• 제목/요약/키워드: melting study

검색결과 1,652건 처리시간 0.032초

Selective Laser Melting 방식으로 적층가공된 Ti-6Al-4V 합금의 내마모성 특성에 미치는 고온 UNSM 처리 영향에 대한 연구 (Effects of High-temperature UNSM Treatment on Wear Resistance of Ti-6Al-4V Alloy Prepared by Selective Laser Melting)

  • 산성충호;노준석;편영식;아마노프 아웨즈한
    • Tribology and Lubricants
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    • 제36권1호
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    • pp.47-54
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    • 2020
  • In this study, the effects of ultrasonic nanocrystal surface modification (UNSM) treatment at room and high temperatures (RT and HT of 400℃) on friction and wear behavior of Ti-6Al-4V alloy prepared by selective laser melting (SLM) were investigated. The objective of this study is to improve the mechanical properties and frictional behavior of Ti-6Al-4V alloy by UNSM treatment. Dry friction and wear tests were conducted using a ball-on-disk method at RT with a bearing steel as the counter ball. Due to the high HT and UNSM treatment, the surface hardness tended to increase and surface roughness tended to reduce. X-ray diffraction (XRD) analysis showed that nanocrystallization structure and compressive residual stress were formed at the surface layer after UNSM treatment at both RT and HT. After UNSM treatment, it was observed that the wear rate was reduced by about 6% for the specimen treated at RT and a 28% reduction for the specimen treated at HT in comparison with the untreated one. Based on scanning electron microscope (SEM) images showed that the damage caused by fatigue wear occurred in the wear track of the heat-treated specimen, and it is believed to be the cause of the highest wear rate. Mechanical properties and wear resistance of Ti-6Al-4V alloy were improved and prospect of industrial application was confirmed. Further research is still required to improve the characteristics of SLM Ti-6Al-4V alloy to the level of wrought Ti-6Al-4V alloy.

DNA 바코딩과 고해상 융해곡선분석에 기반한 인삼속 식물의 종 판별 (Internal Transcribed Spacer Barcoding DNA Region Coupled with High Resolution Melting Analysis for Authentication of Panax Species)

  • 방경환;김영창;임지영;김장욱;이정우;김동휘;김기홍;조익현
    • 한국약용작물학회지
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    • 제23권6호
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    • pp.439-445
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    • 2015
  • Background : Correct identification of Panax species is important to ensure food quality, safety, authenticity and health for consumers. This paper describes a high resolution melting (HRM) analysis based method using internal transcribed spacer (ITS) and 5.8S ribosomal DNA barcoding regions as target (Bar-HRM) to obtain barcoding information for the major Panax species and to identify the origin of ginseng plant. Methods and Results : A PCR-based approach, Bar-HRM was developed to discriminate among Panax species. In this study, the ITS1, ITS2, and 5.8S rDNA genes were targeted for testing, since these have been identified as suitable genes for use in the identification of Panax species. The HRM analysis generated cluster patterns that were specific and sensitive enough to detect small sequence differences among the tested Panax species. Conclusion : The results of this study show that the HRM curve analysis of the ITS regions and 5.8S rDNA sequences is a simple, quick, and reproducible method. It can simultaneously identify three Panax species and screen for variants. Thus, ITS1HRM and 5.8SHRM primer sets can be used to distinguish among Panax species.

선택적 레이저 용융공정을 이용한 316L 스테인리스강 분말 3차원 조형체의 미세조직 및 경도 연구 (Study on Microstructures and Hardness of STS316L Fabricated by Selective Laser Melting)

  • 신기훈;최준필;김경태;김병기;유지훈
    • 한국분말재료학회지
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    • 제24권3호
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    • pp.210-215
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    • 2017
  • In this study, STS316L powders prepared by gas atomization are used to manufacture bulk structures with dimensions of $10{\times}10{\times}10mm^3$ using selective laser melting (SLM). The microstructures and hardness of the fabricated 316L stainless steel has been investigated with the laser beam overlap varied from 10% to 70%. The microstructures of the fabricated STS316L samples show a decrease in the balling and satellite of powders introducing defect in the bulk samples and the porosity caused by the gap between the molten metal pools disappearing as the overlap ratio increases, whereas a low overlap ratio results in significant balling and a large amount of isolated powders due to the increased gap between the melt pools. Furthermore, the highest value in Vickers hardness is obtained for the sample fabricated by 30% overlapped laser beams. These results show that the overlap ratio of laser beams in the SLM process should be considered as an important process parameter.

