• 제목/요약/키워드: metallurgical technology

검색결과 691건 처리시간 0.023초

Low temperature-operating NiO-CoO butane gas sensors

  • 정동호;최순돈;민봉기
    • 센서학회지
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    • 제17권4호
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    • pp.303-307
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    • 2008
  • $NiO,\;Cu_2O,\;Mn_2O_3$ and $Cr_2O_3$ as p-type semiconductors were added in CoO with 15 wt.% ethylene glycol binder and measured the butane gas sensing characteristics. The highest sensitivity is obtained for the NiO-CoO sensors. CoO-20 at.% NiO sensor with 15 wt.% ethylene glycol binder sintered at $1100^{\circ}C$ for 24 h exhibits high sensitivity of 90 % to 5000 ppm butane gas at the sensor temperature of $250^{\circ}C$, compared to low sensitivities at the low operating temperature for commercial sensors. Response and recovery times are, respectively, within few seconds and 1min in the static flow system, indicating rapid adsorption and desorption of butane gas on sensor surface even at this low temperature.

Density of Molten Salt Mixtures of Eutectic LiCl-KCl Containing UCl3, CeCl3, or LaCl3

  • Zhang, C.;Simpson, M.F.
    • 방사성폐기물학회지
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    • 제15권2호
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    • pp.117-124
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    • 2017
  • Densities of molten salt mixtures of eutectic LiCl-KCl with $UCl_3$, $CeCl_3$, or $LaCl_3$ at various concentrations (up to 13 wt%) were measured using a liquid surface displacement probe. Linear relationships between the mixture density and the concentration of the added salt were observed. For $LaCl_3$ and $CeCl_3$, the measured densities were significantly higher than those previously reported from Archimedes' method. In the case of $LiCl-KCl-UCl_3$, the data fit the ideal mixture density model very well. For the other salts, the measured densities exceeded the ideal model prediction by about 2%.

Fe-7%Ni-0.4%C 마르텐사이트합금의 미세조직과 진동감쇠능에 미치는 용체화처리온도의 영향 (Effect of Solution-Treatment Temperature on Microstructure and Damping Capacity of a Martensitic Fe-7%Ni-0.4%C Alloy)

  • 이영국;지광구;최종술
    • 열처리공학회지
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    • 제11권1호
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    • pp.1-9
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    • 1998
  • The objective of this study is to investigate the effect of solution-treatment temperature on the microstructure and damping capacity of a martensitic Fe-7%Ni-0.4%C alloy. The size of lath increased from $0.3{\mu}m$ to $0.55{\mu}m$ with increasing the solution-treatment temperature from 700 to $1100^{\circ}C$. In addition, the size of block, packet, and austenite grain had tendency to increase with increasing solution-treatment temperature. The damping capacity of the Fe-7%Ni-0.4%C martensitic alloy decreased with increasing the solution treatment temperature. The reason is not attributed to the increase in the size of lath, block, packet, and austenite grain, but to the increase in vacancy concentration which hinders dislocation motion.

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열간단조공정중 강의 재결정거동 유한요소해석 (Prediction of Recrystallization Behaviors in Hot Forging by the Finite Element Method)

  • 곽우진;이경종;권오준;황상무
    • 소성∙가공
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    • 제5권4호
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    • pp.305-319
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    • 1996
  • In this paper a finite element based system is presented for the prediction of the distributions of the recrystallized grain sizes in the workpiece in hot forging. The system adopts a fully coupled finite element thermo-mechanical model for predicting plastic deformation and heat transfer occurring in the workpiece and employs existing metallurgical models relating the recrystalliza-tion behavior with the thermo-mechanical variables such as temperatures strain and strain rate. The system is applied to upsetting of cylindrical preform. The predicted grain sizes are compared with the measurements. It is further applied to forging of a complex-shaped product.

