• Title/Summary/Keyword: mechanical properties.

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High Temperature Oxidation Behavior of Fe-14Cr Ferritic Oxide Dispersion Strengthened Steels Manufactured by Mechanical Alloying Process (기계적 합금화 공정으로 제조된 Fe-14Cr Ferritic 산화물 분산 강화(ODS) 합금 강의 고온 산화 거동)

  • Kim, Young-Kyun;Park, Jong-Kwan;Kim, Hwi-Jun;Kong, Man-Sik;Lee, Kee-Ahn
    • Journal of Powder Materials
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    • v.24 no.2
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    • pp.133-140
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    • 2017
  • This study investigates the oxidation properties of Fe-14Cr ferritic oxide-dispersion-strengthened (ODS) steel at various high temperatures (900, 1000, and $1100^{\circ}C$ for 24 h). The initial microstructure shows that no clear structural change occurs even under high-temperature heat treatment, and the average measured grain size is 0.4 and $1.1{\mu}m$ for the as-fabricated and heat-treated specimens, respectively. Y-Ti-O nanoclusters 10-50 nm in size are observed. High-temperature oxidation results show that the weight increases by 0.27 and $0.29mg/cm^2$ for the as-fabricated and heat-treated ($900^{\circ}C$) specimens, and by 0.47 and $0.50mg/cm^2$ for the as-fabricated and heat-treated ($1000^{\circ}C$) specimens, respectively. Further, after 24 h oxidation tests, the weight increases by 56.50 and $100.60mg/cm^2$ for the as-fabricated and heat-treated ($1100^{\circ}C$) specimens, respectively; the latter increase is approximately 100 times higher than that at $1000^{\circ}C$. Observation of the surface after the oxidation test shows that $Cr_2O_3$ is the main oxide on a specimen tested at $1000^{\circ}C$, whereas $Fe_2O_3$ and $Fe_3O_4$ phases also form on a specimen tested at $1100^{\circ}C$, where the weight increases rapidly. The high-temperature oxidation behavior of Fe-14Cr ODS steel is confirmed to be dominated by changes in the $Cr_2O_3$ layer and generation of Fe-based oxides through evaporation.

Permeability Characteristics of Soft Clay using the Piezocone Test and a Laboratory Test (피에조 콘 시험과 실내시험을 이용한 점토지반의 투수특성 연구)

  • Gu, Nam-Sil;Kim, Young-Min;Park, Jae-Hwhan;Jang, Ji-Guen
    • The Journal of Engineering Geology
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    • v.21 no.4
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    • pp.349-359
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    • 2011
  • The consolidation behavior of soft clay is controlled mainly by its compressibility and deformation characteristics. Soil permeability depends on various soil characteristics, including the soil type and anisotropy. The coefficient of permeability of soft clay is determined by using a laboratory test (the Oedometer test) or a piezocone test. The latter test is useful for estimating the permeability characteristics from $c_h$ and $k_h$ by performing an excess pore-pressure dissipation test. This study seeks to validate an existing theoretical formula in applying it to marine clay, and to assess the relation between $k_h/k_c$ and the mechanical properties of soft clay. Piezocone tests and laboratory tests were performed using sediment from the Yellow Sea and from the South Sea near Korea. We compared $k_h/k_v$ values obtained using the piezocone test and using laboratory consolidation tests. The obtained values are similar to the values obtained by Jamiolkowski et al. (M application); therefore, the latter values are recommended to be used as $k_h/k_v$.

Preparation of Borosilicate Foamed Glass Body with Sound Absorption Characteristics by the Recycling Waste Liquid Crystal Display Glass (폐 LCD 유리를 이용한 흡음특성을 갖는 붕규산유리발포체 제조)

