• Title/Summary/Keyword: method validation #5

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Finite element based modeling and thermal dynamic analysis of functionally graded graphene reinforced beams

  • Al-Maliki, Ammar F.H.;Ahmed, Ridha A.;Moustafa, Nader M.;Faleh, Nadhim M.
    • Advances in Computational Design
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    • v.5 no.2
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    • pp.177-193
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    • 2020
  • In the present research, dynamic analysis of functionally graded (FG) graphene-reinforced beams under thermal loading has been carried out based on finite element approach. The presented formulation is based on a higher order refined beam element accounting for shear deformations. The graphene-reinforced beam is exposed to transverse periodic mechanical loading. Graphene platelets have three types of dispersion within the structure including uniform-type, linear-type and nonlinear-type. Convergences and validation studies of derived results from finite element approach are also presented. This research shows that the resonance behavior of a nanocomposite beam can be controlled by the GPL content and dispersions. Therefore, it is showed that the dynamical deflections are notably influenced by GPL weight fractions, types of GPL distributions, temperature changes, elastic foundation and harmonic load excitation frequency.

A Practical Power System Stabilizer Tuning Method and its Verification in Field Test

  • Shin, Jeong-Hoon;Nam, Su-Chul;Lee, Jae-Gul;Baek, Seung-Mook;Choy, Young-Do;Kim, Tae-Kyun
    • Journal of Electrical Engineering and Technology
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    • v.5 no.3
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    • pp.400-406
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    • 2010
  • This paper deals with parameter tuning of the Power System Stabilizer (PSS) for 612 MVA thermal power plants in the KEPCO system and its validation in a field test. In this paper, the selection of parameters, such as lead-lag time constants for phase compensation and system gain, is optimized using linear and eigenvalue analyses. This is then verified through the time-domain transient stability analysis. In the next step, the performance of PSS is finally verified by the generator's on-line field test. After the field test, measured and simulated data are also compared to prove the effectiveness of the models used in the simulations.

Vortex excitation model. Part II. application to real structures and validation

  • Lipecki, T.;Flaga, A.
    • Wind and Structures
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    • v.16 no.5
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    • pp.477-490
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    • 2013
  • This paper presents results of calculations performed according to our own semi-empirical mathematical model of critical vortex excitation. All calculations are carried out using own computer program, which allows the simulation of both the across-wind action caused by vortices and the lateral response of analysed structures. Vortex excitation simulations were performed in real time taking into account wind-structure interaction. Several structures of circular cross-sections were modelled using a FEM program and calculated under the action of critical vortex excitation. Six steel chimneys, six concrete chimneys and two concrete towers were considered. The method of selection and estimation of the experimental parameters describing the model are also presented. Finally, the results concerning maximum lateral top displacements of the structures are compared with available full-scale data for steel and concrete chimneys.

An Efficient Rectification Algorithm for Spaceborne SAR Imagery Using Polynomial Model

  • Kim, Man-Jo
    • Korean Journal of Remote Sensing
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    • v.19 no.5
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    • pp.363-370
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    • 2003
  • This paper describes a rectification procedure that relies on a polynomial model derived from the imaging geometry without loss of accuracy. By using polynomial model, one can effectively eliminate the iterative process to find an image pixel corresponding to each output grid point. With the imaging geometry and ephemeris data, a geo-location polynomial can be constructed from grid points that are produced by solving three equations simultaneously. And, in order to correct the local distortions induced by the geometry and terrain height, a distortion model has been incorporated in the procedure, which is a function of incidence angle and height at each pixel position. With this function, it is straightforward to calculate the pixel displacement due to distortions and then pixels are assigned to the output grid by re-sampling the displaced pixels. Most of the necessary information for the construction of polynomial model is available in the leader file and some can be derived from others. For validation, sample images of ERS-l PRI and Radarsat-l SGF have been processed by the proposed method and evaluated against ground truth acquired from 1:25,000 topography maps.

