• Journal of the Korean Society for Precision Engineering
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• v.25 no.4
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• pp.61-68
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• 2008

Of the seven base units of the international system of units, only the kilogram is still defined in terms of a material artifact. One of the experimental approaches opening the way to a new definition of the kilogram is the watt balance To improve the performance of the NPL watt balance, we need to quantify and reduce hysteresis effects in the balance knives. In this paper, we discuss the mechanical characteristics of the knife edges used in the NPL watt balance. The hysteresis mechanism is analyzed using the finite element method. It is found that the cause of hysteresis is not normal stress but shear, and the deformation of the flat, rather than the knife, is an important factor in the hysteresis mechanism. The study presented here, using finite element analysis, suggests that parameters such as material property, tip radius and knife straightness can be more important than others, such as friction coefficient, tip angle, etc.

• Journal of the Korean institute of surface engineering
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• v.35 no.2
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• pp.129-137
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• 2002

The purpose of solderability assessment is to predict the effectiveness of soldering process. It is important for companies pursuing zero defects manufacturing because poor solderability is the major cause of two third of soldering failures. The most versatile solderability method is wetting balance method. However, there exist so many indices for wettability in the wetting balance test e.g. time to reach 2/3 values of maximum wetting force, tine to reach zero wetting force, maximum withdrawal force. In this study, three solderability assessment methods, which were the maximum withdrawal force, the wetting balance and the dynamic contact angle (DCA), were evaluated by comparing each other. The wetting balance technique measures the solderability by recording the forces exerted from the specimen after being dipped into the molten solder. Then the force at equilibrium state can be used to calculate a contact angle, which is known as static contact angles. The DCA measures contact angles occurred during advancing and withdrawing of the specimen and the contact angles are known as dynamic contact angles. The maximum withdrawal force uses the maximum force during withdrawal movement and then a contact angle can be calculated. In this study, the maximum withdrawal force method was found to be an objective index for measuring the solderability and the experiment results indicated good agreement between the maximum withdrawal force and the wetting balance method.

• Steel and Composite Structures
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• v.44 no.1
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• pp.91-104
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• 2022

The purpose of the present work is to study the parametric nonlinear vibration behavior of three layered symmetric laminated plate. In the analytical formulation; both normal and shear deformations are considered in the core layer by means of the refined higher-order zig-zag theory. Harmonic balance method in conjunction with Galerkin procedure is adopted for simply supported laminate plate, to obtain its natural and damping properties. For these aims, a set of complex amplitude equations governed by complex parameters are written accounting for the geometric nonlinearity and viscoelastic damping factor. The frequency response curves are presented and discussed by varying the material and geometric properties of the core layer.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.22 no.3
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• pp.483-492
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• 1998

An inverse analysis been applied to obtain the flow stress of the material. In this method, a ring-shaped specimen is compressed between two flat tools. This procedure employs, as the object function of inverse analysis, the balance of measured loads and reaction forces calculated by using rigid-plastic finite element method. The balance is explicit scalar function of flow stress which is a function of some unknown constants. For minimizing the balance, Newton-Raphon scheme is used. The friction factor, m, between flat tools and the specimen is determined by using friction area-divided method. The proposed method allows an accurate identification by avoiding the usual assumptions made in order to convert experimental measures into stress-strain relation. In this paper, the proposed method is numerically tested. A commercial pure aluminum was selected, as an example, to apply the method and the results are compared with stress-strain relation obtained by experiments.

• Nuclear Engineering and Technology
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• v.48 no.3
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• pp.733-743
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• 2016

The purpose of this study is to present a rational depreciation method for a pyroprocess cost calculation. Toward this end, the so-called advanced decelerated depreciation method (ADDM) was developed that complements the limitations of the existing depreciation methods such as the straight-line method and fixed percentage of declining-balance method. ADDM was used to show the trend of the direct material cost and direct labor cost compared to the straight-line or fixed percentage of the declining-balance methods that are often used today. As a result, it was demonstrated that the depreciation cost of the ADDM, which assumed a pyroprocess facility's life period to be 40 years with a deceleration rate of 5%, takes up 4.14% and 27.74% of the pyroprocess unit cost ($781/kg heavy metal) in the $1^{st}$ and final years, respectively. In other words, it was found that the ADDM can cost the pyroprocess facility's capital investment rationally every year. Finally, ADDM's validity was verified by confirming that the sum of the depreciation cost by year, and the sum of the purchasing cost of the building and equipment, are the same.

