• Journal of the Korean Society of Tobacco Science
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• v.25 no.2
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• pp.144-153
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• 2003

This study was carried out to determine the relationship between smoke components and sensory evaluation by changes tobacco leaf blending. Seven different cigarettes were made by adding different types of oriental, reconstituted and expanded tobacco leaves. 62 kinds of smoke components which were 6 of general components, 34 of semi-volatile and volatile components, 9 of acid components, and 13 of phenolic components were analyzed. Eight kinds of sensory item were evaluated and also electronic nose system data was collected. All smoke components and sensory characteristics of mainstream smoke were changed by the different blending. To determine the relationship between smoke components and sensory test, the correlation and regression analysis were carried out by using SPSS statistical program. Tar, pH, and CO showed a high correlation with sensory evaluation item. As tar related to hotness, CO have a high correlation with offensive aroma. Semi-volatile and volatile components of smoke related to sensory characteristics such as aroma, taste, irritation, hotness and smoothness. When propylene, l,3-butadiene, butane, isoprene, and 2-methylfuran showed a high correlation with aroma; methyl chloride, methanol, toluene, ethyl benzene showed a high correlation with irritation. Some acidic components and phenolic components of smoke also had a high relation to smoke volume. Especially the acidic components such as 2-furoic acid, 2-hydroxybutyric acid, phenylacetic acid and palmitic acid; the phenolic components such as 4-vinyl phenol, pyrocatechol, 3-methyl catechol, hydroquinone showed a high correlation with smoke volume. As using regression analysis, it was possible to estimate the results of sensory evaluation from the smoke analysis data. From the results of electronic nose system analysis, we can find the different pattern by adding expanded tobacco leaf.

• Journal of the Korean Society of Tobacco Science
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• v.27 no.1 s.53
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• pp.141-152
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• 2005

This study focused on the relationships among leaf and smoke components and sensory properties following tobacco leaf blending. A completely randomized experimental design was used to evaluate components of leaf and smoke and sensory properties for sample cigarettes with four mixtures of flue cured and burley tobacco (40:60, 60:40, 80:20 and 100:0). Eleven leaf components, six smoke components, and eight sensory properties of smoking taste were analyzed. A sensory evaluation method known as quantitative descriptive analysis was used to evaluate perceptual strength on a fifteen score scale. Raw data from ten trained panelists were obtained and statistically analyzed. Based on the MANOVA, clustering analysis, correlation matrix and partial least square (PLS) method were applied to find out which smoke component most affected sensory properties. The PLS method was used to remove the influence between explanatory variables in the leaf, smoke components derived from the results. High correlations (p<0.0l) were found among ten specific leaf and smoke components and sensory attributes. Total nitrogen, ammonia, total volatile base, and nitrate in the leaf were significantly correlated (p<0.05) with impact, bitterness, tobacco taste, irritation, smoke volume, and smoke pungency. From the results of PLS analysis, influence variables are used to explain about the correlation. In terms of bitterness, with only two explanatory variables, Leaf $NO_3$ and Leaf crude fiber were enough for guessing their correlation. In the distance weighted least square fitting analysis, carbon monoxide highly influenced bitterness, hay like taste, and smoke volume.

• Journal of the Korean Society of Tobacco Science
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• v.28 no.2
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• pp.83-93
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• 2006

The aim of this study is to develop a simple and rapid field method for the determination of chloride content in tobacco green or cured leaves. To set up a practical process, several factors such as the proper sampling position of each leaf, the size of leaf lamina pieces for blending, the substitution of deionized water fur the extracting solution, 0.1N $HNO_3$, the submerging durations before blending, and the standing times before measuring were studied using flue-cured and burley tobacco with a stable and reproducible Chloride Meter, KRK CL-2Z. From the results, chloride contents of tobacco leaves could be analyzed with the Chloride Meter(CL-2Z) using the suspension of 14 mm diameter leaf disks after soaking in distilled water for 30 min., blending with a mini-blender for 30 seconds. The chloride contents measured in this way showed highly significant correlations with ones by the conventional potentiometric method using an ion meter-chloride electrode and $AgNO_3$ titration. In our method, the procedures such as drying, powdering and weighing samples, and using chemical reagents for extraction (0.1N $HNO_3$) and titration(0.028N $AgNO_3$) could be eliminated. These results suggest that the newly constructed method using the Chloride Meter is more efficient to determine the chloride content of tobacco leave in comparison with the one by the Ion $Meter:AgNO_3$ titration.

