• 제목/요약/키워드: magnesium reduction

검색결과 149건 처리시간 0.026초

산화마그네슘 함량이 실험적 알지네이트 인상재의 특성에 미치는 영향 (EFFECT OF MAGNESIUM OXIDE CONTENTS ON THE PROPERTIES OF EXPERIMENTAL ALGINATES)

  • 배일환;우이형;최대균
    • 대한치과보철학회지
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    • 제41권5호
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    • pp.551-564
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    • 2003
  • Statement of problem : Magnesium oxide may increase pH of alginate, and supply magnesium ions to the polymerization reaction of alginate. Purpose : This study was designed to evaluate the influence of incorporation of magnesium oxide to alginate composition. Material and Method : Seven kinds of experimental alginates were prepared and used for the experiments. Components with unchanging concentrations were sodium alginate 15%, calcium sulfate 14%, sodium phosphate 2%, and zinc fluoride 3%. Contents of magnesium oxide were varied as 0%, 1%, 2%, 3%, 4%, 5%, 6%. Diatomaceous earth were added to each experimental groups as balance to be 100%. Control group was a MgO 0% group. Working time, setting time, elastic recovery strain in compression, compressive strength and tear resistance were measured were measured. Sample size for each groups were 10. Arithmetic means were used as each groups representative values. Regression test between MgO contents and results, Duncan's multiple range test, and One-way ANOVA test were done between groups at level of 0.05. Results : 1 Magnesium oxide made the working time and setting time as longer(p<0.0001). 2 Magnesium oxide did not alter the elastic recovery(p>0.05). 3. Magnesium oxide contents between 2% and 4% exhibited the lowest strain in compression on alginates(p<0.0001). 4. Magnesium oxide made the compressive strength and the tear resistance stronger(p<0.0001). Conclusion : These results mean that setting time of alginate maybe controlled and that mechanical properties maybe improved by the incorporation of magnesium oxide into alginate, without any reduction of elasticity.

Intravenous Magnesium Infusion for the Prevention of Symptomatic Cerebral Vasospasm after Aneurysmal Subarachnoid Hemorrhage

  • Jeon, Jin-Sue;Sheen, Seung-Hun;Hwang, Gyo-Jun;Kang, Suk-Hyung;Heo, Dong-Hwa;Cho, Yong-Jun
    • Journal of Korean Neurosurgical Society
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    • 제52권2호
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    • pp.75-79
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    • 2012
  • Objective : The study examined the difference in the incidence of symptomatic cerebral vasospasm with magnesium supplementation in aneurysmal subarachnoid hemorrhage (SAH) in a Korean population. Methods : This retrospective analysis was performed in 157 patients diagnosed with aneurysmal SAH from January 2007 to December 2011 at a single center. Seventy patients (44.6%) received a combination treatment of nimodipine with magnesium and 87 patients (55.4%) received only nimodipine. A matched case-control study using propensity scores was conducted and 41 subjects were selected from each group. A dosage of 64 mmol/day of magnesium was administrated. Results : The infusion of magnesium did not reduce the incidence of symptomatic cerebral vasospasm (n=7, 17.1%, p=0.29) compared with simple nimodipine injection (n=11, 26.8%). The ratios of good clinical outcome (modified Rankin scale 0-2) at 6 months were similar, being 78% in the combination treatment group and 80.5% in the nimodipine only group (p=0.79). The proportions of delayed cerebral infarction was not significantly lower in patients with combination treatment (n=2, 4.9% vs. n=3, 7.3%; p=0.64). There was no difference in the serum magnesium concentrations between the patients with symptomatic vasospasm and without vasospasm who had magnesium supplementation. No major complications associated with intravenous magnesium infusion were observed. Conclusion : Magnesium supplementation (64 mmol/day) may not be beneficial for the reduction of the incidence of symptomatic cerebral vasospasm in patients with aneurysmal SAH.