Ni-Ti actuators and genetically optimized compliant ribs for an adaptive wing

  • Mirone, Giuseppe
    • Smart Structures and Systems
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    • v.5 no.6
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    • pp.645-662
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    • 2009
  • Adaptive wings are capable of properly modifying their shape depending on the current aerodynamic conditions, in order to improve the overall performance of a flying vehicle. In this paper is presented the concept design of a small-scale compliant wing rib whose outline may be distorted in order to switch from an aerodynamic profile to another. The distortion loads are induced by shape memory alloy actuators placed within the frame of a wing section whose elastic response is predicted by the matrix method with beam formulation. Genetic optimization is used to find a wing rib structure (corresponding to the first airfoil) able to properly deforms itself when loaded by the SMA-induced forces, becoming as close as possible to the desired target shape (second airfoil). An experimental validation of the design procedure is also carried out with reference to a simplified structure layout.

Quantification of intact ambroxol tablet using near-infrared spectroscopy

  • Kim, Do-Hyung;Lim, Hun-Rang;Woo, Young-Ah;Kim, Hyo-Jin;Kang, Shin-Jung;Choi, Hyun-Chul;Choi, Han-Gon
    • Proceedings of the PSK Conference
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    • 2003.04a
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    • pp.279.1-279.1
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    • 2003
  • NIR reflectance spectroscopy, using a fiber-optic probe was used to determine rapidly and non-destructively the content of ambroxol in intact ambroxol 30 mg (nominal content 12.5% m/m ambroxol) tablets by collecting NIR spectra in range 1100 - 1750 nm and using PLSR calibration method. The tablets (10.3 - 15.9% m/m ambroxol, i.e., 82 - 127% of the nominal label content) were used 7 calibration set and 5 validation set. (omitted)

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Nonlinear viscous material model

  • Ivica Kozar;Ivana Ban;Ivan Zambon
    • Coupled systems mechanics
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    • v.12 no.5
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    • pp.419-428
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    • 2023
  • We have developed a model for estimating the parameters of viscous materials from indirect tensile tests for asphalt. This is a simple Burger nonlinear rheological two-cell model or standard model. At the same time, we begin to develop a more versatile and complex multi-cell model. The simple model is validated using experimental load-displacement results from laboratory tests: The recorded displacements are used as input values and the measured force data are simulated with the model. The optimal model parameters are estimated using the Levenberg-Marquardt method and a very good agreement between the experimental results and the model calculations is shown. However, not all parts of the model are active in the loading phase of the experiment, so we extended the validation of the model to the simulation of the relaxation behaviour. In this stage, the other model parameters are activated and the simulation results are consistent with the literature. At this stage, we have estimated the parameters only for the two-cell uniaxial model, but further work will include results for the multi-cell model.

Determination of methamphetamine and amphetamine enantiomers in human urine by chiral stationary phase liquid chromatography-tandem mass spectrometry

  • Sim, Yeong Eun;Ko, Beom Jun;Kim, Jin Young
    • Analytical Science and Technology
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    • v.32 no.5
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    • pp.163-172
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    • 2019
  • Methamphetamine (MA) is currently the most abused illicit drug in Korea and its major metabolite is amphetamine (AP). As MA exist as two enantiomers with the different pharmacological properties, it is necessary to determine their respective amounts in a sample. Thus a chiral stationary phase liquid chromatography-tandem mass spectrometric (LC-MS/MS) method was developed for identification and quantification of d-MA, l-MA, d-AP, and l-AP in human urine. Urine sample ($200{\mu}L$) was diluted with pure water and purified using solid-phase extraction (SPE) cartridge. A $5-{\mu}L$ aliquot of SPE treated sample solution was injected into LC-MS/MS system. Chiral separation was carried out on the Astec Chirobiotic V2 column with an isocratic elution for each enantiomer. Identification and quantification of enantiomeric MA and AP was performed using multiple reaction monitoring (MRM) detection mode. Linear regression with a $1/x^2$ as the weighting factor was applied to generate a calibration curve. The linear ranges were 25-1000 ng/mL for all compounds. The intra- and inter-day precisions were within 3.6 %, while the intra- and inter-day accuracies ranged from -5.4 % to 11.8 %. The limits of detection were 2.5 ng/mL (d-MA), 3.5 ng/mL (l-MA), 7.5 ng/mL (d-AP), and 7.5 ng/mL (l-AP). Method validation parameters such as selectivity, matrix effect, and stability were evaluated and met acceptance criteria. The applicability of the method was tested by the analysis of genuine forensic urine samples from drug abusers. d-MA is the most common compound found in urine and mainly used by abusers.

