• Title/Summary/Keyword: magnetic dilution

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Review on innovative small refrigeration methods for sub-Kelvin cooling

  • Dohoon, Kwon;Junhyuk, Bae;Sangkwon, Jeong
    • Progress in Superconductivity and Cryogenics
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    • v.24 no.4
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    • pp.71-77
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    • 2022
  • Sub-Kelvin cooling has been generally demanded for the fields of low temperature physics, such as physical property measurements, astronomical detection, and quantum computing. The refrigeration system with a small size can be appropriately introduced when the measurement system does not require a high cooling capacity at sub-Kelvin temperature. The dilution refrigerator which is a common method to reach sub-Kelvin, however, must possess a large 3He circulation equipment at room temperature. As alternatives, a sorption refrigerator and a magnetic refrigerator can be adopted for sub-Kelvin cooling. This paper describes those coolers which have been developed by various research groups. Furthermore, a cold-cycle dilution refrigerator of which the size of the 3He circulation system is minimized, is also introduced. Subsequently, a new concept of dilution refrigerator is proposed by our group. The suggested cooler can achieve sub-Kelvin temperature with a small size since it does not require any recuperator and turbo-molecular vacuum pump. Its architecture allows the compact configuration to reach sub-Kelvin temperature by integrating the sorption pump and the magnetic refrigerators. Therefore, it may be suitably utilized in the low temperature experiments requiring low cooling capacity.

Rheological behavior study of Marine Lubricating oil on the amount of MGO (Marine Gas Oil) dilution (해상용 경유의 희석량에 따른 선박용 윤활유의 유변학적 거동연구)

  • Song, In Chul;Lee, Young Ho;Yeo, Young Hwa;Ahn, Su Hyun;Kim, Dae il
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.22 no.2
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    • pp.240-245
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    • 2016
  • This paper describes the rheological behavior study such as viscosity and change of shear stress regarding marine lubricating oil according to the amount of Marine Gas Oil (MGO) dilution. The viscosity reduction due to fuel dilution is crucially important characteristic to decreasing engine durability because of the abrasion of piston ring or liner. The lubricating oil used in this paper was blended with magnetic stirrer diluted High Sulfur Diesel (HSD, 0.05 wt%) ratio of 3 %, 6 %, 10 %, 15 % and 20 %. The viscosity and shear stress of diluted lubricating oil were measured with the temperature range from $-10^{\circ}C$ to $80^{\circ}C$ using a rotary viscometer (Brookfield Viscometer). As the amount of MGO dilution increasing in lubricating oil, the viscosity and stress of those decreased, because the lubricating oil diluted MGO with low viscosity show the trends to decreased viscosity and shear stress. Especially, the viscosity and shear stress of lubricating oil radically decreased at low temperature ($0{\sim}-10^{\circ}C$) and doesn't effect in MGO dilution at over $40^{\circ}C$. As temperature risen, the reduction of the viscosity and shear stress in lubricating oil shows the Newtonian behavior. The lubricating oil was required to check up periodically to improve engine durability since the viscosity reduction by MGO dilution accelerating the engine abrasion.

Structural and Magnetic Properties of Dilute Spinel Ferrites: Neutron Diffractometry and Magnetometry Investigations

  • Mamiya, H.;Terada, N.;Kitazawa, H.;Hoshikawa, A.;Ishigaki, T.
    • Journal of Magnetics
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    • v.16 no.2
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    • pp.134-139
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    • 2011
  • Magnetic properties of highly zinc-substituted manganese ferrites are discussed on the basis of cation distribution. High throughput neutron powder diffractometry indicates that the prepared samples possess a nearly normal spinel structure, where the substitution of nonmagnetic zinc ions mainly causes the dilution of magnetic ions in the A-sublattice and consequently affects bond-randomness in the B-sublattice. On the other hand, the estimated occupancy of manganese ions in the B site indicates that random anisotropy effects due to local Jahn-Teller distortions gradually weaken with the substitution. Bulk magnetometry indicates that the substitution smears the transition from a paramagnetic phase to a soft-magnetic phase. Furthermore, at lower temperatures, such a soft-magnetic phase is destabilized and a magnetic glassy state appears. These features of the magnetic properties of dilute spinel ferrites are discussed from the viewpoint of the above-mentioned various types of disorders.