  • Lee, Chul-Tae
    • Applied Chemistry for Engineering
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    • v.27 no.6
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    • pp.612-619
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    • 2016
  • In this research, an alumino-borosilicate foamed glass with sound absorption property was prepared using the waste borosilicate glass obtained from the recycling process of waste liquid crystal display (LCD) panel. A 100 g of pulverized waste borosilicate glass with the particle size of under 325 mesh, was mixed with 0.3 g (wt/wt) of graphite, each 1.5 g (wt/wt) of $Na_2CO_3$, $Na_2SO_4$ and $CaCO_3$ as a foaming agent, and 6.0 g (wt/wt) of $H_3BO_3$ and 3.0 g (wt/wt) of $Al_2O_3$ as a pore control agent. Following mixture was under the foaming process for 20 minutes at a foaming temperature of $950^{\circ}C$. The result yielded the foaming agent with 45% of the opened porosity and 0.5-0.7 of the sound absorbing coefficient. This alumino-borosilicate foamed glass with the sound absorption property showed excellent physical and mechanical properties such as density of $0.21g/cm^3$, bending strength of $55N/cm^2$ and compression strength of $298N/cm^2$ which can be ideally used as sound absorption materials with heat-resisting and chemical-resisting property.

The Basic Study of Position Recognition Cow-teats Used Scanning Range Finder (레이저스캔 센서를 이용한 유두위치인식에 관한 기초연구)

  • Kim, Woong
    • Journal of Animal Environmental Science
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    • v.17 no.2
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    • pp.93-100
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    • 2011
  • This study was conducted to verify the applicability of robot milking system through acquisition and analysis of model teat's position information using scanning range finder (SRF). Model teats, same size and shape as real teats, were designed to analyze the properties according to the material, distance error and angle error of the sensor. In addition, 2-dimensional distance information of each teats was obtained at same time with 4 teat models and the result were as follows. 1. In the case of the fingers on the experiment for selection of materials for teat model, the distance error was from 4.3 mm to 1.3 mm, average was 2.8 mm as a minimum record. In the case of rubber material, average distance error was 4.3 mm. So, this material was considered to be a most suitable model. 2. The distance error was maximum at 100 mm distance. The more distance increased, the less error increased up to 300 mm. Then the error increased after 300 mm and decreased again. 3. The maximum angle error of 10.1 mm was measured at $170^{\circ}$, in case of $70^{\circ}$ the error was 0.2 mm as a minimum value. There was no specific tendency to error of angle. 4. In the 2-dimensional location error for 4 teat models, distance error was 3.8 mm as minimum and 7.2 mm as maximum. The angle error was $1.2^{\circ}$ as maximum. All of errors were included within the accuracy of sensor, the robot milking system was considered to be applicable to measure the distance of teats due to the measuring velocity of SRF and the hole size of teat-cup.

Sterilization and Storage of Spices by Irradiation -I. Sterilization of Powdered Hot Pepper Paste- (방사선(放射線)에 의(依)한 향신료(香辛料)의 살균(殺菌) 및 저장(貯藏)에 관(關)한 연구(硏究) -제(第) 1 보(報) : 고추장분말(粉末)의 살균(殺菌)-)

  • Byun, Myung-Woo;Kwon, Joong-Ho;Cho, Han-Ok
    • Korean Journal of Food Science and Technology
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    • v.15 no.4
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    • pp.359-363
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    • 1983
  • Effects of irradiation on the physicochmical properties and its quality of powdered hot pepper paste which was used as a minor matrial of meat products, were investigated during the three months storage. Proximate components of powdered hot pepper paste were not remarkably changed according to the irradiation dose except the slight increase of total and reducing sugars. Capsanthin was insignificantly decreased by the increase of irradiation dose. Color difference according to the irradiation dose could not be distinguished by naked eye but was slightly changed by mechanical measurement. Total bacteria and E.coli were sterilized by the irradiation of 10kGy and 5kGy, respectively and no microorganisms were grown up after three months storage at $37^{\circ}C$. Sterilization of powered hot pepper paste by irradiation was expected to be superior to the traditional methods in the wholsomeness and sterilizing efficacy.

