• Proceedings of the Korea Concrete Institute Conference
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• 2004.11a
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• pp.577-580
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• 2004

Recently, DFRCCs (Ductile Fiber Reinforced Cementitious Composites), materials with remarkable ductility when compared to ordinary fiber-reinforced concrete (FRC), have been developed and studied actively in the US, Japan, and many European countries. The transformation of failure behavior from brittle to ductile is achieved by incorporating with fracture mechanics concept especially micro-mechanical models approach of cementitious composite materials in manufacturing ordinary fiber-reinforced composites. The purpose of this study is to accurately understand the shear behavior of DFRCC repaired RC beams. Using a four-point bending test, the shear strengths and shear stress-deflection relations of DFRCC repaired RC specimens are obtained. The results show that DFRCC can be effectively used for repairing materials for concrete structures.

• Proceedings of the Korea Concrete Institute Conference
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• 2006.11a
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• pp.229-232
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• 2006

The HPFRCCs show that the multiple crack propagation, high tensile strength and ductility due to the interfacial bonding of the fibers to the cement matrix. Moreover, performance of cement composites varies according to type and weight contents of reinforcing fiber. and HPFRCCs with hybrid fiber have better performance than HPFRCCs with single fiber in damage tolerance. Total four cylindrical specimens were tested, and the main variables were the type and weight contents of fiber, which was polyvinylalchol (PVA), polyethylene (PE). In order to clarify effect of hybrid types on the characteristics of fracture and damage process in cement composites, AE method was performed to detect micro-cracking in HPFRCCs under cyclic compression. Loading conditions of the uniaxial compression test were monotonic and cyclic loading. And from AE parameter value, it is found that the second and third compressive load cycles resulted in successive decrease of the amplitude as compared with the first compressive load cvcle.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2015.05a
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• pp.124-124
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• 2015

Acoustic microscopy and scanning electron microscopy were applied to non-destructively evaluate the hydrogen-induced cracking of API X-80 steels and to find the initiation time of the crack. The API X-80 steel had the average grain size of about $4-10{\mu}m$. The hardness was reduced from 240 to 202 [Hv] after exposing in HIC environment for 2-days. Friction coefficient and wear loss were 0.745 and 0.392 mm, respectively. Empirical equation of corrosion potential and corrosion rate of the steel with HIC time in $5%NaCl-0.5%CH_3COOH$ at $25^{\circ}C$ were $Eh\;(up)=0.06^*t[day]+0.2951$, $Eh(down)=0.376^*t[day]+0.5938$, respectively. HIC grew with micro-size after 1-day exposure. The HIC tended to propagate on the surface with Al, Si, Ti, and Mn.

• Journal of Surface Science and Engineering
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• v.25 no.3
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• pp.133-143
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• 1992

Titanium nitride(TiN) films have been prepared by HCD plasma enhanced reactive ion plating. Density and temperature of the plasma generated by the HCD were investigated. It was shown that parameters such as the substrate bias voltage(0 350V) and N2 flow rate(10 180SCCM) influenced the growth, the growth, the microstructure and the color tone of the film mostly. In order to study the interface region, surface analysis by AES combined with sputter depth profiling was performed. Microhardness of the coated TiN films were measured by micro Vickers hardness tester. Also, the effect of coating parameters on composition, coating surface and fracture morphology, grain size and growth rate were examined.

• Advances in concrete construction
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• v.3 no.1
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• pp.15-37
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• 2015

Ongoing efforts for improved fracture toughness of engineered cementitious materials address the inherent brittleness of the binding matrix at several different levels of the material's geometric scale through the addition of various types of reinforcing fibers. Crack control is required for crack widths that cover the entire range of the grain size spectrum of the material, and this dictates the requirement of hybrid mixes combining fibers of different size (nano, micro, macro). Use of Carbon Nano-Tubes (CNT) and Carbon Nano-Fibers (CNFs) as additives is meant to extend the crack-control function down to the nanoscale where cracking is believed to initiate. In this paper the implications of enhanced toughness thus attained at the material nanostructure are explored, with reference to the global smeared constitutive properties of the material, through consistent interpretation of the reported experimental evidence regarding the behavior of engineered cementitious products to direct and indirect tension.

• Coupled systems mechanics
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• v.11 no.5
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• pp.411-438
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• 2022

In this paper, we present the parameter identification for inelastic and multi-scale problems. First, the theoretical background of several fundamental methods used in the upscaling process is reviewed. Several key definitions including random field, Bayesian theorem, Polynomial chaos expansion (PCE), and Gauss-Markov-Kalman filter are briefly summarized. An illustrative example is given to assimilate fracture energy in a simple inelastic problem with linear hardening and softening phases. Second, the parameter identification using the Gauss-Markov-Kalman filter is employed for a multi-scale problem to identify bulk and shear moduli and other material properties in a macro-scale with the data from a micro-scale as quantities of interest (QoI). The problem can also be viewed as upscaling homogenization.

