• 제목/요약/키워드: metallurgical

검색결과 2,375건 처리시간 0.03초

BSCCO 고온초전도 선재의 접합특성 연구 (A Study of Joint Characteristic of BSCCO Superconductor Tape)

  • 김정호;김중석;김태우;지봉기;주진호;나완수
    • 한국초전도학회:학술대회논문집
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    • 한국초전도학회 1999년도 High Temperature Superconductivity Vol.IX
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    • pp.378-382
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    • 1999
  • We evaluated the effect of joining process such as contact method, shape of joined area and pressure on the electrical property of Bi-2223 superconducting tape. It was observed that the current capacity was reduced at the transition area of the joined tape and was significantly dependent on the uniaxial pressure. The lap-joined tape, fabricated with a pressure of 1,000-1,600 MPa, show the highest value of current capacity(80-90%) of the tape itself. It is believed the highest value of current capacity results from improvement in core density, contacting area and grain alignment, etc. In addition, the irreversible strain( ${\varepsilon}$ irrev) for the joined tape· was measured to be 0.1%, smaller than that of enjoined tape( ${\varepsilon}$ irrev = 0.3%). The decrease in the strength and irreversible strain for joined tape is believed to be due to the irregular geometry/morphology of the transition area of the tape.

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Investigation of long-term stability of pentacene thin-film transistors encapsulated with transparent $SnO_2$

  • Kim, Woo-Jin;Koo, Won-Hoe;Jo, Sung-Jin;Kim, Chang-Su;Baik, Hong-Koo
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2005년도 International Meeting on Information Displayvol.II
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    • pp.1276-1279
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    • 2005
  • The long-term stability of pentacene thin-film transistors (TFTs) encapsulated with a transparent $SnO_2$ thin-film prepared by ion beam assisted deposition (IBAD) was investigated. With a buffer layer of thermally evaporated 100 nm $SnO_2$ film deposited prior to IBAD process, our encapsulated OTFTs sustained its initial field-effect mobility up to one month and then gradually degraded showing only 37% reduction compared to 90% reduction of non-encapsulated OTFTs after 100 days in air ambient. The encapsulated OTFTs also exhibited superior on/off current ratio of over $10^5$ to that of the unprotected devices $({\sim}10^4)$ which was reduced from ${\sim}10^6$ before aging. Therefore, the enhanced long-term stability of our encapsulated OTFTs should be attributed to well protection of permeation of $H_2O$ and $O_2$ into the devices by the IBAD $SnO_2$ thin-film which could be used as an effective inorganic gas barrier for transparent organic electronic devices.

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Ni-MH 2차 전지용 Zr계 수소저장합금전극의 특성에 미치는 치환원소(Co, Cr, Fe)의 영향 (The effect of substitution elements(Co, Cr, Fe) on the properties of Zr-based hydrogen storage alloy electrode for Ni-MH secondary battery)

  • 최승준;정소이;서찬열;최전;박충년
    • 한국수소및신에너지학회논문집
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    • 제10권3호
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    • pp.185-189
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    • 1999
  • Effects of alloy modification with the $Zr_{0.6}Ti_{0.4}V_{0.4}Ni_{1.2}Mn_{0.4}$ alloy for an electrode use have been investigated. For the alloy composition, a part of Mn was substituted by Co, Cr and Fe. The experimental results showed that Co accelerated activation of alloy, and Fe and Cr improved the discharge capacity. These results agree with P-C-T curves of each alloy. But substituting Fe for Mn showed the decrease of the discharge capacity when discharged at high rate (60mA, about 1C rate). Considering both the discharge capacity and the high rate discharge property, $Zr_{0.6}Ti_{0.4}V_{0.4}Ni_{1.2}Mn_{0.3}Cr_{0.1}$ alloy was found to be the best alloy among the alloys subjected to the test.