Magnesium Sulfate Induced Toxicity in Vitro in AGS Gastric Adenocarcinoma Cells and in Vivo in Mouse Gastric Mucosa

  • Zhang, Xulong;Bo, Agula;Chi, Baofeng;Xia, Yuan;Su, Xiong;Sun, Juan
    • Asian Pacific Journal of Cancer Prevention
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    • 제16권1호
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    • pp.71-76
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    • 2015
  • Magnesium sulfate is widely used as a food additive and as an orally administered medication. The aim of this study was to evaluate the possible cytotoxicity of magnesium sulfate on AGS human gastric adenocarcinoma cells and gastric mucosa in mice. A trypan blue exclusion assay was used to determine the reduction in viability of AGS cells exposed to magnesium sulfate, and then effects on cell proliferation were quantified. The role of magnesium sulfate-mediated pro-inflammatory cytokine production in AGS cells was also investigated. mRNA expression for IL-$1{\beta}$, IL-6, IL-8, and TNF-${\alpha}$ was determined by RT-PCR, and secretion of these cytokines was measured by ELISA. Immunohistochemical evaluation of IL-$1{\beta}$, IL-6, and TNF-${\alpha}$ expression was conducted in mouse gastric mucosa. Addition of 3 to 50 mM magnesium sulfate to AGS cells inhibited both cell proliferation and cell viability in a dose-dependent manner. Magnesium sulfate had little effect on production of IL-$1{\beta}$ or IL-6 but significantly inhibited production of IL-8. The animal model demonstrated that magnesium sulfate induced production of IL-$1{\beta}$, IL-6, and TNF-${\alpha}$. These preliminary data suggest that magnesium sulfate had a direct effect on the stomach and initiates cytotoxicity in moderate concentrations and time periods by inhibiting viability a nd proliferation of AGS cells and by regulating expression and/or release of pro-inflammatory cytokines.

PLASTICITY-BASED WELDING DISTORTION ANALYSIS OF THIN PLATE CONNECTIONS

  • Jung, Gonghyun;Tsai, Chon L.
    • 대한용접접합학회:학술대회논문집
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    • 대한용접접합학회 2002년도 Proceedings of the International Welding/Joining Conference-Korea
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    • pp.694-699
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    • 2002
  • In autobody assembly, thin-wall, tubular connections have been used for the frame structure. Recent interest in light materials, such as aluminum or magnesium alloys, has been rapidly growing for weight reduction and fuel efficiency. Due to higher thermal expansion coefficient, low stiffness/strength, and low softening temperature of aluminum and magnesium alloys, control of welding-induced distortion in these connections becomes a critical issue. In this study, the material sensitivity to welding distortion was investigated using a T-tubular connection of three types materials; low carbon steel (A500 Gr. A), aluminum alloy (5456-H116) and magnesium alloy (AZ91C-T6). An uncoupled thermal and mechanical finite element analysis scheme using the ABAQUS software program was developed to model and simulate the welding process, welding procedure and material behaviors. The predicted angular distortions were correlated to the cumulative plastic strains. A unique relationship between distortion and plastic strains exists for all three materials studied. The amount of distortion is proportional to the magnitude and distribution of the cumulative plastic strains in the weldment. The magnesium alloy has the highest distortion sensitivity, followed by the other two materials with the steel connection having the least distortion. Results from studies of thin-aluminum plates show that welding distortion can be minimized by reducing the cumulative plastic strains by preventing heat diffusion into the base metal using a strong heat sink placed directly beneath the weld. A rapid cooling method is recommended to reduce welding distortion of magnesium tubular connections.

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변형속도에 따른 M1 마그네슘 합금의 고온변형 중 미세조직 형성 거동 (Effect of Strain Rate on Microstructure Formation Behavior of M1 Magnesium Alloy During High-temperature Deformation)

  • 이규정;김권후
    • 열처리공학회지
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    • 제32권1호
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    • pp.1-11
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    • 2019
  • In this study, microstructure evolution and crystallographic orientation are investigated under various deformation conditions in M1 magnesium alloy. M1 magnesium ingot was rolled at 673 K with the rolling reduction of 30%. The compression test specimens were machined out from rolled plate, and then the specimens were annealed at 823 K for 1h. Uniaxial compression tests were conducted at 723 K and under the strain rate ranging from $5.0{\times}10^{-4}s^{-1}$ to $5.0{\times}10^{-2}s^{-1}$ up to a true strain of -1.0. For observation of crystal orientation distribution, EBSD measurement was performed. Occurrence of the dynamic recrystallization and grain boundary migration were confirmed in all case of the specimens. The distribution of the grains is not uniformed in the experimental conditions.

