• 한국분말재료학회지
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• 제8권3호
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• pp.210-213
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• 2001

$Si_3N_4$/TiN nano/nano-type composites were successfully fabricated by the combination of a mechano-chemical grinding (MCG) method and a short time sintering process, and their wear resistance was evaluated. Powder mixtures of $\alpha-Si_3N_4$and Ti were prepared using mechano-chemical grinding process and the resulting nanocomposite powder mixtures were consolidated using pulsed electric current sintering (PECS). TEM observation showed that the nano/nano-type composites consisted of homogeneous and very fine matrix grains with the size less than 100 nm. The obtained $Si_3N_4$-based nano/nano-type showed high wear resistance and electric discharge machinability.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.321-322
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• 2006

Nano-structured ceramics, which consist of structural elements with nanometer-size crystallites, are expected to show various unusual properties. We developed the novel nano-structured ceramics which consists of $Si_3N_4$ and TiN and a self-lubricant material. The ceramics was fabricated by powder metallurgy process using mechano-chemical grinding process and short-time sintering process. Each grain size of matrix and the self-lubricant particle was under about 50 nm and a few namometer. It showed high wear resistance and low friction coefficient by controlling of microstructure.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2001년도 하계학술대회 논문집
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• pp.620-623
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• 2001

The peculiarities of using Self-propagating High-temperature Synthesis (SHS) and solid state phase synthesis for production of high temperature superconductor materials are discussed. Oxide superconductors with general formula $ReBa_2$$Cu_3$$O_{7-x}$ (Re= Y, Yb, Sm, Nd) have been made with using barium oxide initial powder instead of traditional barium carbonate. X-ray powder diffraction showed a single phase orthorhombic perovskite structure was produced in all reactions. Phenomena observed during the grinding of the reactant mixture are presented. Mechano-chemical activation - as a pretreatment of the reactant mixture - strongly influences the kinetic parameters, the reaction mechanism, and the composition and structure of the final product.

• 한국분말재료학회지
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• 제16권1호
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• pp.43-49
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• 2009

Titanium carbides are widely used for cutting tools and grinding wheels, because of their superior physical properties such as high melting temperature, high hardness, high wear resistance, good thermal conductivity and excellent thermal shock resistance. The common synthesizing method for the titanium carbide powders is carbo-thermal reduction from the mixtures of titanium oxide($TiO_2$) and carbon black. The purpose of the present research is to fabricate nano TiC powders using titanium salt and titanium hydride by the mechanochemical process(MCP). The initial elements used in this experiment are liquid $TiCl_4$(99.9%), $TiH_2$(99.9%) and active carbon(<$32{\mu}m$, 99.9%). Mg powders were added to the $TiCl_4$ solution in order to induce the reaction with Cl-. The weight ratios of the carbon and Mg powders were theoretically calculated. The TiC and $MgCl_2$ powders were milled in the planetary milling jar for 10 hours. The 40 nm TiC powders were fabricated by wet milling for 4 hours from the $TiCl_4$+C+Mg solution, and 300 nm TiC particles were obtained by using titanium hydride.

• 한국전기전자재료학회논문지
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• 제15권3호
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• pp.275-280
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• 2002

The peculiarities of using Self-propagating High-temperature Synthesis (SHS) and solid-stave chase synthesis for production of high temperature superconductor materials were discussed. Oxide superconductors with general formula of $ReBa_2Cu_3O_{7-x}$ (Re=Y, Sm) haute been made by using barium oxide initial powder instead of traditional barium carbonate. Phenomena observed during the grinding of the reactants mixture are presented. Mechano-chemical activation - as a pre-treatment of the reactants mixture - strongly influences the kinetic parameters, the reaction mechanism, and the composition and structure of the final product.

• 한국해양환경ㆍ에너지학회지
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• 제10권2호
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• pp.102-106
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• 2007

선박 제조에 사용되고 있는 FRP(Fiber-reinforced plastic)를 재활용하기 위한 노력이 지속되고 있는 가운데 보다 친환경적이며 가치를 재창출할 수 있는 방법들이 연구되고 있다. 본 연구진들은 선박용 FRP에 쓰이는 유리섬유의 구조가 그 짜임새의 형태에 따라 로빙층과 매트층으로 구분된다는 사실에 착안하여 FRP를 분쇄하지 않고 층을 분리할 수 있었다. 그 중 로빙층을 적절한 크기로 잘라 장섬유(약 50 mm, 이후 'F섬유')를 만들었다. F섬유의 인장강도 증가와 화학적 내식성 증가는 잔재하는 수지(전체 섬유의 무게비 25% 정도)의 영향인 것으로 보인다. 본 연구에서는 F 섬유의 재활용의 한 방법으로 섬유강화 모르타르를 제조한 결과 2%(v/v)의 F섬유를 포함한 모르타르는 28일 양생 후 휨 강도가 34.6% 증가함을 보였다. 수입 합성섬유 P-54를 사용한 모르타르와 유사한 정도의 휨 강도를 얻을 수 있었다. 이는 F섬유가 골재로 사용이 가능하며 수입품을 대체할 수 있음을 의미한다.