• Title/Summary/Keyword: membrane thickness

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A study on wet etching for silicon membrane construction formation (실리콘 Membrane 구조 형성을 위한 Wet Etching에 관한 연구)

  • 김동수;정원채
    • Proceedings of the IEEK Conference
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    • 2001.06b
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    • pp.237-240
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    • 2001
  • In this paper, we have presented processing technique about wet etching for silicon membrane construction formation. In order to make selective etching of backside silicon wafer, we used Si$_3$N$_4$ layer by PECVD(Plasma Enhanced Chemical Vapor Deposition). We have measured the surface thickness in backside silicon wafer after anisortropic wet etching with KOH:distilled water solutions. Through this experiment, we acquired the etching rate for 1.29${\mu}{\textrm}{m}$/min. The average rough of Si-membrane frontside and backside was 0.26${\mu}{\textrm}{m}$, 0.90${\mu}{\textrm}{m}$, respectively.

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Fabrication of Waterproof and Moisture-permeable Polyurethane Nanofiber Multi-Membrane (투습방수성 Polyurethane 나노섬유 Multi-Membrane의 제조)

  • Yang, Jeong-Han;Yoon, Nam-Sik;Kim, In-Kyo;Yeum, Jeong-Hyun
    • Textile Coloration and Finishing
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    • v.23 no.2
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    • pp.107-117
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    • 2011
  • Polyurethane (PU) was synthesized by one-shot process and the PU nanofiber was prepared by electrospinning. In this study, electrospun PU multi-membranes were prepared with various coating thickness ratio of base resin to top resin, where the base resin contains melamine curing agent and acid catalyst and the top resin contains water-repellent agent of fluoro-carbon compounds. The PU nanofiber multi-membranes were analyzed by field-emission scanning electron microscopy, differential scanning calorimeter, breathability, tensile strenth, air permeability and water resistance. The results showed that the PU multi-membrane provided excellent waterproof and moisture permeability.

Development of Metal Substrate with Multi-Stage Nano-Hole Array for Low Temperature Solid Oxide Fuel Cell (저온 고체산화물연료전지 구현을 위한 다층 나노기공성 금속기판의 제조)

  • Kang, Sangkyun;Park, Yong-Il
    • Journal of the Korean Ceramic Society
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    • v.42 no.12 s.283
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    • pp.865-871
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    • 2005
  • Submicron thick solid electrolyte membrane is essential to the implementation of low temperature solid oxide fuel cell, and, therefore, development of new electrode structures is necessary for the submicron thick solid electrolyte deposition while providing functions as current collector and fuel transport channel. In this research, a nickel membrane with multi-stage nano hole array has been produced via modified two step replication process. The obtained membrane has practical size of 12mm diameter and $50{\mu}m$ thickness. The multi-stage nature provides 20nm pores on one side and 200nm on the other side. The 20nm side provides catalyst layer and $30\~40\%$ planar porosity was measured. The successful deposition of submicron thick yttria stabilized zirconia membrane on the substrate shows the possibility of achieving a low temperature solid oxide fuel cell.

Synthesis of Cholesterol-Containing Molecular Multilayer Structure (콜레스테롤을 갖는 분자 다층 구조의 합성)

  • 신재섭
    • Membrane Journal
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    • v.6 no.4
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    • pp.213-218
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    • 1996
  • Cholesterol-containing monomeric surfactants were synthesized, and sonicated in water to form a vesicle solution. This vesicle solution was dried to construct a membrane which had a molecular multilayer structure. Using UV irradiation the surfactants in this membrane were polymerized and molecular weight was determined. Using a X-ray diffractomelet, the thickness of one layer and the regularity of the multilayer were measured.

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Alcohol Production to reduce Energy Consumption by Membrane Separation and Heat Medium -Basic Studies on Alcohol Recovery with Fermentation Process Using the Membrane- (분리막과 열매체를 이용한 저에너지 소비형 알코올 제조 -분리막을 이용한 발효공정에서 알코올 회수의 기초적 연구-)

  • 김재형;박돈희
    • KSBB Journal
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    • v.6 no.4
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    • pp.379-383
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    • 1991
  • Pervaporation can be successfully utilized to recover alcohol from fermentation broths and dilute process streams. Polydimethylsiloxane (thickness: $60\mu$m), such as hydrophobic membrane have been employed in this application to produce an enriched product. The fermented alcohol was continuously extracted, and simultaneously concentrated by pervaporation, from the membrane bioreactor, and the extracted alcohol concentration was 6 to 10 times higher than in the broth. This experimental conditions were 6-10 Torr vacuum line, pH=5, $32^{\circ}C$, 3.5 liters of working volume, 200rpm of agitator speed, and 0.14 wm aeration flow rate.

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Pd-based metallic membranes for hydrogen separation and production

  • Tosti, Silvano;Basile, Angelo
    • Proceedings of the Membrane Society of Korea Conference
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    • 2003.07a
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    • pp.25-28
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    • 2003
  • Low cost composite metallic membranes for the hydrogen separation and production have been prepared by using thin Pd-Ag foils reinforced by metallic (stainless steel and nickel) structures. Especially, “supported membranes” have been obtained by a diffusion welding procedure in which Pd-Ag thin foils have been joined with perforated metals (nickel) and expanded metals (stainless steel): in these membranes the thin palladium foil assures both the high hydrogen permeability and the perm-selectivity while the metallic support provides the mechanical strength. A second studied method of producing "laminated membranes" consists of coating non-noble metal sheets with very thin palladium layers by diffusion welding and cold-rolling. Palladium thin coatings over these metals reduce the activation energy of the hydrogen adsorption process and make them permeable to the hydrogen. In this case, the dense non-noble metal has been used as a support structure of the thin Pd-Ag layers coated over its surfaces: a proper thickness of the metal assures the mechanical strength, the absence of defects (cracks, micro-holes) and the complete hydrogen selectivity of the membrane. membrane.

