• Bulletin of the Korean Chemical Society
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• v.34 no.6
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• pp.1703-1707
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• 2013

A fast and simple sampling and sample preparation device, (NTD) has been developed and applied to sample and analyze volatile components from ground coffee beans. Coffee fragrances and other volatile organic compounds (VOCs) were sampled by the NTD and then analyzed by gas chromatograph-mass spectrometry (GC/MS). Divinylbenzene (DVB) particles (80/100 mesh size) were the sorbent bed of the NTD. More than 150 volatile components were first identified based on the database of the mass library and then finally 30 fragrances including caffeine were further confirmed by comparing experimental retention indices (i.e. Kovat index) with literature retention indices. Total sampling time was 10 minutes and no extra solvent extraction and/or reconstitution step need. Straight n-alkanes (C6-C20) were used as retention index probes for the calculation of experimental retention indices. In addition, this report suggests that an empty needle can be an alternative platform for analyzing polymers by pyrolysis-GC/MS.

• Journal of the Korean Society of Environmental Restoration Technology
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• v.19 no.2
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• pp.83-93
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• 2016

This study purposed to examine the water retention capacity of floor litter in deciduous forests. Water holding capacity(WHC) and interception storage capacity of Alnus hirsuta Turcz. ex Rupr., Quercus acutissima, Quercus mongolica litters were experimentally estimated. Physical characteristics of litters were also obtained to understand the relationships between water-retention capacity and litter characteristics. Experiments showed that WHC increases with specific volume of litter, varying 244.4% to 416.8% of its dry mass. Interception storage have estimated with rainfall simulation experiments. Maximum interception storage ($C_{max}$) and minimum interception storage ($C_{min}$) of litters were 220% and 138% of dry mass in Alnus hirsuta Turcz. ex Rupr., 218% and 137% in Quercus acutissima, and 240% and 156% in Quercus mongolica. Both $C_{max}$ and $C_{min}$ increased linearly with litter mass, and the values of $C_{min}$ in broadleaf litters have also linear relation to leaf area.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2008.11a
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• pp.89-92
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• 2008

This research analyzed the basic characteristics of unhardened concrete and the compression strength characteristics of hardened concrete according to liquidity retention agent mix rate change to improve the liquidity fluidity retention performance of high performance concrete, and produced the following results. The moment fluidity retention agent is added according to fluidity retention agent mix rate change, which increased fluidity retention agent mix rate, slump flow decreased, and in the case of slump flow according to the progress time change by the fluidity retention agent mix rates, the more fluidity retention agent mix rate increased, the lower slump flow change rate became. The moment fluidity retention agent is added according to fluidity retention agent mix rate change, fluidity retention agent mix rate increased compared to non-mixture of fluidity retention agent, and the air amount by progress time change by the fluidity retention agent mix rates slightly increased, however target range is still met and unit volume mass is inversely proportional to air amount. Compression strength according to age progress by the fluidity retention agent mix rates was shown to increase slightly with increase in fluidity retention agent mix rate, and yet the difference was not significant.

• The Journal of Korean Obstetrics and Gynecology
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• v.15 no.4
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• pp.218-227
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• 2002

Pelvic Inflammatory Disease(PID) is a spectrum of inflammatory disorders of the female genital tract involving at least the endrometrium and may include the fallopian tubes, ovaries, and pelvic cavity. Women with PID acutely experience pain and are at risk for sepsis; however, the long-term complications such as chronic pelvic pain, organic changes like chronic salpingitis, adhesions, etc., and the significant increases in ectopic pregnancy and infertility are more important and hard to control. This study is about one patient who has chronic PID with inflammatory pelvic mass. The patient was treated with retention enema therapy which use herbs effective for reducing inflammation, resolution abdominal mass, promoting blood circulation. Also, treated with herbal medication of Danchisoyosan(丹梔逍遙散) and Moxibution at Zhongwan(中脘), Guanyuan(關元). After total treatment for three months, the patient's symptoms are improved and the size of inflammatory pelvic mass is reduced. This results indicates that the combination treatment, especially the retention enema therapy is effective on reducing symptoms of PID and the size of secondary inflammatory organic changes.

• Nuclear Engineering and Technology
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• v.48 no.4
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• pp.906-914
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• 2016

We investigated the heat load imposed on the lower head of a reactor vessel by the natural convection of the oxide pool in a severe accident. Mass transfer experiments using a $CuSO_4-H_2SO_4$ electroplating system were performed based on the analogy between heat and mass transfer. The $Ra^{\prime}_H$ of $10^{14}$ order was achieved with a facility height of only 0.1 m. Three different volumetric heat sources were compared; two had identical configurations to those previously reported, and the other was designed by the authors. The measured Nu's of the lower head were about 30% lower than those previously reported. The measured angular heat flux ratios were similar to those reported in existing studies except for the peaks appearing near the top. The volumetric heat sources did not affect the Nu of the lower head but affected the Nu of the top plate by obstructing the rising flow from the bottom.

