• Title/Summary/Keyword: magnetic phase stability

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Phase Stability of $Fe_{16}C_2$ and $Fe_{16}C_4$ from First-principles Calculations

  • Rahman, Gul;Kim, In-Gee
    • Proceedings of the Korean Magnestics Society Conference
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    • 2009.12a
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    • pp.74-75
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    • 2009
  • First-principles calculations were carried out to investigate the crystal stability and magnetism of $Fe_{16}C_2$ and $Fe_{16}C_2$. Our precise calculations show that the structure of high carbon phase is $Fe_{16}C_2$ and this structure is more stable in the ferromagnetic state than the nonmagnetic state. The Fe atoms induced negative magnetic moment at the C atoms, which interact with the nearest Fe atoms.

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A Study on the Magnetic Properties of Medicinal Ointments by Mossbauer Spectroscopy. (뫼스바우어 분광법에 의한 의약용 연고제의 자기적 특성 연구)

  • 도태성;김응찬;남효덕;최세곤
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1998.11a
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    • pp.327-330
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    • 1998
  • The stability of the properties of magnetite particles in novel medicinal magnetic ointments of multipurpose application was examined by Mossbauer spectroscopy. Comparative analysis of the results obtained by model fitting of $\^$57/Fe nuclei spectra with those known for the system Fe$_3$O$_4$-${\gamma}$-Fe$_2$O$_3$ allowed to identify the phase composition of the particles. This composition, as well as that of the initial pure component in the form of a highly dispersed fraction (∼ 100${\AA}$), differs noticeably from the stoichiometric one. Despite their small sizes, the particles exhibit no superparamagnetism ( in the temperature range from 95 to 300k ). Radiative sterilization of the ointments has no effect on the magnetic component composition.

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Influence of Ni Addition on Mechanical and Magnetic Properties of Yttria-Stabilized Tetragonal Zirconia

  • Kondo, H.;Sekino, T.;Choa, Y.H.;Kusunose, T.;Nakayama, T.;Niihara, K.
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 2000.06a
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    • pp.243-248
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    • 2000
  • Effect of NiO addition on microstructure, stability of tetragonal phase and mechanical properties was investigated. (Y, Ni)-TZP solid solution was obtained by pressureless sintering. The fracture toughness was increased by solid solution of NiO. Neither reaction phase nor glassy phase was observed at the grain boundaries. From these results, it was determined that solid solution of NiO was destabilized tetragonal phase of Y-TZP. Y-TZP/Ni nanocomposite that contained nano-sized Ni particles was also fabricated by internal reduction method. Some evaluations and discussions were carried out for both (Y, Ni)-TZP solid solution and Y-TZP/Ni nanocomposite.

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Development of the Six Degree-of-Freedom Active Vibration Isolation System by Using a Phase Compensated Velocity Sensor (위상 보상된 속도 센서를 이용한 6자유도 능동 방진 시스템의 개발)

  • Kim, Yong-Dae;Kim, Sang-Yoo;Park, Kyi-Hwan
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.33 no.11
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    • pp.1347-1352
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    • 2009
  • Magnetic force driven six degree-of-freedom active vibration isolation system is developed. The velocity sensor using an electromagnetic principle that is commonly used in the vibration control is investigated since its phase lead characteristic causes an instability problem for a low frequency vibration. A lag-type compensator is adopted to reduce the phase lead and the stability test is performed by using a Bode analysis. The performance of the AVIS is validated by comparing with the passive isolation system by using the frequency responses.

Development of Controller for MPB BLDC Motor (MPB BLDC 전동기의 제어기 개발)

  • 김상욱;김보열
    • The Transactions of the Korean Institute of Electrical Engineers P
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    • v.50 no.3
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    • pp.117-124
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    • 2001
  • The aim of this paper is to develop a controller of multi-phase bipolar brushless DC (MPB BLDC) motors for an electric bicycle. A MPB BLDC motor has a Permanent magnet rotor in which the magnetic arrangement is radial to the shaft and integral to the rotor laminations. This technique concentrates flux, giving a higher flux density than a surface-mounted PM motor and increases reluctance torque. The stator of MPB BLBC motor has parallel winding, allowing multi-phase separate independent controllability. It gets much more high power than wye-connection at same low voltage. The conventional techniques of exited with modulation(EWM), bidirection control, and partial square wale control are Proposed with one H-bridge and two photo sensors per phase. The Proposed controller is satisfied for the limited speed control and designed for system stability Experimental results show the performance of the proposed controller of MPB BLDC motors for an electric bicycle.

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Magnetic Characteristics of CoNbZr amorphous Films with Pd addition

  • Song, J.S.;Wee, S.B.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.05d
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    • pp.90-95
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    • 2003
  • The present paper is to investigate the phase stability and soft magnetic properties of amorphous CoNbZr films when Pd is added as a substitution for CoNbZr alloys. The films were prepared by a RF magnetron sputtering method. The CoNbZrPd films deposited on Si wafers exhibited amorphous structures being independent upon the amount of Pd added in the films. On the addition of 4.34% Pd, the excellent soft magnetic characteristics of the films were observed with a coercive force of 0.54 Oe and an anisotropy field of 11 Oe, whereas a coercive force of 1 Oe and an anisotropy field of 3.5 Oe were shown in the film without the addition of Pd. The increased anisotropy field and low coercive force of the films may be attributed to the occupancy of Pd in the preferred sites parallel to the external magnetic field applied on the deposition process. A permeability of about 1100 was kept constant in the operation frequency ranging up to 100 MHz, which can be explained by the Landau-Lifshitz formula.

