• 제목/요약/키워드: liquid-phase

검색결과 4,285건 처리시간 0.031초

신개발 Ni-3Cr-4Si-3B 삽입금속으로 액상확산접합한 내열주강 접합부의 특성 (Characteristics of Liquid Phase Diffusion Bonded Joints Using Newly Developed Ni-3Cr-4Si-3B Insert Metal of Heat Resistant Alloy)

    • Journal of Welding and Joining
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    • 제18권6호
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    • pp.62-67
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    • 2000
  • Metallurgical characteristics of bonded region and high temperature mechanical properties of heat resistant alloy, Fe-35Ni-26Cr during liquid phase diffusion bonding were investigated employing AM17 insert metal. The insert metal for bonding, AM17 was newly developed Ni-base metal using interpolation method. Bonding of specimens were carried out at 1,403~1,463K for 600s in vacuum. The microconstituents in the bonded interlayer disappeared in the bonding temperature over 1,423K. The microstructures, alloying elements and hardness distribution in the base metal. The tensile strength and elongation of the joints at elevated temperatures were the same level as one of the base metal in the bonding temperature over 1,423K. The creep rupture strength and rupture lives of joints were almost identical to those of base metal.

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Liquid-phase epitaxy로 성장시킨 A $I_x$Ga${1-x}$As(x.<=.0.15)의 photoreflectance (Photoreflectance of A $I_x$Ga${1-x}$As(x.<=.0.15) grown by liquid-phase epitaxy)

  • 배인호;김인수;이철욱;최현태;김말문;김상기
    • E2M - 전기 전자와 첨단 소재
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    • 제7권4호
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    • pp.300-305
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    • 1994
  • We determined the alloy composition of the liquid-phase epitaxy(LPE) grown $Al_{x}$G $a_{1-x}$ As by the photoreflectance(PR), and observed the variation of PR signal by changing the condition of annealing and thickness of epilayer. As the measuring temperature was decreased, the broadening parameter was decreased, and the amplitude of PR signal was increased. When the temperature of annealing was increased, the surface carrier concentration was decreased and then the shape and amplitude of PR signal were affected by the surface electric field. The structure change was observed when the specimen was annealed for long time at a high temperature. We found that the surface electric field increased when the thickness of epilayer was decreased by etching, because the band bending was increased by the decreased of the width of depletion layer....

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EGR율 변화에 대한 액상 LPG분사 엔진의 운전 및 배출가스특성 (Performance and Emission Characteristics of Liquid-Phase LPG Injection Engine with Different EGR Rate)

  • 염기태;우영민;장진영;박용국;배충식
    • 한국자동차공학회논문집
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    • 제11권5호
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    • pp.7-14
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    • 2003
  • Exhaust Gas Recirculation (EGR) system is used to reduce NOx emission, to improve fuel economy, and to suppress knock since it offers the benefits of the inlet charge dilution. The effects of EGR was investigated on the performance and emission to reduce exhaust thermal load with a single cylinder liquid-phase LPG injection engine, in a wide range of EGR rate, engine conditions and LPG proportions. As EGR rate was increased, NOx was reduced while HC was increased. Pumping loss reduction by EGR improved bsfc and increased EGR lowered exhaust gas temperature. And, LPG proportions were made a difference on the performance and emission characteristics.

Effect of Crystal Shape on the Grain Growth during Liquid Phase Sintering of Ceramics

  • Jo, Wook;Hwang, Nong-Moon;Kim, Doh-Yeon
    • 한국세라믹학회지
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    • 제43권11호
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    • pp.728-733
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    • 2006
  • The equilibrium or growth shape of ceramic materials is classified largely into two categories according to the thermodynamic conditions imposed. One is a polyhedral shape where the surface free energy is anisotropic, and the other a spherical shape where the surface free energy is isotropic. In the case of grains with a polyhedral shape of anisotropic surface free energy, socalled abnormal grain growth usually takes place due to a significant energy barrier for a growth unit to be attached to the crystal surface. In the case of grains with a spherical shape of isotropic surface free energy, however, normal grain growth with a uniform size distribution takes place. In this contribution, the state-of-the-art of our current understanding of the relationship between the crystal shape and the microstructure evolution during the sintering of ceramic materials in the presence of a liquid phase was discussed.

LPE 성장법으로 성장시킨 La 을 첨가한 YIG 막의 자성특성 (Magnetic Properties of La-doped YIG films prepared by LPE(Liquid Phase Epitaxy))

  • 김동영;한진우;김명수;이상석
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 추계학술대회 논문집
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    • pp.89-92
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    • 2000
  • Liquid Phase Epitaxy 법을 이용하여 La이 첨가된 YIG(Yitrium Ion Garnet)막을 성장시켰다. X선 회절 분석을 이용하여 La의 첨가량을 변화시키며 제조된 막의 격자상수를 조사한 결과, La의 첨가량이 증가함에 따라 성장된 막의 격자상수도 증가하였으며 Y/La이 20인 경우, 막의 격자상수가 기판으로 사용한 GGG의 격자상수와 일치하였다. VSM(Vibration Sample Magnetometer)를 이용하여 구한 막의 포화자화 값은 La의 첨가량과 관계없이 순수한 YIG의 경우와 같은 값인 1750정도로 거의 일정하였다. FMR(Ferro Magnetic Resonance) 측정장치를 이용한 막의 강자성 공명선폭을 측정결과 막의 공명선폭은 La의 첨가량과 관계없이 모든 경우에 순수한 YIG보다 감소하였다. 실험범위내의 La의 첨가에 대해서 기판과의 격자불일치가 순수한 YIG의 경우보다 감소하기 때문이다. La의 첨가량이 많은 조건에서 성장시킨 막은 공명선폭이 크고 두께의 증가에 따라서 선폭이 증가하였으며, Y/La가 20과 30일 때 성장시킨 막에서는 공명선폭의 절대값도 작고 두께에 따른 공명선폭의 변화도 관찰되지 않았다.