• Journal of Korea Technical Association of The Pulp and Paper Industry
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• v.39 no.1 s.119
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• pp.8-15
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• 2007

In an effort to develop control strategies for the wet-end of paper machines, dynamic models for retention and formation processes have been developed. The retention process, including headbox total and filler consistencies, white water total and filler consistencies, the basis weight and the ash content of paper, can be modeled from first-principles (mass balances). To include the effect of wet-end chemistry variables, first-pass retention was included as a parameter dependent on operating conditions. In addition, dynamics of formation was simulated by developing an empirical model of formation and coupling with the dynamic models for the retention process. A series of experiments were performed using a pilot paper machine. The experimental results and the model predictions showed relatively good agreement.

• Nuclear Engineering and Technology
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• v.49 no.7
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• pp.1405-1413
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• 2017

To investigate the heat loads imposed on a reactor vessel through the natural convection of core melts in severe accidents, mass transfer experiments were performed based on the heat transfer/mass transfer analogy, using two- (2-D) and three-dimensional (3-D) facilities of various heights. The modified Rayleigh numbers ranged from $10^{12}$ to $10^{15}$, with a fixed Prandtl number of 2,014. The measured Nusselt numbers showed a trend similar to those of existing studies, but the absolute values showed discrepancies owing to the high Prandtl number of this system. The measured angle-dependent Nusselt numbers were analyzed for 2-D and 3-D geometries, and a multiplier was developed that enables the extrapolation of 2-D data into 3-D data. The definition of $Ra^{\prime}_H$ was specified for 2-D geometries, so that results could be extrapolated for 3-D geometries; also, heat transfer correlations were developed.

• Preventive Nutrition and Food Science
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• v.3 no.2
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• pp.111-118
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• 1998

To develop a simple, rapid and simultaneous analytical method of phenolic compounds using gas chromatography (GC) and gas chromatography/mass spectrophometer (GC/Ms), this experiment was carried out to search the retention times of capillary columns and the characteristics of fragment ions in electron impact mass spectra. Most of trimethylsilyl derivatives and underivatized phenolic compounds were separated very well on three kinds of capillary columns(HP-1), Ultra-2 and HP-35). Quantitiative determination of phenolic compounds was achieved by internal standards (p-hydroxybenzoic acid iopropyl ester, p-hydroxybenzoic acid ethyl ester). Calibration plts were linear in the investigated range, and the limits of detection were about 5 ng at split mode method. When analyzed by three columns, theseparation times were fairly constant on two nonpolar columns, but a few compounds showed slightly different separation order by the itnermediate polar HP-35 column. The important characteristic patterns of TMS derivatives of phenolic compounds on the EI/MS spectrra appeared at the base peak of [M-15]+ ion and presented at high abundance in most TMS derivatives of phenoloc compounds. [M]+, [M-CH3-COO]+, [M-Si(CH3)4]+ and [M-Si(CH3)4 -CH3]+ also observed in mass spectra of these compounds . Although several compounds have the same retention times on GC column, it might be possible to identify these compounds by the different patternsof mass frgement ions. The TMS derivatives, thus , provide additional information for identification of phenolic compounds in biological systems.

• Journal of Korea Soil Environment Society
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• v.2 no.1
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• pp.73-81
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• 1997

Retention ponds have been dug along some of the motorways to control water flow during rainstorms and to minmize environmental pollution. A retention pond located at Les Ardilleres about 20km South of Orleans along the A-71 motorway has been selected to evaluate the effectiveness of such a pond as a trap for heavy metals. Based on the "index of geoaccumulation" and the "enrichment factor" normalized to Fe introduced by Muller in 1979 and by Helz in 1976, respectively, the degree of contamination by heavy metals for the roadside soil and the settling particles was evaluated. As expected, the contamination was very severe in the roadside soil, while it was not so great in the settling particles. Using these methods, cadmium anomaly was traced in the settling particles of the retention pond, their occurrence being attributed partly to natural and partly to anthropogenic pollution. The estimated input of heavy metals associated with settling particles to the pond was 0.9 g/day Pb, 2.1 g/day Zn and 6mg/day Cd. A tentative mass balance of Pb and Zn originated by motor vehicles suggested that only 5 to l1% of heavy metals deposited on the surface of the motorway is carried to the retention pond by runoff water ; suggestions are made to improve their efficiency.ve their efficiency.

• Journal of Nutrition and Health
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• v.28 no.11
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• pp.1049-1055
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• 1995

This study was designed to investigate the effects of calcium supplementation on calcium metabolism in seven healthy college women, aged from 19 to 21 years old. For this purpose, metabolic studies were conducted for two weeks. During the first week, the subjects ate experimental diet which nutrients composition was similar to their usual intake. And during the consecutive second week, they ate the same experimental diet supplemented with 500mg of calcium daily. The results were summarized as follows ; 1) Fecal excretion of calcium increased significantly (P<0.05), but urinary excretion of that did not show any change after supplementary intake of calcium. 2) Mean apparent calcium absorption was 28.5% and retention was 182mg/day when subjects ate the experimental diet without calcium supplementation. Calcium retention was significantly ate the experimental diet without calcium supplementation. Calcium retention was decreased to 24.1% by additional intake of calcium. 3) Phosphorus balance did not show any change after additional intake of calcium. 4) Serum calcium level was also not changed by additional intake of calcium. 5) Serum calcium level increased significantly(P<0.05) but serum phosphorus level did not show any change after additional intake of calcium. The above results showed that supplementation of 500mg calcium daily can be helpful to increase calcium retention as well as the peak bone mass in young women eating usual Korean diets.