• Structural Engineering and Mechanics
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• v.84 no.2
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• pp.253-268
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• 2022

Using non-destructive Acoustic Emission (AE) and optical Digital Image Correlation (DIC) methods, the moment-curvature behavior of steel and GFRP bars reinforced concrete beams under flexure was explored in this study. In the tension zone, laboratory studies were carried out on steel-RC and GFRP-RC beams with varying percentages of longitudinal reinforcement ratios of 0.33 %, 0.52%, and 1.11%. The distinct mechanism of cracking initiation and fracture progression of failure in steel-RC and GFRP-RC beams were effectively correlated and picked up using AE waveform characteristics of the number of AE hits and their amplitudes, AE energy as well as average frequency and duration. AE XY event plots and longitudinal strain profiles using DIC gives an online and real-time visual display of progressive AE activity and strains respectively to efficaciously depict the crack evolution and their advancement in steel-RC and GFRP-RC beams. They display a close matching with the micro and macro-cracks visually observed in the actual beams at various stages of loading.

• Journal of the Microelectronics and Packaging Society
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• v.19 no.4
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• pp.57-64
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• 2012

Ball shear test was performed by test variables such as loading speed and annealing time in order to investigate the effect of surface finishes on the bonding strength of Sn-1.2Ag-0.7Cu-0.4In Pb-free solder. The shear strength increased and the ductility decreased with increasing shear speed. With increasing shear speed, the electroless nickel immersion gold (ENIG) finish showed dominant brittle fracture mode, while organic solderability preservative (OSP) finish showed pad open fracture mode. The shear strength and toughness for both surface finishes decreased with increasing annealing time under the high-speed shear test of 500 mm/s. Typically, the thickness of intermetallic compound increased with increasing annealing time, which means that exposure of brittle fracture became much easier. With increasing annealing time, the both ENIG and OSP finishes exhibited the pad open fracture mode. Overall, ENIG finish showed higher shear strength rather than OSP finish due to its superior barrier stability.

• Journal of the Korea Concrete Institute
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• v.21 no.4
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• pp.457-464
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• 2009

Fiber is an important ingredient in fiber-reinforced cement composite (FRCC) which can control fracture of cement composite by bridging action. In compliance with the action of the fiber and the aggregate size, it also showed a different failure mechanism. For practical application, it is needed to investigate the fracture behavior of the FRCC and to understand the micro-mechanism of cement matrix with reinforcing fiber. In order to evaluate a characteristics of fracture process in the FRCC, acoustic emission (AE) technique was used for the analysis and evaluation of FRCC damage by acoustic emission under flexural and cyclic compressive loadings. The AE signals were monitored by AMSY4 AE instrument during the entire loading period. The specimens are reinforced with 0, 1.0, 1.5 and 2.0% (by volume) Polyvinyl alcohol (PVA) fiber. The test results showed that the damage progress of the FRCC was characteristic for the fiber replacement ratio. As a result of analyzing the felicity ratio (FR) values, it is shown that this values can be used for evaluating the degree of FRCC damage. On the whole the felicity ratio values of FRCC are shown between 0.4 and 1.1. And, the AE kaiser effect was shown in the all FRCC specimen. In addition, the damage behavior and the microscopic fracture process of the FRCC are evaluated using the AE parameters, such as calm ratio, b-value and felicity ratio. The purpose of this reserch was to advance the state of knowledge regarding the applicability of acoustic emission as an evaluation method for FRCC.

• Korean Journal of Materials Research
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• v.12 no.9
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• pp.750-760
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• 2002

In this study, three solders, Sn-37Pb, Sn-3.5Ag, and Sn-3.8Ag-0.7Cu were screen printed on both electroless Ni/Au and OSP metal finished micro-via PCBs (Printed Circuit Boards). The interfacial reaction between PCB metal pad finish materials and solder materials, and its effects on the solder bump joint mechanical reliability were investigated. The lead free solders formed a large amount of intermetallic compounds (IMC) than Sn-37Pb on both electroless Ni/Au and OSP (Organic Solderabilty Preservatives) finished PCBs during solder reflows because of the higher Sn content and higher reflow temperature. For OSP finish, scallop-like $Cu_{6}$ /$Sn_{5}$ and planar $Cu_3$Sn intermetallic compounds (IMC) were formed, and fracture occurred 100% within the solder regardless of reflow numbers and solder materials. Bump shear strength of lead free solders showed higher value than that of Sn-37Pb solder, because lead free solders are usually harder than eutectic Sn-37Pb solder. For Ni/Au finish, polygonal shaped $Ni_3$$Sn_4$ IMC and P-rich Ni layer were formed, and a brittle fracture at the Ni-Sn IMC layer or the interface between Ni-Sn intermetallic and P-rich Ni layer was observed after several reflows. Therefore, bump shear strength values of the Ni/Au finish are relatively lower than those of OSP finish. Especially, spalled IMCs at Sn-3.5Ag interface was observed after several reflow times. And, for the Sn-3.8Ag-0.7Cu solder case, the ternary Sn-Ni-Cu IMCs were observed. As a result, it was found that OSP finished PCB was a better choice for solders on PCB in terms of flip chip mechanical reliability.