• Title/Summary/Keyword: melt process

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Melt-spining 공법에 의한 Mg-33.5%Ni 수소 저장 합금 제조 및 수소저장 특성 (Fabricatin and Hydrogen Storage Property of Mg-33.5%Ni Alloy Powder Prepared by Melt-Spining Process)

  • 홍성현;임창동;배종수;나영상
    • 한국수소및신에너지학회논문집
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    • 제18권4호
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    • pp.399-405
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    • 2007
  • The hyper-eutectic Mg-33.5%Ni alloy was rapidly solidified by melt spinning process. The melt-spun Mg-33.5%Ni has amorphous structure and crystallization occurred above $162^{\circ}C$. The hydriding and dehydriding rates of melt-spun Mg-33.5%Ni increased with cycle and high rate of hydrogen storage occurred at 3rd cycle. The maximum hydrogen amount absorbed in melt-spun Mg-33.5%Ni at $300^{\circ}C$ is about 4.5%.

Flux Pinning Enhancement in $(Y_{0.5}Nd_{0.25}Sm_{0.25})Ba_{2}Cu_{3}O_y$ Oxides by Zone Melt Growth Process

  • Kim So-Jung
    • KIEE International Transactions on Electrophysics and Applications
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    • 제5C권6호
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    • pp.251-256
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    • 2005
  • Directionally melt-textured high $T_c\;(Y_{0.5}Nd_{0.25}Sm_{0.25})Ba_{2}Cu_{3}O_y$ [(YNS)-123] superconductor was systematically investigated by the zone melt growth process in air. A sample prepared by this method showed well-textured microstructure, and $(Y_{0.5}Nd_{0.25}Sm_{0.25})_{2}BaCuO_5$[(YNS)211] inclusions were uniformly dispersed in large $(Y_{0.5}Nd_{0.25}Sm_{0.25})Ba_{2}Cu_{3}O_y$ [(YNS)123] matrix. High irreversibility field and magnetization hysteresis loop of the zone melt-textured (YNS)-123 sample exhibited the enhanced flux pinning, compared with $YBa_{2}Cu_{3}O_y$ (Y-123) sample without RE(rare earth). Critical current density of (YNS)-123 sample was $2.5{\times}10^4\;A/cm^2$ at 2 T and 77 K.

보호가스 종류에 따른 고출력 레이저 용접특성 (The Effect of Shielding Gas Composition on High Power Laser Welding Characteristics)

  • 안영남;김철희
    • Journal of Welding and Joining
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    • 제33권4호
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    • pp.17-23
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    • 2015
  • Laser-gas metal arc hybrid welding has been considered as an alternative process of gas metal arc welding for offshore pipe laying. Fiber delivered high power lasers which enable deep penetration welding were recently developed but high power welding characteristics were not fully understood yet. In this study, the influence of shielding gas composition on welding phenomena in high power laser welding was investigated. Bead shapes, melt ejection and dropping were observed after autogenous laser welding with 100% Ar, Ar-20% $CO_2$, Ar-50% $CO_2$, and 100% $CO_2$ shielding gas. Process parameter window was widest with Ar-50% $CO_2$ shielding gas and the penetration was deepest with 100% $CO_2$ shielding gas. The melt dropping was not observed when Ar-50% $CO_2$ or 100% $CO_2$ shielding gas was supplied.

스컬(Skull)법에 의한 큐빅 $ZrO_2$단결정 성장 : 융액의 균질화가 결정성장에 미치는 영향 (Cubic $ZrO_2$ Single Crystals Growth by Skull Method : Effect of Melt Homogenization in Crystallization)

  • 정대식;오근호
    • 한국세라믹학회지
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    • 제27권5호
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    • pp.597-604
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    • 1990
  • In Cubic ZrO2 crystal growth by Skull method, it was examined on effect of homonization on melt as keeping ZrO2(90mol%)-Y2O3(10mol%) melt with 1hr, 2hr, 4hrs, 8hrs, 16hrs, respectively. The optimum homonizing condition in this system was obtained by the examination between quality of grown crystals and soaking time of melt. It was obtained that the lower quality crystal could be produced in the longer holding melt than the optimum soaking time of melt in spite of the supposedly well homonized state, because the melt stability is sensibly dependent on the convective state of melt in skull method (cold crucible process).

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감압 하에서 마그네슘 합금(AM50) 스크랩 용탕의 증발 거동에 관한 연구 (A Study on the Evaporation Behavior of Magnesium Alloy (AM50) Scrap Melt under Reduced Pressure)

  • 위창현;홍성훈;유병돈
    • 대한금속재료학회지
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    • 제48권3호
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    • pp.241-247
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    • 2010
  • In order to develop the vacuum distillation process of magnesium alloy scrap, a fundamental study on the evaporation behavior of magnesium alloy (AM50) scrap melt was carried out. Melt temperature, pressure, reaction time, and initial specific surface area of melt were considered as experimental variables. The evaporation rate of magnesium increased with the increase of melt temperature and initial specific surface area of melt, and with the decrease of the pressure. The activation energy of magnesium evaporation reaction calculated by an Arrhenius plot decreased with the decrease of the pressure and with the increase of the initial specific surface area of melt. An empirical equation was derived for the evaporation rate of magnesium from AM50 alloy melt.