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액상환원법에 의한 저온 열처리용 Ag 나노분말의 합성 (Synthesis of Ag Nanopowder for Low Temperature Heat Treatment Prepared by Liquid Phase Reduction Method)

  • 이종국;최남규;송대성;양권승;서동석
    • 열처리공학회지
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    • 제18권4호
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    • pp.242-246
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    • 2005
  • Silver nanoparticles were synthesized by liquid phase reduction method from aqueous silver nitrate solution and borohybride as a reduction agent. The morphology, particle size and shape were influenced by the reaction conditions such as the concentration of $AgNO_3$, a reduction agent and addition of surfactant. The particle size decreased with decreasing the concentration of silver nitrate and using a borohydride. The obtained Ag particles showed the spherical shape with the range of 10-20 nm.

$Ni/\gamma -Al_2O_3$ Catalyst Prepared by Liquid Phase Oxidation for Carbon Dioxide Reforming of Methane

  • 정경수;조병율;이호인
    • Bulletin of the Korean Chemical Society
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    • 제20권1호
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    • pp.89-94
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    • 1999
  • Carbon dioxide reforming of methane on Ni/γ-Al2O3 catalyst was studied. A new 10 wt% Ni/γ-Al2O3 catalyst prepared by the liquid phase oxidation method (L10O) exhibited much higher activity as well as resistances to both sintering and coke formation during the reaction than the catalyst prepared by the conventional impregnation method (D10). The electrically strong attractive interaction between nickel and support during the liquid phase oxidation process and the resultant high nickel dispersion made the L10 have superior activity and stability to the D10. To elucidate the results, the experiments with nickel catalysts on the other supports as well as 7-AI203 were performed. The effect of sodium as a promoter was also studied.

Liquid Crystal Spatial Light Phase Modulator and its Applications

  • Hara, Tsutomu
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2002년도 International Meeting on Information Display
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    • pp.939-942
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    • 2002
  • The optically addressed and electrically addressed spatial phase only light modulators without pixelized structures have been developed. A sufficient phase modulation capability and a high diffraction efficiency of these devices are useful for practical applications.

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피부장벽에 대한 Bio-Mimic Liquid Crystal Emulsion (BLCE)의 긍정적 효과에 관한 연구 (Study on the beneficial effect of Bio-Mimic Liquid Crystal Emulsion (BLCE) on Skin Barrier Function)

  • 안영훈;배순민;정진교;황정근
    • 대한화장품학회지
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    • 제33권4호
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    • pp.227-230
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    • 2007
  • 최근 기능성화장품과 피부관련 의약품 분야에서 multi-lamellar와 liquid crystal의 구조가 커다란 관심을 끌고 있다. 결합수와 고정된 유상을 함유하는 multi-lamellar 구조는 피부의 세포간지질의 lamellar 구조의 재건과 보습을 유지하는 작용으로써 보습기능이나 장벽기능의 복구에 우수하며, 이 지질들은 각질층에 침투하여 유지된다. 본 연구에서 고급 지방 알코올, 레시틴, 콜레스테롤을 사용하여 제조한 bio-mimic liquid crystal emulsion (BLCE)의 피부장벽 기능을 측정하였고 일반적인 계면활성제와 세포독성을 비교하였다.

Mobile Phase Compositions for Ceramide III by Normal Phase High Performance Liquid Chromatography

  • Hong, Seung-Pyo;Lee, Chong-Ho;Kim, Se-Kyung;Yun, Hyun-Shik;Lee, Jung-Heon;Row, Kyung-Ho
    • Biotechnology and Bioprocess Engineering:BBE
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    • 제9권1호
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    • pp.47-51
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    • 2004
  • Ceramide III was prepared by the cultivation of Saccharomyces cerevisiae. Ceramide III was partitioned from the cell extracts by solvent extraction and analyzed by Normal Phase High Performance Liquid Chromatography (NP-HPLC) using Evaporative Light Scattering Detector (ELSD). We experimentally determined the mobile phase composition to separate ceramide III with NP-HPLC. Three binary mobile phases of n-hexane/ethanol, n-hexane/lsoprophyl Alcohol(IPA) and n-hexane/n-butanol and one ternary mobile phase of n-hexane/IPA/methanol were demonstrated. For the binary mobile phase of n-hexane/ethanol, the first mobile phase composition, 95/5(v/v), was step-increased to 72/23(v/v) at 3 min. In the binary mobile phase, the retention time of ceramide III was 7.87min, while it was 4.11 min respectively in the ternary system, where the mobile phase composition of n-hexane/IPA/methanol, 85/7/8(v/v/v), was step-increased to 75/10/15(v/v/v) at 3 min. However, in the ternary mobile phase, the more peak area of ceramide III was observed.