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Optimization of the Preparation of Domestics Wheat Cookies by Addition of Red Radish (Raphanus sativus L.) Sprout Powder (어린잎 적양무가루를 첨가한 우리밀 쿠키의 제조조건 최적화)

  • Cheon, Chun Jin;Kim, Young-Ho;Oh, Jong Chul;Kim, Jin Kon;Yu, Hyeon Hee
    • Korean Journal of Food Science and Technology
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    • v.45 no.4
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    • pp.441-450
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    • 2013
  • The purpose of this study was optimization of the conditions for mixing different amounts of red radish (Raphanus sativus L.) sprout powder, butter, and sugar when baking domestic wheat cookies prepared using red radish sprout powder. Response surface methodology, with a central composite design comprising 5 levels and 3 variables, was used to identify the best possible combination of amounts of red radish sprout powder ($X_1$), butter ($X_2$), and sugar ($X_3$). The physical and mechanical properties of each of the 20 samples analyzed, including color L (p<0.001), color a (p<0.01), color b (p<0.001), spread ratio (p<0.001), and hardness (p<0.01), differed significantly. The results of sensory evaluations, including color (p<0.001), appearance (p<0.001), texture (p<0.001), flavor (p<0.01), taste (p<0.001), and overall quality (p<0.001) also differed significantly among the samples. The optimal compositional ratios were 5.15 g for the red radish sprout powder, 64.84 g for the butter, and 47.18 g for the sugar.

Study on the Superplasticity in Al-Li Alloy Systems (AI-Li계 합금의 초소성에 관한 연구)

  • Jin, Y.C.;Kook, J.S.;Kim, Y.S.;Hong, E.S.;Lee, M.S.;Lee, M.H.;Yoo, C.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.5 no.1
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    • pp.41-49
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    • 1992
  • The effects of alloying elements on the superplastic properties of Al-Li based alloys had been investigated. The intermediate thermo-mechanical treated (ITMT) Al-2.0wt%Li, Al-2.0wt%Li-1.0wt%Mg, Al-2.0wt%Li-0.12wt%Zr and Al-2.0wt%Li-1.2wt%Cu-1.0wt%Mg-0.12wt%Zr alloys were tested in tension at various temperature (400, 450, 500 and $550^{\circ}C$) and strain rate($6.7{\times}10^{-3}$, $1.0{\times}10^{-2}$, $1.6{\times}10^{-2}$ and $5.0{\times}10^{-2}/sec$). The results were as follows : The superplasticity in binary, ternary and pentanary alloys appeared at 500 to $550^{\circ}C$, and good strain rate for superplasticity. $1.6{\times}10^{-2}/sec{\sim}1.0{\times}10^{-2}/sec$ for a binary alloy and $1.0{\times}10^{-2}/sec{\sim}6.7{\times}10^{-3}/sec$ for ternary and pentanary alloys. A Zr-added ternary alloy had best value of elongation (730%) in four alloys at $550^{\circ}C$ of tension temperature and $1.0{\times}10^{-2}/sec$ of strain rate. The strain rate was greatly dependent on tension temperature and true strain rate was more than 1.0 at all test temperature and strain rate. In binary and Mg-added teranry alloys. the necks were slightly formed and their fracture surface had lips shape, but Zr-added ternary and pentanary alloy fractured along the grain boundary without necking. Their dislocations moved to grain boundary during superplasticity deformation and arranged perpendicular to grain boundary. Super plastic deformation was made by grain boundary slip of dislocation slip creep and model of core and mantle.

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A Study on the Property Changes of Rigid Polyurethane Foams by Nucleating Effects of PFA and MWCNT (PFA 및 MWCNT의 기핵효과에 의한 경질 폴리우레탄 폼의 물성 변화에 대한 연구)

  • Ahn, WonSool
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.16 no.4
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    • pp.2945-2950
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    • 2015
  • While perfluoroalkane (PFA), a liquid state nucleating agent for a rigid polyurethane foam (RPUF) to enhance the thermal insulation property, has the excellent nucleating characteristics, it is very expensive as well as environmentally harmful due to the fluoride compound. Many researches, therefore, have been performed to develop the alternative nucleating agents to replace PFA. In the present work, a multi-wall carbon nanotube (MWCNT) was used as a sloid state nucleating agent, and thereby the effects on the property changes of the RPUF were carried out. Average cell size decreased from 165.6 for base RPUF to $162.9{\mu}m$ and cell uniformity was also enhanced, showing the standard cell-size deviation of 45.6 and 35.2, respectively. While k-factor of base PUF was $0.01763kcal/m.hr.^{\circ}C$, that of the sample with 0.01 phr MWCNT showed 1.02% reduced value of $0.01745kcal/m.hr.^{\circ}C$. Though the compressive yield stress is nearly the same as $0.030{\times}105Pa$ for the both samples, initial modulus of the sample with 0.01 phr MWCNT was higher than that of base sample. it was considered as the results that small amount of MWCNT could play a sufficient role as the effective nucleating agent for RPUF, showing that an echo-friendly RPUF with reduced-cost could be fabricated, which has an enhanced thermal and mechanical properties.

