• Title/Summary/Keyword: material tests

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Contact fatigue and strength degradation in dental ceramics (치아용 세라믹스에서의 접촉피로 및 강도저하)

  • 정연길;이수영;최성철
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.5
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    • pp.527-533
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    • 1999
  • Hertzian indentation tests with spherical indenters in water were conducted to examine the contact fatigue in three dental ceramics, such as feldspathic porcelain, micaceous glass-ceramic (MGC) and glass-infiltrated alumina, which was used as dental restorations, and evaluated the effect of contact damage on strength. Initial damage was dependent of microstructure, showing cone cracks of brittle behavior in the feldspathic porcelain and deformation of quasi-plastic behavior in the MGC, with an intermediate case in the glass-infiltrated alumina. However, as increasing the number of cyclic loading (n=1~n =$10^6$)all materials showed an abrupt strength degradation, at which fracture was originated from damage in the contact fatigue. There were two strength degradation with increasing the number of cyclic loading in specific loads (200N, 500N, 1000N):first was from the cone cracks, and second was from the radial cracks created by cyclic loading. The radial cracks, once formed, led to rapid degradation in strength properties, Finally the material was failed at the high number of cyclic loading. Strength degradation with indentation load at fixed number of cyclic loading indicated that the feldspathic porcelain should be highly damage tolerant to the contact fatigue.

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A Study on the Evaluation of Shear Strength of Geotextile & Geomembrane by Traffic Load in Landfill Final Cover System (폐기물 매립지 최종복토층에서 교통하중에 의한 부직포 및 Geomembrane의 전단강도의 변화에 대한 사례연구)

  • Park, Sang-Hyun;Lee, Jai-Young;Choi, Mun-Young
    • Journal of the Korean Geosynthetics Society
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    • v.1 no.1
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    • pp.3-11
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    • 2002
  • The Geotextiles have been used for the protection of Geomembrane and the prevention of clogging phenomenon; however, the material can be easily damaged by construction equipments. It generally recommended to use at least $500g/m^2$ of Geotextile in Korea landfill, but few researcher were performed about the damage of Geotextile. Therefore, we intended to evaluate the potential damage of Geotextile by the traffic load simulating the final cover system in a field scale. Tensile strength and strain were appraised to understand the degree of damaged Geotextile. The tests were conducted under the condition of cross direction of Geotextile. Four different weight of Geotextile was used for the evaluation $500g/m^2$, $700g/m^2$, $1,000g/m^2$ and $1,500g/m^2$. The initial strain of $500g/m^2$ of Geotextile showed 50% that did not meet the standard 60%. The strain of $700g/m^2$ of Geotextile was below the standard after the traffic load test; however, the others met the requirement in the test. In conclusion, the weight of Geotextile used in landfill to protect the Geomembrane should be at least $700g/m^2$ in a view of strain requirement. We expect this study provides fundamental information for the construction of Geotextile in landfill.

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Hydraulic Conductivity and Microscopic Analysis of Fly Ash Liner (플라이애쉬 혼합차수재의 투수특성과 미세구조 분석)

  • Jeong, Mun-Gyeong;Seo, Gyeong-Won;Lee, Yong-Su
    • Geotechnical Engineering
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    • v.14 no.1
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    • pp.109-126
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    • 1998
  • The use of fly ash as a contaminant barrier material was studied. Mixing ratio of fly ash to bentonite to meet the requirements for landfill liners was determined. The hydraulic behavior exhibited by the fly ash-bentonite liner and the effects of CaO were investigated through hydraulic conductivity tests under various conditions and microscopic analyses including XRD, SEM, helium porosimetry, and image analysis. The hydraulic conductivity of compacted fly ash decreased with the addition of bentonite, which was due mainly to the expanding of bentonite and partly to the filling of voids by chemical reaction products among constituents of the artificial liner. Because of insufficient CaO content, and rich in content but low-reactive $SiO_2$ contained in the fly ashes used, pozzolanic reaction and resulting effects in the artificial liner were not significant. The reactions among constituting materials and their resulting effects on hydraulic conductivity were controlled not by the apparent amounts of each constituent, but by reaction activities of the materials in the artificial liner.

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An Experimental Study for Substitutability of Sand Mat with Fiber Mat (Fiber Mat의 Sand Mat 대체가능성평가를 위한 실험적 연구)

  • Lee Song;Jeong Yong-Eun
    • Journal of the Korean Geotechnical Society
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    • v.21 no.5
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    • pp.225-230
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    • 2005
  • At present, there are several problems related with sand mat which is used as a way to accelerate consolidation settlement, to act like an underground drainage layer and to increase trafficability simultaneously. First of all, the unbalance of the demand and supply of sand is one of the biggest problems, which causes not only price rise but also delay of the term of the total construction work. Secondly, the damage of ecosystem and scenery is triggered by thoughtless sand dredging or mining. So, the need that sand mat should be replaced with a new environmentally friendly material has been increased. Fiber mat may be one of the proper materials that suits the need. Therefore, we intended to compare the drainage properties of sand mat with those of fiber mat by experimental model tests. On the basis of the test results, fiber mat took shorter period of consolidation than sand mat and the amount of settlement in the farmer showed a little bit bigger than in the latter. As a conclusion, the substitutability of sand mat with fiber mat could be placed highly in view of drainage efficiency. Furthermore, when fiber mat is used, it has an advantage that spoiled soil of the construction site or nearby site can be used for the purpose of increasing trafficability in addition to a role of drainage layer.