용접·용단 작업 중 사고 예방을 위한 제도 개선 연구 (A Study on the Improvement of System to Prevent Accidents during Welding and Melting Operations)

  • 한경수;조규선;김영세;김병직;박주영;박교식
    • 한국가스학회지
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    • 제24권1호
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    • pp.76-81
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    • 2020
  • 최근 가연물이 있는 장소에서 용접·용단 작업 중 불꽃 비산 등으로 인한 화재·폭발사고가 빈발하고 있으며, 이러한 화재사고의 원인은 위험물 제거, 불꽃 비산방지 조치 등 기본적인 안전수칙 미준수가 대부분으로 산업안전보건법의 제도적인 보완이 필요하다. 본 연구에서는 국내 용접·용단 작업 등 화기작업에서의 화재·폭발 사고를 시스템적 관점에서 분석하고 그 결과를 반영하여 화재감시자 배치 확대, 화재위험작업의 사전승인, 화재예방 안전교육 강화 등 제도개선방안을 제안하였다.

Study of properties of $YBa_2Cu_3O_x$ with PbO and $BapbO_3$ additives

  • Soh, Dae-Wha;Fan, Zhanguo
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2004년도 하계학술대회 논문집 Vol.5 No.1
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    • pp.543-546
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    • 2004
  • The melting temperature and critical temperature(Tc) of $YBa_2Cu_3O_x$ with deferent content impurities of PbO and $BaPbO_3$ were studied. When the PbO was used as addition in $YBa_2Cu_3O_x$, although the melting point could be reduced, the superconductivity(the transition width, ${\Delta}T_c$) became poor. From the XRD pattern of the sintered mixture of $YBa_2Cu_3O_x$ and PbO it was known that there is a reaction between $YBa_2Cu_3O_x$ and PbO, and the product is $BaPbO_3$. In the process of the reaction the superconducting phase of $YBa_2Cu_3O_x$ was decreased and in the sample $BaPbO_3$ became the main phase. Therefore the superconductivity was reduced. $BaPbO_3$ was chosen as the impurity for the comparative study. The single phase BaPbO3 was synthesized by the simple way from both mixtures of $BaPbO_3$ and PbO, $BaPbO_3\;and\;PbO_2$. Deferent contents of $BaPbO_3$(10%, 20%, 30%) were added in the $YBa_2Cu_3O_x$. By the phase analysis in the XRD patterns it was proved that there werenot reactions between $YBa_2Cu_3O_x$ and $BaPbO_3$. When $BaPbO_3$ was used as impurity in $YBa_2Cu_3O_x$ the superconductivity was much better than PbO as impurity in $YBa_2Cu_3O_x$. But the melting point of $YBa_2Cu_3O_x$ with $BaPbO_3$ could not be found when the temperature was lower than $1000^{\circ}C$ in the DTA measurement.

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전자빔용해법(溶解法)에 의한 탄탈럼 스크랩의 재활용(再活用) 및 정련(精鍊) (Recycling and refining of tantalum scraps by electron beam melting)

  • 이백규;오정민;최국선;김형석;임재원
    • 자원리싸이클링
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    • 제21권2호
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    • pp.59-65
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    • 2012
  • 본 연구는 전자산업용 탄탈럼 스크랩의 재활용을 위하여 전자빔 용해에 의한 정련 효과를 조사 하였고 정련된 탄탈럼의 극미량 불순물은 글로방전 질량분석기를 이용하여 분석하였다. 탄탈럼 내 대부분의 불순물은 전자빔 용해에 의하여 수 ppm 수준으로 제거되어 초기 탄탈럼 스크랩의 순도인 4 N(99.996%)급에서 5 N(99.9991%)급으로 향상되었다. 탄탈럼 내 금속 불순물의 경우 초기 30 ppm에서 전자빔 반복 용해에 의해 8 ppm으로 감소된 것을 확인하였다. 또한 탄탈럼 내 가스 불순물의 경우 초기 470 ppm에서 전자빔 반복 용해에 의해 50 ppm으로 크게 감소하였다. 본 연구 결과를 통하여 탄탈럼 스크랩에 있어서 전자빔 용해에 의한 재활용 가능성 및 반복 용해에 의한 정련 효과를 확인하였다.

