumor. The results may be helpful to prediction of fracture risk by metastatic bone tumor.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.39 no.4
• /
• pp.447-451
• /
• 2015

The objective of this study is to predict the structural characteristics of a heat exchanger mounted on an aircraft engine using finite element analysis. The plastic fracture and life of the heat exchanger were estimated by a thermo-mechanical analysis. Tensile tests were conducted under high temperature conditions (700, 800, 900, 1000 K) using five specimens to obtain the mechanical properties of the Inconel 625 tubes. To assess the structural characteristics of the heat exchanger, the full and partial models were applied under the operating conditions given by the thermo-mechanical and inertial load. As a result, the case, tubesheet, flange, and mounting components have a reasonable safety margin to the allowable stress assuming a fatigue strength of Inconel 625 of 10000 cycles under 1000 K.

• Smart Structures and Systems
• /
• v.3 no.1
• /
• pp.51-68
• /
• 2007

High-strength concrete (HSC) is becoming increasingly attractive for various construction projects since it offers a multitude of benefits over normal-strength concrete (NSC). Unfortunately, current design provisions for shear capacity of RC slender beams are generally based on data developed for NSC members having a compressive strength of up to 50 MPa, with limited recommendations on the use of HSC. The failure of HSC beams is noticeably different than that of NSC beams since the transition zone between the cement paste and aggregates is much denser in HSC. Thus, unlike NSC beams in which micro-cracks propagate around aggregates, providing significant aggregate interlock, micro-cracks in HSC are trans-granular, resulting in relatively smoother fracture surfaces, thereby inhibiting aggregate interlock as a shear transfer mechanism and reducing the influence of compressive strength on the ultimate shear strength of HSC beams. In this study, a new approach based on genetic algorithms (GAs) was used to predict the shear capacity of both NSC and HSC slender beams without shear reinforcement. Shear capacity predictions of the GA model were compared to calculations of four other commonly used methods: the ACI method, CSA method, Eurocode-2, and Zsutty's equation. A parametric study was conducted to evaluate the ability of the GA model to capture the effect of basic shear design parameters on the behaviour of reinforced concrete (RC) beams under shear loading. The parameters investigated include compressivestrength, amount of longitudinal reinforcement, and beam's depth. It was found that the GA model provided more accurate evaluation of shear capacity compared to that of the other common methods and better captured the influence of the significant shear design parameters. Therefore, the GA model offers an attractive user-friendly alternative to conventional shear design methods.

• Computers and Concrete
• /
• v.22 no.5
• /
• pp.481-492
• /
• 2018

In this paper, a new hybrid fiber system (NHFS) is investigated for the application of slab. The steel fiber, polyvinyl alcohol (PVA) fiber and calcium carbonate ($CaCO_3$) whisker is added to form NHFS. The four-point bending test is carried out on the flexural properties of slab with plain, steel fiber, traditional hybrid fiber system (THFS) and NHFS reinforced cementitious composites. The flexural behavior is evaluated by ASTM C1018-97, JCI-SF4 and post-crack strength (PCS) technique. The evaluation parameters of flexural toughness such as toughness index (TI), equivalent flexural strength (EFS) and PCS are determined. The size of slab specimens is $15mm(thickness){\times}50mm(width){\times}200mm(length)$. The results show that adding $CaCO_3$ whisker to THFS can significantly improve the flexural strength, TI, EFS, PCS of the slab. The empirical relation between reinforcing index ($RI_v$) and flexural parameters show that flexural parameters of slabs increase first and then decrease; which indicates that optimum $RI_v$ values can be helpful in the considering the mix design of steel-PVA fibers-$CaCO_3$ whisker composites for achieving the desired flexural-related properties. The scanning electron microscopy is performed to observe the micro-morphological characteristics of the fracture surface, which proved the positive hybrid effect among the different fibers in cementitious composites. The NHFS can arrest the generation and propagation of the crack from micro to macro level.