A Study of Hydrogen Embrittlement on a Material of CNG Storage Tank (CNG 저장용기 재료의 수소취성에 관한 연구)

  • Han, J.O.;Lee, Y.C.;Lee, J.S.;Chae, J.M.;Hong, S.H.
    • Journal of the Korean Institute of Gas
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    • v.15 no.2
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    • pp.9-14
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    • 2011
  • A set of test was conducted on a SA-372 steel for CNG storage tank to study the effect of hydrogen embrittlement. Tensile tests were carried out several conditions such as CNG, HCNG and H2 gas environment including air and Ar under the 35 MPa. Also, the test speed was set at 4*10^-4/s and 4*10^-5/s respectively. To maintain the high pressure for environmental gas during test process, we chose MTS which was installed autoclave. Test results showed that tensile stress, elongation rate and cross sectional contraction under Ar and CNG charging condition were similar to that of reference of air. And there was little bit change with test speed variations. However, hydrogen added conditions such as HCNG and H2 were revealed noticeable change in elongation rate and cross sectional contraction. Tensile stress was still uniform for all conditions. From the results, the effect of hydrogen embrittlement was confirmed on the hydrogen enriched conditions. Also its effect was showed more strong with much hydrogen concentration and slower test speed.

Catalytic Decomposition of SF6 by Hydrolysis over γ - Al2O3 Supported Metal Oxide Catalysts (금속산화물이 담지된 γ - Al2O3 촉매상에서 가수분해에 의한 SF6의 촉매분해)

  • Park, Hyeon-Gyu;Park, No-Kuk;Lee, Tae-Jin;Chang, Won-Chul;Kwon, Won-Tae
    • Clean Technology
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    • v.18 no.1
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    • pp.83-88
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    • 2012
  • In order to improve the stability of ${\gamma}-Al_2O_3$ on hydrolysis of $SF_6$, the catalytic promoters were investigated in this study. The crystal phase of ${\gamma}-Al_2O_3$ is transformed to their ${\alpha}$-phase during hydrolysis of $SF_6$. Various metal oxides were applied as the promoter material that is Ga, Mg, and Zn and the promoter of 1, 5, and 10 wt% was impregnated over ${\gamma}-Al_2O_3$ by the impregnation method. Specially, it were confirmed in the catalytic activity tests and XRD analysis that ZnO/${\gamma}-Al_2O_3$ catalyst had the high activity for decomposition of $SF_6$ by catalytic hydrolysis and the crystal phase of ZnO promoted ${\gamma}-Al_2O_3$ was not transformed. From these results, it could be known that the stability of ${\gamma}-Al_2O_3$ is enhanced with the catalytic promotion of ZnO impregnated over the surface of catalyst.

The Change in Interfacial and Mechanical Properties for Glass Fiber/p-DCPD Composites with Degree of Ruthenium Catalyst Activation (루테늄촉매 활성정도에 따른 유리섬유/폴리다이사이클로펜타다이엔 복합재료의 기계 및 계면물성 변화)

  • Shin, Pyeong-Su;Kim, Jong-Hyun;Baek, Yeong-Min;Park, Ha-Seung;Kwon, Dong-Jun;Park, Joung-Man
    • Journal of Adhesion and Interface
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    • v.19 no.1
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    • pp.13-18
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    • 2018
  • At ruthenium (Ru) catalyst was exposed from the atmosphere, the degree of catalyst activation decreased. The change of catalyst activity with the number of days of exposure to air for the Ru catalyst was confirmed using the surface tension method quantitatively. Mechanical properties and surfactant change after polymerization by DCPD using Ru catalyst for each air exposure day was evaluated. The Ru catalyst mixed with a dilution agent was exposed in the air and color was monitored for each day. Surface tension was measured using Wilhelmy and PTFE and associated with different catalyst activities. Heat was measured in real time during polymerizing DCPD with Ru catalyst. After polymerization, tensile strength was measured for p-DCPD and the change of material property was measured. Interfacial properties were also evaluated via microdroplet pull-out tests between glass fiber and p-DCPD. The surface tension was stable until the 4 days (33 dyne/cm) whereas the surface energy increased at the 10 days (34 dyne/cm), which could be correlated with oxidation of the catalyst. Tensile property and interfacial shear strength (IFSS) was also stable until the 4 days (tensile strength: 38 MPa and IFSS: 26 MPa) whereas the mechanical property decrease at 10 days (tensile strength: 15 MPa and IFSS: 3 MPa) dramatically.