Local Structure and Magnetic Properties of Fe-Mn Nanocrystalline Alloys Fabricated by Mechanical Alloying Technique as a Function of Milling Time

  • Tarigan, Kontan;Yang, Dong Seok;Yu, Seong Cho
    • Journal of Magnetics
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    • v.18 no.1
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    • pp.1-4
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    • 2013
  • Structural and magnetic properties of $Fe_{50}Mn_{50}$ nanocrystalline alloys prepared by the mechanical alloying technique (using commercial Fe and Mn powders as the precursors) are studied as a function of milling time, 1 hr to 48 hrs. The nano-crystallite size and shape are examined by using scanning electron microscopy (SEM). The effect of milling time on structural characterization was investigated using X-ray diffractometer (XRD) and extended X-ray absorption fine structure spectroscopy (EXAFS). Both XRD and EXAFS studies showed that the alloying process should be completed after 36 hrs milling. Concerning the magnetic behavior, the data obtained from superconducting quantum interference devices (SQUID) exhibited both magnetic saturation ($M_s$) and coercivity ($H_c$) depend strongly on the milling time, which are related to the changes in the crystallite size and magnetic dilution.

Mossbauer Effect on the Influences of Substituted $Al^{3+}$ of Goethit in Clay Cheju Island (제주도 찰흙에 함유된 Goethite에서 $Al^{3+}$ 치환 영향에 대한 Mossbauer 효과)

  • 강동우;김두철;고정대;홍성락;송관철
    • Journal of the Korean Magnetics Society
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    • v.7 no.4
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    • pp.196-204
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    • 1997
  • In order to study the effect of substituted $Al^{3+}$ of goethite, which was collected from Shinpyeongli in Cheju Island, we used X-ray diffractometer and Mossbauer spectrometer. In X-ray diffraction analysis, the X-ray diffraction peaks of goethite are not detected due to the high substituted Al contents of goethite. Isomer shifts indicated that the valence of Fe ions is almost oxidized trivalent of high spin state. It is believed that the contents of substituted diamagnetic $Al^{3+}$ for $Fe^{3+}$ is about 15.5 mol%. It seems that Neel temperature and saturated magnetic hyperfine field of the clay goethite are about 250 K and 498 kOe, respectively. For the temperature lower than Neel temperature, quadrupole splittings of the clay goethite are greatly influenced by $Al^{3+}$ substitution. It is believed that the high decrease of Neel temperature and magnetic hyperfine field of the clay goethite results from the magnetic dilution produced by substituting the diamagnetic $Al^{3+}$/TEX> for $Fe^{3+}$.

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Development of Hybrid Insulating Coating for Fe-based Soft Magnetic Powder (철계 연자성 분말용 하이브리드 절연 코팅막 개발)

  • Kim, Jungjoon;Kim, Sungyeom;Kim, Youngkyun;Jang, Taesuk;Kim, Hwi-jun;Kim, Youngjin;Choi, Hyunjoo
    • Journal of Powder Materials
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    • v.28 no.3
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    • pp.233-238
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    • 2021
  • Iron-based amorphous powder attracts increasing attention because of its excellent soft magnetic properties and low iron loss at high frequencies. The development of an insulating layer on the surface of the amorphous soft magnetic powder is important for minimizing the eddy current loss and enhancing the energy efficiency of high-frequency devices by further increasing the electrical resistivity of the cores. In this study, a hybrid insulating coating layer is investigated to compensate for the limitations of monolithic organic or inorganic coating layers. Fe2O3 nanoparticles are added to the flexible silicon-based epoxy layer to prevent magnetic dilution; in addition TiO2 nanoparticles are added to enhance the mechanical durability of the coating layer. In the hybrid coating layer with optimal composition, the decrease in magnetic permeability and saturation magnetization is suppressed.

천문관측을 위한 극저온 발생장치 개발

  • 김동락;정원묵;양형석
    • Bulletin of the Korean Space Science Society
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    • 2003.10a
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    • pp.67-67
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    • 2003
  • 적외선 고감도천문관측 등 우주탑재체에서의 천문관측에서는 망원경 또는 관측용 센서를 4K 또는 그 이하로 냉각하여 고감도 관측을 하고 있다. 이와 관련하여 액체헬륨-4, 초유동헬륨, 액체헬륨-3, magnetic cooling 또는 dilution refrigeration 등의 방법으로 4K∼0.05K 영역까지의 극저온을 얻을 수 있다 우주탑재체에서의 극저온을 발생하는 방법과 본 연구실에서 개발 중인 ∼1K 까지의 극저온 발생장치의 설계 등에 관하여 논의한다.