• Macromolecular Research
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• v.11 no.6
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• pp.399-409
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• 2003

The first esterification reactor in the continuous polymerization of poly(ethylene terephthalate) has been analyzed by solving the material balances for the two-phase system with respect to the solubility of terephthalic acid. The Newton-Raphson method was used to solve the material balance equations instead of the Simplex method that is frequently used for finding a minimum point of a residual rather than a solution of an equation. A solution for the material balance equations, with the constraint of non-zero liquid phase fraction, could not be obtained with the solubility data of Yamada et al., but could be obtained with solubilities over a minimum value that is larger than their data. Thus, the solubility data of Yamada et al. are considered to be too small. On the other hand, the solubility data of Baranova and Kremer are so large that they gave a solution with the liquid phase only. Based on our results, several typical solubility curves satisfying the constraint of a non-zero liquid phase fraction are suggested in this study; we studied the reaction characteristics of the system using these curves. A higher temperature and a lower pressure are preferred for reducing the content of diethylene glycol.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.7 s.178
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• pp.1753-1762
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• 2000

An inverse method is presented to obtain material's flow properties by using small punch test. This procedure employs, as the objective function of inverse analysis, the balance of measured load-di splacement response and calculated one during deformation. In order to guarantee convergence to global minimum, simulated annealing method was adopted to optimize the current objective function. In addition, artificial neural network was used to predict the load-displacement response under given material parameters which is the most time consuming and limits applications of global optimization methods to these kinds of problems. By implementing the simulated annealing for optimization along with calculating load-displacement curve by neural network, material parameters were identified irrespective of initial values within very short time for simulated test data. We also tested the present method for error-containing experimental data and showed that the flow properties of material were well predicted.

• Analytical Science and Technology
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• v.32 no.6
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• pp.225-232
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• 2019

Traceability establishment in chemical measurements is a like a linkage established through an unbroken chain from the measured results to the international system (SI) of units. The primary process for traceability establishment is the purity assignment of a target material to be measured. In this study, we studied the purity assignment of 17α-hydroxyprogesterone (17-OHP). The presence of 17-OHP is indicative of congenital adrenal hyperplasia (CAH) and it builds up due to the deficiency of 21-hydroxylase and 11β-hydroxylase enzyme in the human blood. The purity assignment of 17-OHP was performed by the mass balance method, in which the impurities are categorized into four classes: total related structural impurities, water, residual organic solvents, and nonvolatiles/inorganics. The total related structural impurities were characterized by HPLC-UV; water content was determined by Karl-Fisher coulometer; and the total residual solvents and nonvolatiles/inorganics were determined by TGA. The purity of 17-OHP from a commercial manufacturer was calculated as 993.30 mg/g, and the expanded uncertainty was 0.58 mg/g. The proposed method was validated by uncertainty evaluation and comparing with the actual value of purity.

• Analytical Science and Technology
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• v.30 no.5
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• pp.226-233
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• 2017

In general, quantitative chemical analysis in various areas including food, the environment, in vitro diagnostics, etc., requires traceability in order to increase the reliability of the measurements. Measurement traceability is a property of an unbroken chain of comparisons relating an instrument's measurements to SI units. Purity analysis is the first process for establishing traceability to SI units in chemical measurements. The purpose of this study is to develop and validate a method of purity assignment for establishing the traceability of $17{\beta}$-estradiol measurements in an in vitro diagnostics field. The establishment of this method is very important as it can be applied to the development of CRM and to the analysis of the purity of other hormones. The method of assignment of the purity of $17{\beta}$-estradiol was developed using the mass balance method and was validated through participation in an International comparison. In the mass balance method, impurities are categorized into four classes as follows: total related structure impurities, water, residual organic solvents, and nonvolatiles/inorganics. In this study, total related structure impurities were characterized by a gas chromatography-flame ionization detector (GC-FID) and a high-performance liquid chromatography-ultraviolet (HPLC-UV) detector, water content was determined by a Karl-Fisher coulometer, and total residual solvents and nonvolatiles/inorganics were checked simultaneously by thermogravimetric analysis (TGA). The purity of the $17{\beta}$-estradiol was 985.6 mg/g and the expanded uncertainty was 2.1 mg/g at 95% confidence. The developed method can be applied to the development of certified reference materials, which play a critical role in traceability.

• Proceedings of the KSR Conference
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• 2009.05a
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• pp.73-76
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• 2009

LCA is nowadays getting popular as a tool to assess the environmental impacts. We can assess the environmental impacts of products and also compare the environmental performance between products with LCA. Furthermore, the LCA results can be used for designing eco-friendly products. But LCA needs an enormous amount of data collection, calculations of energy and material balance. which required to spend pretty much time and cost. However, If we use Input-Output Analysis, There is a lot of advantages that we can save time and cost to calculate and also analyze energy-material balance more comprehensively. Therefore, we implemented the fundamental research of the environmental impact assessment on railway system using life cycle inventory analysis and Input-Output Analysis method.