Changes of Characteristics in Red Pepper by Various Freezing and Thawing Methods (홍고추의 저장온도 및 해동조건에 따른 물리화학적 특성 변화)

  • Lee, Hye-Eun;Lim, Chai-Il;Do, Kyung-Ran
    • Food Science and Preservation
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    • v.14 no.3
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    • pp.227-232
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    • 2007
  • The development of an effective long-term storage protocol for harvested fresh pepper is urgently required to increase the market for pepper products. The protocol must minimize quality loss, so that the product may be used either as a spice or as a raw material for processed pepper products, both in the home and in food processing plants. We investigated the optimum size of pepper fruits, freezing temperatures, storage periods, and thawing methods, to establish an optimum storage protocol. This study was conducted not only to develop freezing and thawing methods for long term storage of harvested red pepper, but also to develop processed pepper products utilizing the stored pepper. We aimed to expand the pepper products market and to increase the incomes of pepper growers. Whole red pepper, sliced red pepper, and crushed red pepper were frozen and stored at $-5^{\circ}C,\;-20^{\circ}C,\;or\;-40^{\circ}C$. The soluble solid content and the vitamin C level showed maximal stability at $-40^{\circ}C$, although total free sugars decreased on storage at all temperatures tested. Such Changes were more marked at $-5^{\circ}C$ than at the other(lower) temperature tested. The vitamin C content of whole red pepper was higher than that of sliced red pepper or crushed red pepper. Room-temperature thawing resulted in twice the drip loss seen on low temperature($5^{\circ}C$) thawing or microwave oven thawing. Brown discoloration was a serious problem with room temperature thawing. Total free sugars were higher in samples thawed at low temperature or in the microwave oven, compared to the level seen after room-temperature thawing. pepper samples thawed at low temperature scored higher in sensory tests than samples thawed at room temperature.

Dehydration and Drying Characteristics of Gingers Using Dehydrating Agent by Dextrose Equivalent and Molecular Weight Condition (포도당 당량과 분자량 조건별 탈수제를 적용한 생강의 탈수와 건조 특성)

  • Lee, Hyun-Seok;Kwon, Ki-Hyun;Kim, Byeong-Sam;Jeong, Jin-Woong;Kim, Jong-Hoon;Sung, Jung-Min
    • Food Science and Preservation
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    • v.17 no.6
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    • pp.763-769
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    • 2010
  • We examined variations in ginger dehydration and recovery rate upon use of dextrose of different equivalence values. The dehydration rate varied with dextrose equivalent and the dehydration rate increased as the equivalence value increased. Both dehydration and recovery rates varied with dextrose molecular weight. Moisture content was lowest in samples prepared by freeze-drying, and neither dextrose equivalent nor molecular weight affected moisture level. Upon color analysis, ginger dried using dextrose varying in equivalence and molecular weight was similar in color to the original material, unlike ginger dried by other methods. Hot-air-dried ginger scored lowest in all sensory tests, compared with ginger prepared by molecular press dehydration using dextrose varying in equivalence and molecular weight. With respect to the appearance of ginger, freeze-dried samples were optimal, but molecular press dehydration yielded samples that scored best upon overall evaluation. When all quality evaluation items were taken together, molecular press dehydration resulted in a better quality product than the older hot-air or freeze-drying methods.

Citrus platymamma inhibits the expression of pro-inflammatory cytokines, inducible nitric oxide synthase, and cyclooxygenase-2 in RAW264.7 macrophage (RAW264.7 대식세포에서 Citrus platymamma의 iNOS, COX-2, 염증성 사이토카인 발현 억제 효과)

  • Kim, Sang Suk;Park, Kyung Jin;An, Hyun Joo;Choi, Young Hun
    • Food Science and Preservation
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    • v.23 no.7
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    • pp.1026-1032
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    • 2016
  • Citrus platymamma hort. ex Tanaka is widely used in traditional Korean medicine because of its medicinal benefits including an anti-inflammatory effect. This study aimed to evaluate changes in the flavonoid content and anti-inflammatory activities of C. platymamma during its harvest period. Fruit peel samples were obtained between September 2015 and February 2016. The results indicate that C. platymamma peel extract (CPE) was an effective inhibitor of lipopolysaccharide (LPS)-induced NO production in RAW264.7 cells. The inhibitory effects of CPE at $100{\mu}g/mL$ concentration included dose-dependent decreases in the expression of iNOS and COX-2 proteins. In addition, CPE decreased the expression of pro-inflammatory cytokines TNF-${\alpha}$, IL-$1{\beta}$, and IL-6. The highest anti-inflammatory activity and flavonoid content were observed in CPE of C. platymamma peel harvested during the immature fruit period in September. Further, to assess the suitability of CPE for cosmetic use, we performed MTT assays using HaCaT keratinocytes and observed that CPE did not exhibit any cytotoxicity. To test the potential application of CPE as a cosmetic material, we also performed primary skin irritation tests on normal skin of 30 volunteers and no adverse reactions were observed. The results of this study indicate that CPE may be considered as an anti-inflammatory candidate for inclusion in cosmetic materials.