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Controlled Release of Drugs from Reservoir Type Devices Coated with Porous Polyurethane Membranes (다공성 폴리우레탄으로 피막된 Reservoir형 약물 조절 방출 시스템)

  • Kim, Kil-Soo;Lee, Seung-Jin
    • Journal of Pharmaceutical Investigation
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    • v.23 no.4
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    • pp.207-211
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    • 1993
  • Reservoir type devices were designed for long-term implantable drug delivery system. The reservoir type device was prepared with the polymethacrylic acid gel coated with polyurethane membrane. Release controlling agent (RCA) were employed to control drug release from devices via generation of micropores in the membranes. The polyurethane membrane functioned as a rate controlling barrier. The drug release pattern of hydrogel demonstrated zero order kinetics. The release rate of drugs could be regulated by varying hydrophobicity/hydrophilicity and content of the RCA, as well as the thickness of the polyurethane membrane. The release of drugs from this system was governed by pore mechanism via simple diffusion and osmotic pressure.

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The effect of irradiated cancellous human bone on exophytic bone formation in residual ridge of the beagle dog (방사선 조사 망상골이 외방형 골형성에 미치는 영향)

  • Chung, Mi-Hyun;Herr, Yeek;Kwon, Young-Hyuk;Park, Joon-Bong;Chung, Jong-Hyuk
    • Journal of Periodontal and Implant Science
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    • v.37 no.4
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    • pp.791-803
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    • 2007
  • The purpose of this study was to evaluate exophytically vertical bone formation in residual ridge of the beagle dog by the concept of guided bone regeneration with a titanium reinforced e-PTFE membrane combined with irradiated cancellous human bone. Twelve male beagle dogs(mean age 1.5 years and mean weight 12kg) were used for this study. The alveolar ridges after extraction of all mandibular premolars were surgically and horizontally removed. At 8 weeks after extractions, full-thickness flap was reflected and cortical bone was removed with round bur and copious irrigation. Rectangular parallelepiped(10mm in length, 5mm in width, and 4mm in height) bended with titanium-reinforced e-PTFE(TR e-PTFE) membrane was placed on the decorticated alveolar ridge, fixed with metal pins and covered with full-thickness flap and assigned as a control group. Test groups ere treated with TR e-PTFE membrane filled with irradiated cancellous human bone. Of twelve beagle dogs, four control dogs and four test dogs without membrane exposure to oral cavity were sacrificed at 8 and 16 weeks respectively. The surgical sites were dissected out, fixed in 4% buffered formaldehyde, dyed using a Villanueva staining technique, and processed for embedding in plastic resin. The cutting and grinding methods were routinely processed for histologic and histomophometric analyis of exophytic bone formation as well as statistical analysis. The results of this study were as follows: 1. Exophytic bone formation in the both of experimental groups was increased respectively after surgery from 23.40% at 8 weeks to 46.26% at 16 weeks in the control groups, from 40.23% at 8 weeks to 47.11% at 16 weeks in the test groups(p<0.05). 2. At 8 weeks after surgery, exophytic bone formation was made 40.23% in the test groups and 33.40% in the control groups. Exophytic bone formation was significantly made in the test group more than in the control group. At 16 weeks after surgery, exophytic bone formation was made 44.11% in the test groups and 46.26% in the control groups. Exophytic bone formation was made in the test groups more than in the control groups, but there was no statistically significant differences. 3. The membrane was fixed with metal pins to closely contact it to the bone surface. So, collapse and deviation of the membrane could be prevented and in growth of connective tissue also could be blocked from the periphery of the membrane. On the basis of these findings, wee suggest that intraoral experimental model for exophytic bone formation may be effective to evaluate the effect of bone graft material. And it indicates that combined use of membrane and ICB graft material is more effective than use of membrane only for exophytic bone formation.

A Study on Preparation of Alumina Membranes(1) (알루미나 한외여과막의 제조에 관한 연구(1))

  • 유재근;이응상
    • Journal of the Korean Ceramic Society
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    • v.30 no.7
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    • pp.589-597
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    • 1993
  • The optimum sol solution for making alumina membrane was synthesized by using sol-gel method with aluminium isopropoxide. Two types of supports were made from the $\alpha$-Al2O3 powder. The porosities of supports could be controlled by the forming methods and the heat treatment conditions. After the support was coated with optimum sol solution and heat-treated at 50$0^{\circ}C$ for 1hour, the thickness of crack-free membrane could be controlled reproductively with dipping time.

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Nanofiltration Composite Membranes Based on Poly(vinyl alcohol) (폴리비닐알콜로 제조된 나노복합막)

  • 오남운;제갈종건;이규호
    • Proceedings of the Membrane Society of Korea Conference
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    • 1998.10a
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    • pp.106-108
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    • 1998
  • It has been proved by the study on nanofiltration with PVA dense membranes in our laboratory that the PVA is good material for the formation of chemically stable nanofiltration (NF) membranes. However, the PVA NF composite membranes prepared so far have rarely shown flux and rejection high enough for the commerciallyzation. The reasons for them would be the relatively thick thickness and improper crosslinking degree of the PVA active layers of the composite membranes. In this study, PVA composite membranes with improved nanofiltration properties have been prepared and characterized in terms of the morphology and permeation properties.

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