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압연이 Ni-MH 2차전지용 금속수소화물 전극의 충·방전 특성에 미치는 영향 (The Effect of Rolling on the Charge-Discharge Characteristic of Metal Hydride Electrode for Ni-MH Secondary Battery)

  • 박원;장상민;최승준;노학;최전;박충년
    • 한국수소및신에너지학회논문집
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    • 제7권2호
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    • pp.165-171
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    • 1996
  • The effect of rolling on the charge-discharge property was studied for metal hydride negative electrode. $(LM)Ni_{3.6}Al_{0.4}Co_{0.7}Mn_{0.3}$(pleateau pressure : below 1 atm at room temperature, volume expansion : 9%, entalpy : $8.7kcal/molH_2$) alloy was prepared by arc melting, and then it was coated with various copper weight percent. The copper coated alloys were then rolled with the different reduction ratio. From the results, it was found that the maximum discharge capacity increased with increasing reduction ratio, and 15wt% copper coated sample shows the highest discharge capacity, 324mAh/g, after rolling with 30% reduction ratio. In view of cycle life for the negative electrode, the 15wt% copper coated electrode which was rolled with 13% reduction ratio showed the longest cycle life compared with other electrodes.

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The Direct Recycling of Electric Arc Furnace Stainless Steelmaking Dust

  • Zhang, Chuanfu;Peng, Bing;Peng, Ji;Lobel, Jonathan;Kozinski, Janusz A.
    • 대한전자공학회:학술대회논문집
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    • 대한전자공학회 2001년도 The 6th International Symposium of East Asian Resources Recycling Technology
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    • pp.404-408
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    • 2001
  • This paper focuses on the pilot-scale investigation of direct recycling of electric arc furnace (EAF) stainless steelmaking dust. The direct recycling of EAF dust is to make pellets with the mixture of the dust and the reducing agent carbon, then introduce the pellets to the EAF. The valuable metals in the dust are reduced and get into the steel as the alloying elements. Experiments simulating direct recycling in an EAF were performed using an induction furnace. But it seems difficult to reduce all metal oxides in the dust so that some metal reducing agents added in the late stage of reduction process. The valuable metals in the dust were reduced partly by carbon and partly by metal reducing agent for the economical concern. The recovery of iron, chromium and nickel from the flue dust and the amount of metal oxides in the slag were measured. The results showed that the direct recycling of EAF stainless steelmaking dust is practicable. It wes also found that direct recycling of flue EAF stainless steelmaking dusts does not affect the chemistry and quality of stainless steel produced in the EAF. It is benefit not only for the environmental protection but also for the recovery of valuable metal resources in this way.

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STS 304, 316강의 열처리에 따른 산화거동 (An Oxidation Behavior with Heat-treatment in STS 304 and 316)

  • 이경구;윤동주;기회봉;강창석;이도재
    • 열처리공학회지
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    • 제11권3호
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    • pp.186-191
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    • 1998
  • An oxidation behavior of 304 and 316 stainless steels were studied in dry air. After solution treatment, specimens were polished up to $1{\mu}m$ $A1_2O_3$ grade and then subjected to oxidation treatment in dry air at $800^{\circ}C{\sim}1200^{\circ}C$. The oxidation behavior between matrix and oxide scale was analyzed with SEM, EDS and XRD. When oxidation treatment was conducted at $1200^{\circ}C$, large thickness of Fe oxide scale was formed on top of surface and fine $(Cr,Fe)_2O_3$ oxide film was formed below it. Cr rich zone existed at interface between metal and $(Cr,Fe)_2O_3$ oxide layer, and it was believed that this zone acted as obstacle to oxidation. Most of Ni was detected at the interface between metal and $(Cr,Fe)_2O_3$ and also detected at the interface between $Fe_2O_3$ and $(Cr,Fe)_2O_3$.

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냉간압연한 고 Mn 오스테나이트계 스테인리스강의 기계적 성질에 미치는 서브제로처리의 영향 (Effect of Subzero Treatment on the Mechanical Properties of Cold-Rolled High Manganese Austenitic Stainless Steel)

  • 황태현;정목환;이종영;이향백;강창룡
    • 열처리공학회지
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    • 제25권5호
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    • pp.233-238
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    • 2012
  • The effect of subzero treatment on the mechanical properties of cold rolled high manganese austenitic stainless steel was investagated. ${\alpha}$'-martensite was formed by cold rolling, and it was formed with surface relief and specific direction or crossing each other. The volume fraction of martensite increased by subzero treatment, and it was increased with longer time of subzero treatment and higher temperature of subzero treatment. The hardness and strength increased by subzero treatment, while the elongation decreased. With the increase of volume fraction of martensite, the hardness and strength was increased steeply with proportional relationship, elongation was decreased slowly. The results show that the hardness and strength was strongly controlled by the volume fraction of martensite, and the elongation was affected by transformation behavior of deformation induced martensite in the initial stage of deformation.