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Effects of Ga Substitution in LaFe1-xGaxO3 (χ= 0, 0.1, 0.3, 0.5, and 0.7)

  • Yoon, Sung-Hyun;Park, Seung-Jin;Cha, Deok-Joon;Min, Byung-Ki;Kim, Chul-Sung
    • Journal of Magnetics
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    • v.7 no.2
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    • pp.40-44
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    • 2002
  • Crystallographic and magnetic properties of ;$LaFe_{1-x}Ga_xO_3$($\chi$= 0, 0.1, 0.3, 0.5, and 0.7) were studied using XRD and Mossbauer spectroscopy. The crystal structures were found to be orthorhombic and the lattice parameters $\alpha$, b, and c were found to decrease with increasing Ga substitution. M$\ddot{o}$ssbauer spectra were obtained at various absorber temperatures ranging from 20 K to 750 K. The M$\ddot{o}$ssbauer spectra were all sextets below $T_N$ and were all singlets above $T_N$. Asymmetric broadening of the M$\ddot{o}$ssbauer spectral lines at 20 K was explained by the multitude of possible environments for an iron nucleus. As the temperature increases to $T_N$, a systematic line broadening in M$\ddot{o}$ssbauer spectra was observed and interpreted to originate from different temperature dependencies of the magnetic hyperfine fields at various iron sites.

Evaluation of the signal intensity of magnetic resonance angiography in accordance with the dilution rate of the contrast agent (조영제 희석률에 따른 조영증강 자기공명혈관조영검사의 신호강도 평가)

  • Choi, Kwan-Woo;Seo, Sung-Mi;Son, Soon-Yong
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.15 no.8
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    • pp.5124-5130
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    • 2014
  • Dilution of the contrast agent by analyzing the change in the signal intensity during MR angiography in accordance with the viscosity and osmotic pressure minimizes the side effects, and improves the image quality. The contrast agent molarity changes by the dilution of the contrast agent in the blood, as it is injected, which leads to a change in signal intensity. Based on this principle, a phantom was prepared and experiments were performed. After the phantom experiment, a clinical experiment was conducted using the results of the phantom experiment. From November 2013 to January 2014, a group of patients were classified into diluted contrast agent (30 persons) and undiluted (30 persons), and the signal intensity of the cerebral vessels was compared. The signal intensity of the phantom according to the molarity of the contrast agent increased sharply from 0.0125 mmol, reached a peak at 20 mmol, and achieved equilibrium from 200 mmol. Based on the study results, the signal intensity of the blood vessels in the brain through were compared in a clinical experiment. All the brain vessels in the imaging range with diluting a high content of the gadolinium contrast agent showed high signal intensity. This result supports the phantom experiment and means that using the 500mmol diluted contrast agent is better than using 1000mmol undiluted contrast agent because it is easier to approach the 20mmol level needed to achieve the highest signal intensity. This study has significance in that it can minimize the high viscosity and osmotic pressure, which can cause side effects and improve the image quality using the method of the dilution rate.

HYDROGEN DECREPITATION AND MAGNETIC PROPERTIES OF $Sm_{2}Fe_{17}-TYPE$ ALLOY MODIFIED WITH A SMALL ADDITION OF Nb

  • Kwon, H.W.;Harris, I.R.
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.432-436
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    • 1995
  • The hydrogen decrepitation behaviour of the $Sm_{2}Fe_{17} alloy containing 4at%Nb was examined by means of DTA and SEM metallography, and the magnetic properties of the alloy were studied by means of VSM or TMA. It has been found that a simple hydrogenation and degassing treatment for the alloy caused a poor hydrogen decrepitation. The cycle treatment consisting of repeated hydrogenation and degassing, however, caused a severe hydrogen decrepitation with a combination of intergranular and transgranular failure. The disproportionation temperature of the hydrogenated $Sm_{2}Fe_{17}-type alloy was enhanced significantly by small addition of Nb. It has also been found that the Curie temperature of $Sm_{2}Fe_{17} matrix phase in the Nb-containing alloy has been enhanced by the hydrogenation, and this was attributed to the increase in interatomic distance between the neighbouring iron atoms caused by the interstitial occupancy of the hydrogen atom into the $Sm_{2}Fe_{17}-type lattice. The magnetisation of the $Sm_{2}Fe_{17} alloy containing Nbwas found to be lower than that of the Nb-free alloy, and this was explained by the dilution effect due to the presence of the paramagnetic $Sm_{2}Fe_{17} phase.

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