• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2001년도 추계학술대회 논문집
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• pp.260-263
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• 2001

Mechanical properties have been accepted to be major factor to improve wear resistance. The effect of mechanical properties on wear resistance of 0.27C-0.70Ni-1.42Cr-0.20Mo steel was studied under various test conditions. It is clear that yield strength, tensile strength, impact value, and hardness are strongly related each other. Wear resistance tests as pin on plate type and dry sand / rubber wheel type proved to be that wear depends on mechanical properties. Microstructures were also observed to make clear the wear properties. At quenching and low temperature tempering, the specimen has a good wear resistance.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 1993년도 특별강연 및 춘계학술발표 개요집
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• pp.120-124
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• 1993

The Charpy V impact test on subsize was performed on narrow laser welds of low carbon steel sheets, joined by using a continuous wave 3kW CO$_2$ laser. Under certain conditions, a bimodal fracture behaviour has been experienced in Charpy V impact test of narrow laser beam welds. Deviation of the fracture path from the fusion zone into the base metal was dominated at high test temperature. It can be seen that the deviation always occurred after ductile initiation. If the deviation occurs on a small testing specimen, the same trend would happen on the actual laser welded structure. Fracture will then propagate through the base material even if the weld metal has low toughness.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.936-936
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• 2006

Bulk amorphous materials have been intensively studied to apply for various advanced industry fields due to their high mechanical, chemical and electrical properties. These materials have been produced by several techniques such as mechanical alloying, melt spinning and gas atomization, etc. Among them, the atomization is the most potential technique for commercialization due to high cooling rate during solidification of the melt and mass productivity. However, the amorphous powders still have some limitations because of their low ductility and toughness. Therefore, intensive efforts have to be carried out to increase the ductility and toughness. In this study, the Ni-based amorphous powder was produced by the gas atomization process. And in order to increase the ductile toughness, ductile Cu phase was coated on the Ni amorphous powder by spray drying process. The characteristics of the as-synthesis powders have been examined and briefly mentioned. The master alloy with $Ni_{57}Zr_{20}Ti_{16}Si_2Sn_3$ was prepared by vacuum induction melting furnace with graphite crucible and mold. The atomization was conducted at $1450^{\circ}C$ under the vacuum of $10^{-2}$ torr. The gas pressure during atomization was varied from 35 to 50 bars. After making the Ni amorphous powders, the spray drying was processed to produce the Cu -coated Ni amorphous composite powder. The amorphous powder and Cu nitrate solution were mixed together with a small amount of binder and then it was sprayed at temperature of $130^{\circ}C$ and rotating speed of 15,000 R.P.M.

• Journal of Welding and Joining
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• 제14권5호
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• pp.134-144
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• 1996

A study was performed to investigate the properties of base metal and weldment for two HSLA steels and one HY-100 steel. Tensile, yield strength and elongation of HSLA-A steel were superior to those of HY-100 steel and yield ratios in HSLA-A and HSLA-B steels were higher than HY-100 steel owing to the precipitation of $\varepsilon$-Cu phase. The impact energy of HSLA-A steel was greater at all aging temperatures than that of HY-100 steel. HSLA-A and HY-100 steels had low impact transition temperature of about -l$25^{\circ}C$ and high upper shelf energy, The peak hardness of weldment in HSLA-A, HSLA-B and HY-100 steels were Hv 299, Hv 275 and Hv 441, respectively. The hardenability of HY-100 steel was largest due to the higher amount of carbon. The y-groove test showed that HSLA steels had superior resistance to cold cracking. Toughness of weld joint at the F. L. and F. L. ＋1mm in HSLA-A was almost the same as HY-100, but those at F. L.＋3mm and F. L.＋5mm was greater in HSLA-A steel.