Comparison of Analysis Methods for Ammonia from Swine Production Facilities

  • Kim, Ki Y.;Choi, Hong L.;Kim, Chi N.
    • Asian-Australasian Journal of Animal Sciences
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    • v.17 no.11
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    • pp.1608-1614
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    • 2004
  • This study was performed to evaluate the accuracy, validation and applicability of UV spectrophotometer (UV), Ion Chromatography (IC), and Detector tube (DT) methods for measuring ammonia (NH3) concentration in a swine confinement house and swine slurry storage tank. The mean values of $NH_{3}$ emitted from the house and slurry were 5.333 ppm and 42.192 ppm for the IC method; 4.13 ppm and 36.29 ppm for the Detector tube; and 5.417 ppm and 34.193 ppm for the UV method. The accuracy and the correlation of an ammonia level analyzed by the IC method compared to the UV method were 98% and 0.998($R^{2}$) in the swine confinement house and 94% and 0.997($R^{2}$) in the swine slurry storage tank. On the other hand, those of ammonia level measured by the Detector tube compared to the UV method were 77% and 0.957($R^{2}$) in the swine confinement house and 82% and 0.941($R^{2}$) in the swine slurry storage tank. This indicated that the accuracy and the correlation of the IC method compared to the UV method were higher than those of the Detector tube method compared to the UV method. Therefore, it was concluded that the IC method was more accurate in measuring ammonia concentration in a swine house and a swine slurry storage tank. The Detector tube method should not be applied to the swine slurry storage tank in which ammonia concentration is generally higher than 30 ppm because low accuracy is caused by a gross space between scales inscribed in the Detector tube.

Method Validation for the Determination of Eleutherosides and β-Glucan in Acanthopanax koreanum (탐라오가피의 Eleutheroside B, E 및 β-Glucan 함량 분석 및 분석법 검증)

  • Kim, Young-Hyun;Bae, Da-Bin;Park, Sun-Ok;Lee, Sang-Jong;Cho, Ok-Hyun;Lee, Ok-Hwan
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.42 no.9
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    • pp.1419-1425
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    • 2013
  • The aim of this study was to investigate the method validation for the determination of eleutherosides (B and E) and ${\beta}$-glucan in Acanthopanax (A.) koreanum. This medicinal plant reportedly mainly included eleutherosides which exhibit the pharmacological effects, and ${\beta}$-glucan substantially enhances the function of the immune system by activating macrophages. The specificity, linearity, precision, accuracy, limit of detection (LOD, S/N=3), and limit of quantification (LOQ, S/N=10) were measured by HPLC and enzymatic methods. Our results showed that the coefficient of calibration correlation ($R^2$) for eleutheroside B and E were 0.9997 and 0.9999, respectively. The limits of detection (LOD) for eleutheroside B and E were $0.050{\mu}g/mL$ and $0.025{\mu}g/mL$, respectively. The recovery rate of eleutheroside B and E were revealed in the high range of 100.66~110.04% and 94.26~111.62%, respectively. The inter-day precision of eleutheroside B and E in the root and stem in A. koreanum were 1.4~5.0% and 1.1~2.5%, respectively. The intra-day precision of eleutheroside B and E in the root and stem in A. koreanum were 2.8~2.9% and 0.4~1.1%, respectively. Furthermore, the inter-day and intra-day precision of ${\beta}$-glucan in the stem, leaf, and fruit of A. koreanum were 1.32~5.67% and 8.01~11.76%, respectively. In conclusion, the methods were validated for the detection of eleutherosides and ${\beta}$-glucan in A. koreanum.