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기계적합금화한 FeAl 나노결정립의 회절특성 (Diffraction Characteristics of Mechanically Alloyed Nanocrystalline FeAl)

  • 최근섭;김도향;홍경태
    • Applied Microscopy
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    • 제27권4호
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    • pp.473-481
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    • 1997
  • Disorder-order transformation of nanocrystalline FeAl have been investigated by a combination of electron and X-ray diffraction analysis including high resolution electron microscopy and differential scanning calorimetry. Fe-50at.%Al powders mechanically alloyed for 90 hours consist of $5\sim10$ nm size grains haying either disordered b.c.c. structure or amorphous structure. X-ray and electron diffraction of mechanically alloyed FeAl powders show that disorder-order transformation occurs at the temperature range of $300^{\circ}C\sim320^{\circ}C$. Such a low-temperature ordering behavior exhibiting an exothermic reaction is attributable to the nm-scale grain structure with a large amount of defects accumulated during mechanical alloying process.

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열간금형용강의 희토류붕화처리에 관한 연구 (A Study on the Rare-earth Boronizing Treatment of STD 61 Steel)

  • 김창규;윤재홍;장윤석
    • 열처리공학회지
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    • 제13권4호
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    • pp.217-223
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    • 2000
  • The boronizing effects of STD 61 steel have been studied on the micro structure and hardness. The STD 61 Steel was soaked in molten salt, consisted of KCl, $BaCl_2$, NaF, $B_2O_3$, FeB, and Ce, at various temperatures and times. The boronizing conditions for the peak hardness were the temperature range of $900^{\circ}C$ to $950^{\circ}C$ for 5 hr and that of $1000^{\circ}C$ for 3 hr, respectively. Four boride layers such as FeB, $Fe_2B$, ${\alpha}$ and matrix layer surface were observed from the microscopic surface examination. The thickness of boride layer was increased by increasing the boronizing time and the temperature. The structure of boride layer was tooth shape.

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강제대류시 고순도 Al괴의 응고조직에 미치는 유동의 영향 (A Study on the Effect of Fluid Flow on the Microstructure of High Purity Al Ingot under Forced Flow)

  • 김경민;김헌주;하기윤;윤의박
    • 한국주조공학회지
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    • 제13권6호
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    • pp.540-546
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    • 1993
  • The effects of fluid flow on the purification of aluminum were studied. As the revolution rate(N) increased, the size of columnar grain decreased gradually. The concentration of solidified crystal was decreased with increasing distance from chill and revolution rate(N). Distribution boundary layer thickness(${\delta}$) was calculated from the solute distribution obtained in solid experimentally and by use of BPS equation. The value of ${\delta}$ changed from about $60{\mu}m$ at N value of 27rpm to about $15{\mu}m$ at N value of 1000rpm. From this result, high purification was obtained by decreasing the diffusion boundary layer under forced convection.

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폐주물사의 용융공정에서의 물질 및 에너지 수지의 해석 (Analysis of Energy and Material Balance in Smelting Process of Waste Sand)

  • 정원섭;민동준;윤수종
    • 한국주조공학회지
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    • 제15권5호
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    • pp.477-482
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    • 1995
  • A computer simulation model of various smelting process for melting waste sand was developed by using energy and material balance concept. This model can predict the coal, flux and oxygen consumption and the volume and temperature of off-gas. The major critical variables for smelting process can be explained by using the analysis of energy and material balance. The major conclusions were as follows; 1. The most important variables for smelting process were high post-combustion ratio, high heat transfer efficiency and refractory protection technology. 2. For saving energy in this smelting process, selection of raw materials i.e coal, flux are very important, espacially using of low volatile coal is very profitable. 3. The treatment cost of waste sand is high and environmental restriction is severe, in this reason we must be concerned in the treatment of waste sand by smelting process.

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Effect of the Cooling Rates on the Corrosion Resistance and Phase Transformation of 14Cr-3Mo Martensitic Stainless Steel

  • Park, Jee-Yong;Park, Yong-Soo
    • Corrosion Science and Technology
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    • 제5권1호
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    • pp.1-4
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    • 2006
  • Martensitic stainless steel is used when mechanical properties such as high tensile strength and hardness are required. Medium carbon-contained martensitic stainless steel which contains more than 0.2 wt% of carbon should be heat-treated and quenched at the temperature where undissolved carbides are totally dissolved into the matrix. In particular, the dissolution and reprecipitation behaviors of various forms of carbides are affected by such parameters as heating rate, heating temperature, duration time and cooling rate. This study is to investigate the effects of heat treatment parameters of 14Cr-3Mo martensitic stainless on corrosion resistance and phase transformation in relation to the dissolution and reprecipitation of carbides.