• Title/Summary/Keyword: melting study

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A Study On Temperature Control Of A Glass Melting Furnace Using Fuzzy Logic (퍼지 로직을 이용한 유리 용해로 온도 제어에 관한 연구)

  • Moon, Un-Chul
    • Proceedings of the KIEE Conference
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    • 1999.07g
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    • pp.2920-2922
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    • 1999
  • 본 논문에서는 유리 용해로의 온도 제어 문제에 있어서, 퍼지 이론의 응용 방식을 제시한다. 유리용해로의 동특성을 분석하고, 이에 적합하도륵 기존 고전적인 제어기와 퍼지 로직을 결합하는 알고리듬을 제시한다. 제시된 제어기는 실제 용해로의 생산공정에 효율적으로 적용되었다.

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Effect of Polymer Characteristics on the Thermal Stability of Retinol Encapsulated in Aliphatic Polyester Nanoparticles

  • Cho, Eun-Chul
    • Bulletin of the Korean Chemical Society
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    • v.33 no.8
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    • pp.2560-2566
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    • 2012
  • The present study investigates how the thermal stability of retinol (vitamin A) encapsulated in polyester nanoparticles is influenced by the types of polyester used for the nanoparticles. A variety of polyester-retinol nanoparticles were prepared with various polyesters like: poly(ethylene adipate), PEA; poly(butylene adipate), PBA; poly(hexamethylene adipate), PHMA; and three polycaprolactones, PCL, of different molecular weights ($M_n$ ~10, 40, and 80K). The chemical stability of retinol in these nanoparticles, monitored in an aqueous solution at $25^{\circ}C$ and $40^{\circ}C$ for 4 weeks, was high in the following order of the nanoparticles prepared with PHMA > PCL 40K > PCL 10K > PCL 80K > PBA~PEA at $25^{\circ}C$ and PCL 10K > PCL 40K > PHMA > PCL 80K > PEA > PBA at $40^{\circ}C$. More importantly, this study has also found that the thermal stability of the retinol in the nanoparticles was closely connected with the melting temperatures of polyesters and polyester nanoparticles. The results were further discussed with possible factors - such as sample preparation condition (or history) and miscibility between the polyesters and retinol - affecting $T_m$ of the polyesters and the nanoparticles.

A Study on Liquid Phase Diffusion Bonding of STS304 using Cu-Mn-Si Insert alloy (Cu-Mn-Si Insert 합금을 이용한 스테인리스강의 액상확산접합에 관한 연구)

  • 임종태;안상욱
    • Journal of Welding and Joining
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    • v.15 no.4
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    • pp.136-142
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    • 1997
  • In this study, the amorphous foil filler, thickness of 20 - $20~30\mu\textrm{m}$ was made to develop Cu-7.5wt%Mn-7.5wt%Si insert alloy(melting point temperature : solidus line 1003K, liquidus line 1070K). Liquid phase diffusion bonding of 304 stainless steels (STS304), is carried out successfully by using developed Cu-7.5Mn-7.5Si insert alloy. Bonding conditions are taken from bonding pressure of 5MPa, bonding temperatures from 1073K to 1423K varied within 50K and brazing holding times of 0, 30, 60 and 240 minutes. As the results, the tensile strength in the liquid phase diffusion bonding is a little bit lower than that in the solid phase diffusion bonding. The authors find out that the liquid phase diffusion bonding needs lower bonding pressure than the others. Therefore, the liquid phase diffusion bonding had an excellent brazability in which the bonding process showed the typical mechanism of diffusion bonding. In corresponding, the new developed insert alloy of low melting pointed Cu-7.5Mn-7.5Si makes possible brazing between the STS304.

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A Study of the Thermal Analysis of Horizontal Fillet Joints by Considering the Bead Shape in GMA Welding (GMA 용접에서 비드형상을 고려한 수평필릿용접부의 온도해석에 관한 연구)

  • Jo, Si-Hun;Kim, Jae-Ung
    • Journal of the Korean Society for Precision Engineering
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    • v.18 no.8
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    • pp.71-78
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    • 2001
  • In GMA(Gas Metal Arc)Welding, the weld size that is a locally melted area of a workpiece is one of the most important considerations in determining the strength of a welded structure. Variations in the weld power and the welding heat flux may affect the weld pool formation and ultimately the size of the weld. Therefore, an accurate prediction of the weld size requires a precise analysis of the weld thermal cycle. In this study, a model which can estimate the weld bead geometry and a method for thermal analysis, including the model, are suggested. In order to analyze the weld bead geometry, a mathematical model was developed with transformed coordinates to apply to the horizontal fillet joints. A heat flow analysis was performed with a two dimensional finite element model that was adopted for computing the base metal melting zone. The reliability of the proposed model and the thermal analysis was evaluated through experiments, and the results showed that the proposed model was very effective for predicting the weld bead shape and good correspondence in melting zone of the base metal.