Solid SCR용 암모니아 저장물질인 Magnesium Ammine Chloride의 합성방법 및 물질특성 연구 (A Study on Synthetic Method and Material Characteristics of Magnesium Ammine Chloride as Ammonia Transport Materials for Solid SCR)

  • 신종국;윤천석;김홍석
    • 대한기계학회논문집B
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    • 제39권11호
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    • pp.843-851
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    • 2015
  • 질소산화물 저감에 사용하는 solid SCR용 고체상 암모늄 저장물질의 하나인 magnesium ammine chloride에 대한 실험실 규모에서의 제조방법과 제조한 물질의 분석연구를 수행하였다. 기저물질인 염화마그네슘에 암모니아 가스를 흡착하기 위한 실험조건의 도출을 위하여, Van't Hoff Plot으로 평형압 선도를 계산하였고, 간이반응기를 제작한 후, magnesium ammine chloride를 제조하였다. DA, IC, FT-IR, XRD, SDT 등으로 제조한 시료의 성분을 분석하였고, 제조한 시료에 수분이 존재한다는 것을 알 수 있었다. 암모니아 가스 흡착률을 증대하기 위하여 수분 제거에 적절한 새로운 실험방법을 제안하였고, 제안한 방법을 적용한 결과, 암모니아 가스의 흡착률이 대략 100%에 도달하였다.

마그네슘의 용융염전해시(熔融鹽電解時) 두 가지 염욕조성(鹽浴組成)의 비교실험 (Comparison of Two-Types Compositions of Mixed Salts in Fused Salt Electrolysis of Magnesium)

  • 박형규;박진태;최영윤
    • 자원리싸이클링
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    • 제15권2호
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    • pp.32-36
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    • 2006
  • 마그네슘은 자동차 엔진 경량화재료 및 휴대폰과 노트북 PC케이스 등 기능성 경량재료로서의 용도개발과 함께 수요가 증가하고 있다. 마그네슘 제련법은 원료광의 특성에 따라 달라지는데 크게 용융염전해법과 열환원법 두가지로 구분할 수 있다. 본 연구에서는 염화마그네슘을 사용하여 용융염전해법에 의해 전해 마그네슘을 얻고자 하였다. 흑연양극의 침지깊이를 일정하게 하고 전해전압 7V로 두가지 조성의 염욕을 비교 실험하였다. $760^{\circ}C$에서 전해 실험한 결과 $KCl/NaCl/MgCl_2$ 혼합염욕이 $KCl/NaCl/CaCl_2/CaF_2/MgCl_2$ 혼합염욕보다 전류효율 면에서 더 효과적이었다. 회수된 전해 마그네슘의 순도는 98% 이상이었다. 본 연구를 통하여 용융염 전해장치를 Scale-up 하거나 상용화시 장치설계 등에 필요한 기초자료들을 축적할 수 있었다.

마그네슘 로드 휠의 유동성형 가공에 관한 연구 (A Study on Flow Forming Process of Magnesium Road Wheel)

  • 김정호;이종주;박수민;윤형석
    • 소성∙가공
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    • 제23권2호
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    • pp.116-121
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    • 2014
  • Low pressure die casting and flow forming have been successfully used to produce sound road wheels from magnesium alloy AM80. In the current study, high speed compression testing was initially conducted to simulate the flow forming of a Mg wheel. Subsequently the flow forming was simulated with "Forge$^{TM}$", an FEM software package. On the basis of flow forming simulations, the flow forming of the Mg wheel was performed under different conditions. For the flow forming experiments, the preform castings were made by low pressure die casting from AM80, a commercial magnesium alloy. In flow forming of the magnesium preform wheel, the flow forming of the Mg wheel was successfully accomplished when the feed rate was less than half that for the forming of an aluminum road wheel. The reduction in feed rate was 52%. Finally, a comparison with the flow forming simulations was made.

건식플라즈마 표면처리법에 의한 마그네슘 합금의 내식특성 향상 (A Study on the Enhancement of Corrosion Resistance of Magnesium Alloy by Dry Plasma Process)

  • 윤용섭
    • 해양환경안전학회지
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    • 제17권2호
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    • pp.155-160
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    • 2011
  • 현재 지구온난화 등의 환경문제로 인해 각종 산업분야에서 정량화에 대한 요구가 증대되어 해양산업에도 그 수요가 증가하고 있는 실정이다. 따라서 본 연구에서는 차세대 경량화 재료인 마그네슘이 활용되기 위해서 반드시 극복해야할 가장 중요한 특성인 내식특성에 대하여 고찰하고, 그 내식특성 향상을 위한 마그네슘 박막의 Morphology나 결정배향성의 영향을 해명하고자 하였다. 실험결과로부터 제작한 Mg 박막의 전기화학적 내식특성은 Ar 가스압이 높은 조건에서 제작한 막일수록 내식특성이 우수하였다. 이러한 경향은 표면 및 단면의 Morphology와 결정배향성과의 상관관계를 통하여 설명 가능하였다.