Surface Morphology of PEO-treated Ti-6Al-4V Alloy after Anodic Titanium Oxide Treatment (ATO 처리후, 플라즈마 전해 산화 처리된 Ti-6Al-4V 합금의 표면 형태)

  • Kim, Seung-Pyo;Choe, Han-Cheol
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2018.06a
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    • pp.75-75
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    • 2018
  • Commercially pure titanium (CP-Ti) and Ti-6Al-4V alloys have been widely used in implant materials such as dental and orthopedic implants due to their corrosion resistance, biocompatibility, and good mechanical properties. However, surface modification of titanium and titanium alloys is necessary to improve osseointegration between implant surface and bone. Especially, when titanium oxide nanotubes are formed on the surface of titanium alloy, cell adhesion is greatly improved. In addition, plasma electrolytic oxide (PEO) coatings have a good safety for osseointegration and can easily and quickly form coatings of uniform thickness with various pore sizes. Recently, the effects of bone element such as magnesium, zinc, strontium, silicon, and manganese for bone regeneration are researching in dental implant field. The purpose of this study was researched on the surface morphology of PEO-treated Ti-6Al-4V alloy after anodic titanium oxide treatmentusing various instruments. Ti-6Al-4V ELI disks were used as specimens for nanotube formation and PEO-treatment. The solution for the nanotube formation experiment was 1 M $H_3PO_4$ + 0.8 wt. % NaF electrolyte was used. The applied potential was 30V for 1 hours. The PEO treatment was performed after removing the nanotubes by ultrasonics for 10 minutes. The PEO treatment after removal of the nanotubes was carried out in the $Ca(CH_3)_2{\cdot}H_2O+(CH_3COO)_2Mg{\cdot}4H_2O+Mn(CH_3COO)_2{\cdot}4H_2O+Zn(CH_3CO_2)_2Zn{\cdot}2H_2O+Sr(CH_2COO)_2{\cdot}0.5H_2O+C_3H_7CaO_6P$ and $Na_2SiO_3{\cdot}9H_2O$ electrolytes. And the PEO-treatment time and potential were 3 minutes at 280V. The morphology changes of the coatings on Ti-6Al-4V alloy surface were observed using FE-SEM, EDS, XRD, AFM, and scratch tester. The morphology of PEO-treated surface in 5 ion coating solution after nanotube removal showed formation or nano-sized mesh and micro-sized pores.

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Evaluation of Properties of Artificial Soil Aggregate Based on Ground Granulated Blast-Furnace Slag According to Unit Binder Content (단위결합재량에 따른 고로슬래그 기반 육성용 인공토양골재의 특성평가)

  • Mun, Ju-Hyun;Sim, Jae-Il;Yun, In-Gu
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.20 no.5
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    • pp.85-92
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    • 2016
  • The eight mixes and artificial soil aggregates were prepared for evaluating the practical application of lightweight foamed concrete as soil aggregates. The main parameter was unit binder content ranged between from 100 to $800kg/m^3$. In lightweight foamed concrete, flow, slurry and dried density, and compressive strength at different ages were measured. In Artificial soil aggregates crushed from lightweight foamed concrete, particle size distribution, pH, coefficient of permeability, cation exchange capacity(CEC), and ratio of carbon to nitrogen(ratio of C/N), were measured. The test results showed that flow, slurry and dried density, and compressive strength at different ages of lightweight foamed concrete increased with the increasing of unit binder content. Compressive strength at age of 28, of lightweight foamed concrete with unit binder of more than $500kg/m^3$, was more than 4 MPa. The ammonium phosphate immersion time of more than age of 3, was effective to decrease pH of artificial soil aggregates. In addition, artificial soil aggregates was evaluated as high class in terms of cation exchange capacity(CEC), while satisfied with value of ratio of carbon to nitrogen(ratio of C/N) recommended by landscape specification.