• Nuclear Engineering and Technology
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• 제48권6호
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• pp.1376-1386
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• 2016

This study investigated the loading rate effect on the fracture resistance under cyclic loading conditions to understand clearly the fracture behavior of piping materials under seismic conditions. J-R fracture toughness tests were conducted under monotonic and cyclic loading conditions at various displacement rates at room temperature and the operating temperature of nuclear power plants (i.e., $316^{\circ}C$). SA508 Gr.1a low-alloy steel and SA312 TP316 stainless steel piping materials were used for the tests. The fracture resistance under a reversible cyclic load was considerably lower than that under monotonic load regardless of test temperature, material, and loading rate. Under both cyclic and monotonic loading conditions, the fracture behavior of SA312 TP316 stainless steel was independent of the loading rate at both room temperature and $316^{\circ}C$. For SA508 Gr.1a lowalloy steel, the loading rate effect on the fracture behavior was appreciable at $316^{\circ}C$ under cyclic and monotonic loading conditions. However, the loading rate effect diminished when the cyclic load ratio of the load (R) was -1. Thus, it was recognized that the fracture behavior of piping materials, including seismic loading characteristics, can be evaluated when tested under a cyclic load of R = -1 at a quasistatic loading rate.

• The Journal of Advanced Prosthodontics
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• 제1권3호
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• pp.113-117
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• 2009

STATEMENT OF PROBLEM. Recently Yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) has been introduced due to superior flexural strength and fracture toughness compared to other dental ceramic systems. Although zirconia has outstanding mechanical properties, the phenomenon of decrease in the life-time of zirconia resulted from degradation in flexural strength after low temperature aging has been reported. PURPOSE. The objective of this study was to investigate degradation of flexural strength of Y-TZP ceramics after various low temperature aging treatments and to evaluate the phase stability and micro-structural change after aging by using X-ray diffraction analysis and a scanning electron microscope (SEM). MATERIAL AND METHODS. Y-TZP blocks of Vita In-Ceram YZ (Vita Zahnfabrik, Bad $S\ddot{a}ckingen$, Germany) were prepared in 40 mm (length) $\times$ 4 mm (width) $\times$ 3 mm (height) samples. Specimens were artificially aged in distilled water by heat-treatment at a temperature of 75, 100, 125, 150, 175, 200, and $225^{\circ}C$ for 10 hours, in order to induce the phase transformation at the surface. To measure the mechanical property, the specimens were subjected to a four-point bending test using a universal testing machine (Instron model 3365; Instron, Canton, Mass, USA). In addition, X-ray diffraction analysis (DMAX 2500; Rigaku, Tokyo, Japan) and SEM (Hitachi s4700; Jeol Ltd, Tokyo, Japan) were performed to estimate the phase transformation. The statistical analysis was done using SAS 9.1.3 (SAS institute, USA). The flexural strength data of the experimental groups were analyzed by one-way analysis of variance and to detect statistically significant differences ($\alpha$= .05). RESULTS. The mean flexural strength of sintered Vita In-Ceram YZ without autoclaving was 798 MPa. When applied aging temperature at below $125^{\circ}C$ for 10 hours, the flexural strength of Vita In-Ceram YZ increased up to 1,161 MPa. However, at above $150^{\circ}C$, the flexural strength started to decrease. Although low temperature aging caused the tetragonal-to-monoclinic phase transformation related to temperature, the minimum flexural strength was above 700 MPa. CONCLUSION. The monoclinic phase started to appear after aging treatment above $100^{\circ}C$. With the higher aging temperature, the fraction of monoclinic phase increased. The ratio of monoclinic/tetragonal + monoclinic phase reached a plateau value, circa 75% above $175^{\circ}C$. The point of monoclinic concentration at which the flexural strength begins to decrease was between 12% and 54%.

• 비파괴검사학회지
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• 제33권2호
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• pp.147-153
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• 2013

최근 가압경수로형 원전의 가압기 노즐과 안전단 사이의 이종용접부에서 일차수응력부식균열에 대한 건전성 확보가 중요한 관심사항으로 대두되고 있다. 가압기 노즐은 SA508 Gr.3 저합금강이며 안전단은 F316L 스테인리스강으로, 이들 두 재료 사이에 용접재로는 Alloy 82/182가 사용되었다. 재료 결함에 대한 건전성 평가를 위해서는 재료의 기계적 물성치, 특히 인장물성과 파괴물성이 확보되어야 한다. 그러나, 일반적인 재료 규격과 시험성적서에서는 상온의 인장물성이 제공되지만 고온의 인장물성과 파괴인성이 제공되지 않는다. 따라서, 본 논문에서는 상온과 원전 운전온도에서 SA508 Gr.3과 F316L 스테인리스강에 대한 인장시험과 J-R 파괴인성시험을 수행하고 그 결과를 수록하였다.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2010년도 춘계학술발표대회 초록집
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• pp.70-70
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• 2010

