• Title/Summary/Keyword: magnetometry

Search Result 64, Processing Time 0.017 seconds

Magnetically Soft Nanomaterials Obtained by Devitrification of Metallic Glasses

  • Kulik, Tadeusz;Ferenc, Jaroslaw;Kowalczyk, Maciej;Xiubing, Liang;Nedelko, Natalya
    • Journal of Magnetics
    • /
    • v.9 no.2
    • /
    • pp.65-68
    • /
    • 2004
  • Magnetically soft nanomaterials obtained by controlled crystallisation of metallic glasses are the newest group of materials for inductive components. In particular, research is carried out in the field of alloys for high temperature applications. This kind of materials must meet two basic requirements: good magnetic properties and stability of properties and structure. In the present work the magnetic properties and structure of Fe-Co-Hf-Zr-Cu-B (HIDTPERM-type) alloys were investigated, as well as their stability. Differential thermal analysis, (DTA), X-ray diffractometry (XRD), transmission electron microscopy (TEM), magnetometry (VSM) and quasistatic hysteresis loop recording were used to characterise structure and properties of the alloys investigated. Optimisation against properties and their stability was performed, resulting in formulation of chemical composition of the optimum alloy, as well as its heat treatment.

The Effect of Manganese Substituted M-type Hexagonal Ba-ferrite

  • Lee, In-Kyu;Sur, Jung-Chul;Shim, In-Bo;Kim, Chul-Sung
    • Journal of Magnetics
    • /
    • v.14 no.2
    • /
    • pp.93-96
    • /
    • 2009
  • The Mn-substituted M-type Ba-ferrite ($BaFe_{12-x}Mn_xO_{19}$; x = 0, 2, 4, 6) powders were prepared by the HTTD (High Temperature Thermal Decomposition) method. The effect of $Mn^{3+}$ Jahn-Teller ions on the magnetic properties has been studied by x-ray diffraction, vibrating sample magnetometry, and $M{\ddot{o}}ssbauer$ spectroscopy. With increasing Mn substitution, the lattice parameter $a_0$ increases while $c_0$ decreases. The magnetocrystalline anisotropy constants ($K_1$) were determined as 2.9, 2.2, 1.8, and, $1.3{\times}10^6\;erg/cm^3$ for x = 0, 2, 4, and 6, respectively, by the LAS method. We have studied the change of cation distribution by $M{\ddot{o}}ssbauer$ spectroscopy which is closely related to $K_1$.

Structural and Magnetic Properties of perpendicular Recording Medium CoCrMo thin Film (수직자기기록매체 CoCrMo 박막의 구조와 자기적 성질)

  • 남인탁;홍양기
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 1988.10a
    • /
    • pp.46-46
    • /
    • 1988
  • Structural and magnetic properties of Co-Cr-Mo films were investigated in connection with sputtering conditions. Films were prepared using a convention RF sputtering system. X-ray diffractometry, scanning electron microscopy and transmission electron microscopy were employed to investigate structure properties. Vibrating sample magnetometry was used for coercivity and saturation magnetization measurements. Co-Cr-Mo films displayed reasonable values of perpendicular coercivity and saturation magnetization for perpendicular recording media and showed good perpendicular orientation of the hcp c-axis to the film surface. Perpendicular coercivity was strongly dependent upon substrate technique showed better c-axis orientation than hose using the stationary substrate. Co-Cr-Mo films of 2.9 at. % Mo content showed maximum perpendicular coercivity and saturation magnetization. The films deposited at lower Ar pressure showed good magnetic properties. There was no explicit relationship between the columnar structure and c-axis orientation. Co-Cr-Mo films was found to have suitable structural and magnetic properties for perpendicular recording media.

  • PDF

Ferromagnetic Domain Behaviors in Mn doped ZnO Film

  • Soundararajan, Devaraj;Santoyo-Salazar, Jaime;Ko, Jang-Myoun;Kim, Ki-Hyeon
    • Journal of Magnetics
    • /
    • v.16 no.3
    • /
    • pp.216-219
    • /
    • 2011
  • Mn doped ZnO films were prepared on Si (100) substrates using sol-gel method. The prepared films were annealed at $550^{\circ}C$ for decomposition and oxidation of the precursors. XRD analysis revealed the presence of ZnMnO hexagonal wurtzite phase along with the presence of small quantity of $ZnMn_2O_3$ secondary phase and poor crystalline nature. The 2D, 3D views of magnetic domains and domain profiles were obtained using magnetic force microscopy at room temperature. Rectangular shaped domains with an average size of 4.16 nm were observed. Magnetic moment measurement as a function of magnetic field was measured using superconducting quantum interference device (SQUID) magnetometry at room temperature. The result showed the ferromagnetic hysteresis loop with a curie temperature higher than 300 K.