(Mm)Ni5계 수소저장합금의 전극 특성 (Electrode Characteristics of the (Mm)Ni5-Based Hydrogen Storage Alloys)

  • 한동수;최승준;장민호;최전;박충년
    • 한국수소및신에너지학회논문집
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    • 제6권1호
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    • pp.35-41
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    • 1995
  • The MmNi-based alloy electrode was studied for use as a negative electrode in Ni-MH battery. Alloys with $MmNi_5-_xM_x$(M=Co,Al,Mn) composition were synthesized, and their electrode charateristics of activation rate, temperature dependence, electrode capacity and cycle life were investigated. With increasing Al content and decreasing Mn content in the alloys, the discharge capacity increased while the cycle life decreased. As x in $MmNi_5-_xM_x$ increased from 1.5 to 2.0, decreasing the Ni content, the discharge capacity, the low temperature property and the rate capability decreased. However its cycle life was improved. Increasing Co content resulted in a prolonged cycle life and decrease of high rate discharge capacity. It can be concluded that the most promising alloy in view of discharge capacity and cycle life is $MmNi_{3.5}Co_{0.7}Al_{0.5}Mn_{0.3}$.

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Fe-30Al-5Cr 합금의 미세조직 및 $D0_3{\leftrightarrow}B2$ 천이온도에 미치는 Ti, Hf 및 Zr의 첨가효과 (Effects of Titanium, Hafnium and Zircornium Alloying Elements on Microstructures and $D0_3{\leftrightarrow}B2$ Transition Temperature of Fe-30Al-5Cr Alloys)

  • 김성수;주성민;오선훈;김관휴;최답천
    • 한국주조공학회지
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    • 제21권1호
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    • pp.15-23
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    • 2001
  • The changes in the microstructures and $D0_3{\leftrightarrow}B2$ transition temperature were investigated for Fe-30at.%AI-5at.%Cr alloy with the ordered $D0_3$, structure when Ti, Hf and Zr were added respectively. The addition of Cr has no effect on the microstructure. However, as the amount of Ti addition increased, the grain size became smaller. Addition of Ti+Hf, Ti+Zr and Ti+Hf+Zr also showed the similar effect. When 20at.% of Ti was added, the second phase precipitates on the substrate. The addition of Cr, Hf and Zr alone has no effect on $D0_3{\leftrightarrow}B2$ transition temperature. However, as the amount of Ti addition increased by 5, 10, 15 and 20at.%, the transition temperatures showed 929, 930, 960 and $930^{\circ}C$ respectively.

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Zr/Si 다층박막에서의 고상반응에 의한 비정질상과 결정상의 생성 및 상전이 (Formation of amorphous and crystalline phase, phase sequence by solid state reaction in Zr/Si multilayer thin films)

  • 심재엽;지응준;곽준섭;최정동;백홍구
    • 한국재료학회지
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    • 제4권5호
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    • pp.493-501
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    • 1994
  • DSC와 XRD를 사용하여 Zr/Si 다층박막의 고상반응에 의한 비정질상과 결정상 생성 및 상전이를 확인하고 이를 유효구동력 개념과 유효생성열 개념 및 phase determining factor(PDF)모델을 이용하여 예측한 결과와 비교하였다. Zr/Si 다층박막은 비정질호 반응이 잘 일어났으며 이는 유효구동력 개념으로 예측한 바와 일치하였다. Zr/Si 계에서 생성되는 최초의 결정상은 ZrSi 였으며 유효생성열과 PDF모델로부터 예측된 최초의 결정상은 PDF 모델의 예측 결과와 일치하였다. Zr/Si 다층박막의 원자조성비가 1대 1일경우와 1대 2일 경우의상전이는 ZrSi$\longrightarrow$$ZrSi_{2}$로 되었으며 이러한 상전이 과정은 유효생성열 다이아그램으로 해석되었다. ZrSi의 생성기구는 핵생성이 율속임을 규명하였고 ZrSi와 $ZrSi_{2}$의 생성에 필요한 활성화에너지는 1.64$\pm$0.19eV와 2.28$\pm$0.36eV이었다.

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