Fabrication of a large grain YBCO bulk superconductor by homo-seeding melt growth method

  • Lee, Hee-Gyoun
    • 한국초전도ㆍ저온공학회논문지
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    • 제24권3호
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    • pp.35-40
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    • 2022
  • To fabricate large grain YBCO bulk superconductors by melt process, Sm123 single crystal with a high melting point are mostly used as seeds. However, it also uses Y123 film deposited on MgO single crystal substrate. This study investigated the growth behavior of the Y123 grain during a melt process when single grain YBCO bulk was used as a seed. Single grain Y123 bulk was grown when the seed size was small. When the seed size was relatively large, multiple grains were grown but the grains were still large. Y123 seed crystal was completely decomposed during high temperature anneal at 1040℃ and new Y123 crystals were nucleated during a slow cooling stage below a peritectic temperature. Thereafter, newly formed Y123 crystals from the seed area are thought to grow into the Y1.8 powder compact. The crystallographic orientations of newly nucleated Y123 grains are independent of the crystallographic orientation of Y123 seed. It is thought that the crystallographic orientation of newly nucleated Y123 crystal can be controlled by using Y211-free Y123 single crystal as a seed of homo-seeding melt growth.

A Study of High Viscosity Melt Front Advancement at the Filling Process of Injection-Compression Mold

  • Park, Gyun-Myoung;Kim, Chung-Kyun
    • 한국윤활학회:학술대회논문집
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    • 한국윤활학회 2002년도 proceedings of the second asia international conference on tribology
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    • pp.333-334
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    • 2002
  • Injection-compression molding parts are many cases with complicated boundary condition which is difficult to analysis of mold characteristics precisely. In this study, the effects of various process parameters such as multi-point gate location, initial charge volume, injection time and pressure have been investigated using finite element method to fomulate the melt front advancement during the mold filling process. A general governing equation for tracking the filling process during injection-compression molding is applied to volume of fluid method. To verify the results of present analysis, they are compared with those of the other paper. The results show a strong effect of processing conditions as a result of variations in the three-dimensional complex geometry model.

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Characterization and Electrical Properties in (YNS)BCO Oxides by Rod-type Seeded Melt Growth Process

  • Kim, So-Jung;Park, Jong-Kuk;Lee, Sang-Gyo
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.243-243
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    • 2007
  • We have studied the electrical properties and microstructure of $(Y_{0.5}Nd_{0.25}Sm_{0.25})Ba_2Cu_3O_y[(YNS)-123]$ Oxides by rod-type seeded melt growth process(RSMG) in air atmosphere. Rod-type $NdBa_2Cu_3O_y${Nd-123) seed crystals made a extrusion process method, were used for achieving the ab-plane alignment having large grains perpendicular to the center of (YNS)-123 samples. The observations using SEM and TEM micrographs of the melt-textured (YNS)-123 samples revealed that the nonsuperconducting $(Y_{0.5}Nd_{0.25}Sm_{0.25})Ba_2Cu_3O_y[(YNS)-211]$ inclusions are uniformly distributed in the superconducting matrix. The microstructure and electrical properties were investigated by XRD, SEM, TEM and DC SQUID magnetometer. The sample showed a sharp superconducting transition at 90 K. The magnetization values of the (YNS)-123 sample exhibited the enhanced electrical properties, compared with $YBa_2Cu_3O_y$(Y-123) sample.

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생체흡수성 HA/PLLA 복합재료의 용융혼련조건이 파괴특성에 미치는 영향 (Effect of Melt-mixing Conditions on Fracture Properties of Bioabsorbable HA/PLLA Composite Materials)

  • 박상대;이덕보
    • 대한기계학회논문집A
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    • 제31권7호
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    • pp.732-738
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    • 2007
  • Effects of melt-mixing conditions on fracture properties of hydroxyapatite filled bioabsorbable poly(L-lactic acid)(HA/PLLA) composites was investigated by measuring the firacture toughness value of HA/PLLA composites prepared under different mixing time and rotor speed. The fracture surface morphology was also examined by profile measurement and scanning electron microscopies. It was found that the fracture toughness of HA/PLLA composites decreases due to decrease of ductile deformation of PLLA matrix and debonding of interfaces with increase of the rotor speed and mixing time. Effect of mixing process on neat PLLA was also assessed, and it was found that the fracture toughness of PLLA decreases due to disappearance of multiple craze formation and increase of defects. Such thermal and shear-stress degradation were found to be the primary mechanisms of the degradation of HA/PLLA composites during melt-mixing process.

재활용 플라스틱 재료의 혼합비가 성형품 수축에 미치는 영향 (The Effect of Mixed Rate of Recycled Resin on the Shrinkage in Molded Parts)

  • 김영수;김인관;강태호
    • 한국기계가공학회지
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    • 제2권3호
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    • pp.62-68
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    • 2003
  • In this study, an experimental work was performed to mold tensile specimens by using the injection molding machine. Melt temperature, mold temperature and the mixed rate of recycled resin were selected as processing parameters for studing the effect of those condition on the shrinkage and weight of molded parts. As a result, the shrinkage was increased with the higher mold and melt temperature and It was more senstive to the change of mold temperature. On the other hand, the weight of molded parts was decreased with the increment of mold and melt temperature.

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