A New Method to Determine the Spin Rorientation Angle of Cone Anisotropy from Polcrystalline Magnetization Curves: Anisotropy from Polycrystalline Magnetization Curves Application to $Nd_2Fe_{14}B$ (다결정 자화곡선을 이용한 콘이방성물질의 스핀재배열각 결정법 : $Nd_2Fe_{14}B$에의 적용)

  • ;Jin Han-min
    • Journal of the Korean Magnetics Society
    • /
    • v.8 no.3
    • /
    • pp.144-149
    • /
    • 1998
  • A new method to calculate the spin reorientation angle of cone anisotropy from magnetization curves of magnetically aligned powder is suggested. The spin reorientation angle of polycrystalline $Nd_2Fe_{14}B$ determined by this method coincided with the results obtained from torque magnetometry or magnetization measurements on single crystal. The underestimation of about 9% is expected if the basal plane anisotropy is neglected in determination of the spin reorientation angle of $Nd_2Fe_{14}B$ at 4.2 K.

  • PDF

Identification for the Vivid Yellow Diamonds (비비드 옐로우 다이아몬드의 감별 방안 연구)

  • Song, Jeongho;Yun, Yury;Song, Ohsung
    • Journal of the Korean Ceramic Society
    • /
    • v.49 no.6
    • /
    • pp.493-497
    • /
    • 2012
  • We propose a new reliable, fast, and low cost identification method for similarly looking 0.3ct vivid yellow color of natural, HPHT treated, and synthesized diamonds. Conventional optical microscopy as well as low temperature PL(photoluminescence), FT-IR, UV-VIS-NIR, micro-Raman spectroscopy, and vibrating sample magnetometry(VSM) characterization were executed. We could not distinguish the natural diamonds from the treated or the synthesized stones with an optical microscopy, PL, FT-IR, and UV-VIS-NIR spectroscopy. However, we could identify the treated diamond with micro-Raman spectroscopy due to unique $1440cm^{-1}$ peak appearance. VSM revealed easily the synthesized diamond because of its ferromagnetic behavior. Our preliminary propose on employing the Micro-Raman spectroscopy and VSM might be suitable for identification of the similar looking vivid yellow colored diamonds.

Magnetic anisotropy of Al/Tb-Fe-Co multilayer thin films (Al/Tb-Fe-Co 다층박막의 자기적 이방특성)

  • 김명한;문정탁;신웅식;임기조
    • Electrical & Electronic Materials
    • /
    • v.5 no.1
    • /
    • pp.8-13
    • /
    • 1992
  • 일련의 Al/Tb-Fe-Co 다층박막 시편이 DC마그네트론 스퍼터링에 의해 제조되었다. 이 박막들은 (xA/yB)n의 형태이고 여기서 x와 y는 각각 Al 및 Tb-Fe-Co 박막의 두께를 나타내고 n은 각 박막의 수를 나타낸다. 각 박막의 두께는 2~40nm이다. Al과 Tb-Fe-Co박막의 두께변화에 따른 다층박막의 자기적 성질이 vibration sample magnetometry(VSM)에 의해 측정되었다. 이들 다층박막은 동일한 스퍼터링조건에서 제조되고 수평 자기적 이방성 특성을 보이고 있는 단층 Tb-Fe-Co박막을 기준시편으로 하여 자기적 성질이 비교되었다. 다층박막 시스템에서는 현저한 계면 또는 박막두께의 효과가 발견되었으며 이들 효과에 의해 단층박막의 수평자기체가 다층박막에서는 강한 수직자기체로 변화되는 것을 알 수 있고, 또한 Al과 Tb-Fe-Co합금 경계구역에 스퍼터링에 따른 약 2nm두께의 dead layer가 존재함이 입증 되었다.

  • PDF

Mini-review on fabrication of nitrogen vacancy center in diamond and its application to NMR

  • Oh, Sangwon
    • Journal of the Korean Magnetic Resonance Society
    • /
    • v.23 no.3
    • /
    • pp.73-80
    • /
    • 2019
  • Nitrogen-vacancy (NV) is one of the most popular solid-state spin systems for quantum sensing. NV has been used for vector magnetometry with nanometer spatial resolution and sensors for nuclear magnetic resonance (NMR) in samples with small volume, less than 10 pL. Various studies are in progress to make NV a complementary sensor for current NMR technique. Fabricating and improving diamond itself are one of the research topics. This mini-review contains recent develops in diamond fabrication and treatment for higher NV yield. Additionally, we briefly introduce the development status of NV in NMR.