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Soft Magnetic Properties of CoNbZr amorphous Films with Pd addition

  • Song, J.S,;Wee, S.B,
    • Proceedings of the Korean Society Of Semiconductor Equipment Technology
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    • 2002.11a
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    • pp.54-58
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    • 2002
  • The present paper is to investigate the phase stability and soft magnetic properties of amorphous CoNbZr films when Pd is added as a substitution for CoNbZr alloys. The films were prepared by a RF magnetron sputtering method. The CoNbZrPd films deposited on Si wafers exhibited amorphous structures being independent upon the amount of Pd added in the films. On the addition of 4.34% Pd, the excellent soft magnetic characteristics of the films were observed with a coercive force of 0.54 Oe and an anisotropy field of 11 Oe, whereas a coercive force of 1 Oe and an anisotropy field of 3.5 Oe were shown in the film without the addition of Pd. The increased anisotropy field and low coercive force of the films may be attributed to the occupancy of Pd in the preferred sites parallel to the external magnetic field applied on the deposition process. A permeability of about 1100 was kept constant in the operation frequency ranging up to 100 MHz, which can be explained by the Landau-Lifshitz formula.

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A Study on the Improvement of Performance and Stability of Induction Heating System (유도 가열 시스템의 성능과 안정성 향상에 관한 연구)

  • Gwon, Yeong-Seop;Yu, Sang-Bong;Hyeon, Dong-Seok
    • The Transactions of the Korean Institute of Electrical Engineers B
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    • v.48 no.8
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    • pp.417-425
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    • 1999
  • This paper presents an effective control scheme with the voltage-fed half-bridge series resonant inverter for induction heating system, which is based upon a load-adaptive tuned frequency tracking control strategy using PLL(Phase Locked Loop) and its peripheral control circuits. The proposed control strategy ensures a stable operation characteristics of overall inverter system and ZVS(Zero Voltage Switching) irrespective of sensitive load parameter variations, specially in the non-magnetic materials as well as power regulation. The detail operation principle and the characteristics of inverter system with the proposed control scheme are described and its validity is verified by the simulation and the experimental results for a prototype induction cooking system rated at 1.2kW.

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The Effects of Nitrogen on Microstructure and Magnetic Properties of Nanocrystalline Fe-Nb-B-N Thin Films (나노결정구조 Fe-Nb-B-N 박막의 미세구조 및 자기적 특성)

  • 박진영;서수정;노태환;김광윤;김종열;김희중
    • Journal of the Korean Magnetics Society
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    • v.7 no.5
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    • pp.250-257
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    • 1997
  • The microstructure and magnetic properties of Fe-Nb-B-N thin film alloys, which produced by rf magnetron sputtering method in $Ar+N_2$ mixed gas atmosphere, were investigated. The $Fe_{70}Nb_{14}B_{11}N_5$ films, annealed at 59$0^{\circ}C$, exhibit soft magnetic properties: $4{\pi}M_s=16.5kG$ , $H_c=0.13Oe$ and ${\mu}_{eff}$ (1~10 MHz)=5, 000. The frequency stability of the Fe-Nb-B-N films has also been found to be good up to 10 MHz. The Fe-Nb-B-N thin film alloys annealed at 59$0^{\circ}C$ consist of three phase; fine crystalline $\alpha$-Fe phase with grain size of about 5~10 nm, Nb-B rich amorphous phase and Nb-nitride precipitates with the size of less than 3 nm. Annealed Fe-Nb-B films have two phases; $\alpha$-Fe grains with the size of about 10 nm and Nb-B rich amorphous phase. The addition of N decreased $\alpha$-Fe grain size due to the precipitation of NbN. The good magnetic properties of the Fe-Nb-B-N film alloys are due to fine $\alpha$-Fe grains resulting from the precipitation of NbN.

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Magnetic Properties of Micron Sized Fe3O4 Crystals Synthesized by Hydrothermal Methods (수열합성을 이용하여 제작한 Fe3O4 결정입자의 자기적 특성)

  • Lee, Ki-Bum;Nam, Chunghee
    • Journal of Powder Materials
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    • v.26 no.6
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    • pp.481-486
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    • 2019
  • Iron oxides currently attract considerable attention due to their potential applications in the fields of lithiumion batteries, bio-medical sensors, and hyperthermia therapy materials. Magnetite (Fe3O4) is a particularly interesting research target due to its low cost, good biocompatibility, outstanding stability in physiological conditions. Hydrothermal synthesis is one of several liquid-phase synthesis methods with water or an aqueous solution under high pressure and high temperature. This paper reports the growth of magnetic Fe3O4 particles from iron powder (spherical, <10 ㎛) through an alkaline hydrothermal process under the following conditions: (1) Different KOH molar concentrations and (2) different synthesis time for each KOH molar concentrations. The optimal condition for the synthesis of Fe3O4 using Fe powders is hydrothermal oxidation with 6.25 M KOH for 48 h, resulting in 89.2 emu/g of saturation magnetization at room temperature. The structure and morphologies of the synthesized particles are characterized by X-ray diffraction (XRD, 2θ = 20°-80°) with Cu-kα radiation and field emission scanning electron microscopy (FE-SEM), respectively. The magnetic properties of magnetite samples are investigated using a vibrating sample magnetometer (VSM). The role of KOH in the formation of magnetite octahedron is observed.