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Thermal Characteristic Simulation and Property Evaluation of High Melting Point Materials by Pulsed Current Activated Sintering Process (PCAS공정에 의한 고융점 소결체 열전달 해석 및 특성분석)

  • Nam, Hyo-Eun;Jang, Jun-Ho;Park, Hyun-Kuk;Oh, Ik-Hyun
    • Journal of Sensor Science and Technology
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    • v.26 no.3
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    • pp.214-222
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    • 2017
  • In this study, the effects of internal heat treatment associated sintering temperatures were simulated by the Finite Element Method (FEM). The sintering mechanism of pulsed current activated sintering process (PCAS) is still unclear because of some unexplainable heat transfer phenomena in coupled multi-physical fields, as well as the difficulty in measuring the interior temperatures of metal powder. We have carried out simulation study to find out thermal distributions between graphite mold and Ruthenium powder prior to PCAS process. For PCAS process, heating rate was maintained at $100^{\circ}C/min$ the simulation indicates that the sintering temperature range was between $1000^{\circ}C$ to $1300^{\circ}C$ under 60 MPa. The heat transfer inside the Ruthenium sintered-body sample was modelled through the whole process in order to predict the minimum interior temperature. Thermal simulation shows that the interior temperature gradient decreased by graphite punch length and calculation results well agreed with the PCAS field test results.

An experimental study of behavior of defrosting on the fin-tube heat exchanger (핀-관 열교환기에 대한 제상 거동에 관한 실험적 연구)

  • Lee, Kwan-Soo;Kim, Kyu-Woo;Ji, Sung
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.10 no.6
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    • pp.649-657
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    • 1998
  • In this study, the effects of the various conditions of frosting and defrosting on the behavior of defrosting in a fin-tube heat exchanger have been examined experimentally. The electric heater is used for defrosting in a fin-tube heat exchanger It is shown that there are several local maxima in the water draining rate. The amount of residual water on the heat exchanger after the completion of defrosting is kept constant due to surface tension on the heat exchanger. Without considering the degradation of the thermal performance due to the frosting, the defrosting efficiency is improved with increasing amount of the frost irrespective of the frosting condition. The defrosting behavior is affected by the frosting density as well as the frost accumulation, which vary with the experimental operating conditions during the frosting period. The heat loss to the surrounding air decreases, and the melting and defrosting efficiencies show high values with decreasing heat input.

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A STUDY ON THERMAL ANALYSIS OF HORIZONTAL FILLET JOINTS BY CONSIDERING BEAD SHAPE IN GMA WELDING

  • Cho, Si-Hoon;Kim, Jae-Woong
    • Proceedings of the KWS Conference
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    • 2002.10a
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    • pp.151-155
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    • 2002
  • In GMA(Gas Metal Arc)Welding, the weld size that is a locally melted area of a workpiece is one of the most important considerations in determining the strength of a welded structure. Variations in the weld power and the welding heat flux may affect the weld pool formation and ultimately the size of the weld. Therefore, an accurate prediction of the weld size requires a precise analysis of the weld thermal cycle. In this study, a model which can estimate the weld bead geometry and a method for thermal analysis, including the model, are suggested. In order to analyze the weld bead geometry, a mathematical model was developed with transformed coordinates to apply to the horizontal fillet joints. A heat flow analysis was performed with a two dimensional finite element model that was adopted for computing the base metal melting zone. The reliability of the proposed model and the thermal analysis was evaluated through experiments, and the results showed that the proposed model was very effective for predicting the weld bead shape and good correspondence in melting zone of the base metal.

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Temperature Calibration of a Specimen-heating Holder for Transmission Electron Microscopy

  • Kim, Tae-Hoon;Bae, Jee-Hwan;Lee, Jae-Wook;Shin, Keesam;Lee, Joon-Hwan;Kim, Mi-Yang;Yang, Cheol-Woong
    • Applied Microscopy
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    • v.45 no.2
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    • pp.95-100
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    • 2015
  • The in-situ heating transmission electron microscopy experiment allows us to observe the time- and temperature-dependent dynamic processes in nanoscale materials by examining the same specimen. The temperature, which is a major experimental parameter, must be measured accurately during in-situ heating experiments. Therefore, calibrating the thermocouple readout of the heating holder prior to the experiment is essential. The calibration can be performed using reference materials whose phase-transformation (melting, oxidation, reduction, etc.) temperatures are well-established. In this study, the calibration experiment was performed with four reference materials, i.e., pure Sn, Al-95 wt%Zn eutectic alloy, NiO/carbon nanotube composite, and pure Al, and the calibration curve and formula were obtained. The thermocouple readout of the holder used in this study provided a reliable temperature value with a relative error of <4%.