Fatty Acid Profile and Thermal Behavior of Fat-Rich Edible Insect Oils Compared to Commonly Consumed Animal and Plant Oils

  • Kasidate Chantakun;Tanyamon Petcharat;Saowakon Wattanachant;Muhammad Shahrim Bin Ab Karim;Pensiri Kaewthong
    • 한국축산식품학회지
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    • 제44권4호
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    • pp.790-804
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    • 2024
  • This study compared the physicochemical properties of edible insect oils from silkworm (Bombyx mori) pupa (SP), sago palm weevil (Rhynchophorus ferrugineus) larva (PW), and bamboo caterpillar (Omphisa fuscidentalis; BC) to oils from chicken skin (CK), beef back fat (BF), pork back fat (PF), salmon belly (SB), sea bass belly (BB), coconut (C), and peanut (P). The fatty acid profiles and thermal behaviors (crystallization and melting) of the extracted oils were evaluated. PW and BC oils had more saturated fatty acids (SFAs) than CK, PF, SB, BB, and P oils. SP oil had equivalent SFA content to CK and BB oils. Insect oils exhibited similar monounsaturated fatty acid concentrations in all samples, except C oils. PW and BC oils exhibited a higher content of palmitoleic acid than the other oils. SP oils contained polyunsaturated fatty acids similar to those in SB and BB oils, which were higher than those in PW, BC, CK, BF, and PF oils. SP oil also exhibited the highest concentration of α-linolenic acid (C18:3 n-3). Arachidonic acid (0.01-0.02 g/100 g) in all insect oils was lower level compared to CK, BF, PF, SB, and BB oils. SP oil (0.03 g/100 g) exhibited a slightly higher level of eicosapentaenoic acid compared to PW (0.01 g/100 g) and BC (0.01 g/100 g) oils. The insect oils were liquid at ambient temperature, solid below -15℃, and required less energy (∆Hm-max) for melting than other samples. This study indicated that insects, particularly SP, could serve as an alternative source of fat to meet its growing demand.

고질소강의 열간압연시 변형거동 및 압연효과 (Deformation Behavior & Rolling Effect on the Hot Rolling of High Nitrogen Stainless Steel)

  • 김영득;김동권;이종욱;배원병
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2008년도 추계학술대회 논문집
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    • pp.329-332
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    • 2008
  • Nowadays, It is required human body-friendly, good mechanical properties, and economical efficiency material, simultaneously. The material to meet above requirement condition rear up high nitrogen stainless steel(HNS). However, HNS have a lot of problem such as poor workability, hot crack sensitivity. So, It is needed the condition of plastic working to overcome above many problem. In this study, VIM ingot with 100kg was made by pressurized vacuum induction melting. And then, The slab perform for hot rolling was prepared by open-die forging. Hot rolling process was performed by computer simulation according to change of height reduction, rolling temperature, heating numbers, rolling pass and so forth. The results of analysis were investigated between analysis and lab-scale rolling product.

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폐기물 열분해과정에서 발생된 합성가스의 연소 특성 (Combustion Characteristics of Synthesis Gas Generated in Waste Pyrolysis Process)

  • 안용수;황상순;이성호;이협희
    • 한국연소학회:학술대회논문집
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    • 한국연소학회 제26회 KOSCO SYMPOSIUM 논문집
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    • pp.143-150
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    • 2003
  • The synthesis gas generated in waste pyrolysis melting process which consists of pyrolysis of waste and melting process of ash is known to be an alternative fuel. Since the compositopn of synthesis gas is much different from other synthesis gases, the fundamental combustion characteristics are analyzed in this study. The radiation heat heat flux is used to estimate the heat flux from flames made by many combinations of fuel and oxidant supply. The results show that the synthesis gas needs much more amount of oxidant for equivalent heat flux to methane flame and the inverse diffusion flame type for synthesis gas burner is suitable for better radiation heat transfer.

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$TiO_2$ 함유 고굴절솔 유리의 착색에 관한 연구 (Study on the Color of High Index Glass Containing $TiO_2$)

  • 김병훈
    • 한국세라믹학회지
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    • 제17권4호
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    • pp.203-207
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    • 1980
  • The optical absorption of high index glasses of the system TiO2-BaO-B2O3 prepared from the raw materials for an optical waveguide glass has been measured in the near ultraviolet region. The amount of Ti3+ in the glass could be reduced to a level less than 5 ppm by melting a batch added with pure nitric acid, using a fused quartz crucible in an oxygen gas atmosphere. The ultra-pure glass of 10mm thick prepared in such a way did not show any appreciable color even for the one containing 30 mol% TiO2 and having refractive index nD of 1.84 and Abbe's number vD of 28.8. The wavelength of ultraviolet absorptin edge was longer for the glass of higher index and higher dispersdion. The melting of a TiO2 containing glass in a platinum crucible resulted in a coloration of the glass due to the dissolved plutinum from the crucible, which was more intense for the one containing larger amount of TiO2.

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