In the present study, to estimate the mechanical properties of 800 MPa grade weld metal, welding was carried out using 800 and 600 MPa grade flux cored arc welding (FCAW) consumable and characteristics of the weld metals were investigated. The chemical composition of weld metals was investigated by an optical emission spectroscopy (OES) method. The microstructure of weld metals was analyzed by optical microscopy (OM) and secondary electron microscopy (SEM). The compositions and sizes of inclusions which are the dominant factors for the nuclei of acicular ferrite were analyzed by an transmission electron microscopy (TEM). In addition, mechanical properties of the weld metals were evaluated through tensile tests and charpy impact tests. Mostly the acicular ferrite phase which has high strength and toughness was observed. The 600 MPa grade weld metal was consisted of 75% acicular ferrite and 25% ferrite which was formed at high temperature (grain boundary ferrite, widmanstatten ferrite, polygonal ferrite). However, the 800 MPa grade weld metal was composed of about 73% acicular ferrite and 27% low temperature phase (bainite, martensite). Toughness was considerably decreased due to the increase of tensile strength (from 600 MPa to 800 MPa). The sizes of inclusions which were observed in both weld metal were $0.4{\sim}0.8\;{\mu}m$, it is effective size to form acicular ferrite.

• Journal of Welding and Joining
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• 제17권1호
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• pp.133-144
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• 1999

To fine seam annealer capacity of through thickness seam annealing in terms of through thickness microstructure change with increased toughness and elongation leaving heat trace on it, high strength steel pipes of ERW with different thickness were tested in different seam annealing temperature measured on the outer surface of pipes. Annealing temperature and microstructure of the weld seam were changed through applied seam annealing condition. Toughness and tensile test with hardness and microstructure analysis were done on the annealed weld seam to fine its characteristics as a primary step and annealing characteristics according to different seam annealing condition. Through a study of annealed ERW weld seam characteristics and seam annealing technology, amount of electric power should apply in decreased manner to arranged inductors of annealer in the order of 1st, 2nd, 3rd, so on for proper seam annealing. For example of 15.4mm thick and 610mm outside diameter pipe, applied power for proper seam annealing is 600 -650kw at 1st inductor, 450 - 500kw at 2nd inductor, 200-250 kw at 3rd inductor of annealer during 10 - 12M/minute moving speed of pipe. Also, the penetration depth of heat trace along the thickness direction of weld during seam annealing can be estimated through the equation 17mm/kv$\times$voltage(kv) with the microstructure and hardness analysis of thick weld seam as well as study of seam annealing and comparison of cooling condition to CCT diagram of low carbon high strength steel. From this result, the difference between the technological applicability of full annealing condition based on phase diagram and full penetration of heat trace based on CCT diagram along the thickness of weld seam is discussed.

• 한국재료학회지
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• 제23권9호
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• pp.525-530
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• 2013

This study investigated the continuous cooling transformation, microstructure, and mechanical properties of highstrength low-alloy steels containing B and Cu. Continuous cooling transformation diagrams under non-deformed and deformed conditions were constructed by means of dilatometry, metallographic methods, and hardness data. Based on the continuous cooling transformation behaviors, six kinds of steel specimens with different B and Cu contents were fabricated by a thermomechanical control process comprising controlled rolling and accelerated cooling. Then, tensile and Charpy impact tests were conducted to examine the correlation of the microstructure with mechanical properties. Deformation in the austenite region promoted the formation of quasi-polygonal ferrite and granular bainite with a significant increase in transformation start temperatures. The mechanical test results indicate that the B-added steel specimens had higher strength and lower upper-shelf energy than the B-free steel specimens without deterioration in low-temperature toughness because their microstructures were mostly composed of lower bainite and lath martensite with a small amount of degenerate upper bainite. On the other hand, the increase of Cu content from 0.5 wt.% to 1.5 wt.% noticeably increased yield and tensile strengths by 100 MPa without loss of ductility, which may be attributed to the enhanced solid solution hardening and precipitation hardening resulting from veryfine Cu precipitates formed during accelerated cooling.