• Journal of the Korean Society of Tobacco Science
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• v.24 no.1
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• pp.21-26
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• 2002

This study was carried out to evaluate the effect of forced fermentation on chemical and sensory properties in burley leaf tobacco. Three process steps of burley leaf tobacco(green and redried leaves produced in 2000, and aged leaves in 1998) and four grades(BlT, B2T, C1W and C2W) of leaf for every step were used in this study. The leaves were moistened by 22% moisture content, packed under 200kg/㎥ condition and stored in chamber controlled 6$0^{\circ}C$ and 90% R.H. for 7 days. Nicotine contents in three steps of burley leaf tobacco were significantly decreased by forced fermentation. Except for aged leaf, pH values of green and redried leaves were significantly lowered. Nicotine, tar and CO contents of cigarette smoke showed little difference between cigarettes containing 23%, 26% and 29% of fermented burley leaf and controlled cigarette(containing 19% of aged burley leaf). The cigarette containing 26% of the redried and fermented leaf was significantly better taste and less irritation than controlled cigarette. The results suggest that the forced fermentation may be useful to increase the rate of burley tobacco in leaf blending and to shorten the period of storage for aging.

• Journal of the Korean Society of Tobacco Science
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• v.28 no.1
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• pp.31-35
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• 2006

In this study, the effects of the relative humidity and storage time of blended tobaccos at total blending silo on cut tobacco equilibrium moisture contents, leaf moisture contents and migration of casing materials of tobacco types were investigated. To maintain the cutting moisture content(21 $\pm$ 1 %), it is necessary to keep 75 % relative humidity at 28 $^{\circ}C$ at total blending silo. The moisture content of reconstituted tobacco sheet was changed from $13{\sim}14$ % to $19{\sim}21$ % within 2 h after preblending. The contents of glycerin and fructose of tobacco types followed by storage time after preblending were not changed significantly. From these results, it is suggested that 2 h storage time after preblending was sufficient to maintain physical properties of cut tobaccos and tobacco taste and fragrance.

• Proceedings of the Korean Society of Tobacco Science Conference
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• 2004.05a
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• pp.35-36
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• 2004

• Journal of the Korean Society of Tobacco Science
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• v.33 no.1
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• pp.28-38
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• 2011

This experiment was conducted as a part of Asia collaborative study on purpose of verifying the difference between CM6 and CM7 including 3R4F for reference. It carried out using various analytical categories for example, main stream, sidestream and Av. smoke. Additional analysis such as physical properties, blending ratio, combustibility and general leaf component analysis also implemented in order to investigate the difference. We complied with ISO standard and CORESTA recommended method during analytical operating procedures. In this study, we described that comparative analytical result for CM6 and CM7 known as reference or monitoring cigarettes including 3R4F for reference. All sample cigarettes were conditioned at $22^{\circ}C$, 60% relative humidity for 48 hours. Av. Smoke, MS and SS smoke analysis were performed over five times with two smoking condition, ISO and Health Canada with the exception of Av. smoke analysis. We complied with ISO standard method during analytical operating procedures. And, we conducted additional analysis, such as physical properties, blending ratio, combustibility and leaf component analysis also in order to investigate the difference. In conclusion, we found out some differences between CORESTA monitoring cigarette No. 6 and No 7. The smoke components such as total particulate matters, NFDPM, nicotine and carbon monoxide contents of CM7 were a little lower than CM6. And, these phenomena were the same as not only main stream smoke but also side stream smoke and Av. smoke. This tendency was consistent with ISO and Health Canada smoking condition. Besides, leaf constituents' color of CM7 was darker than CM6. In case of combustibility, it showed short combustion time approximately 30 seconds.

• Journal of the Korean Society of Tobacco Science
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• v.28 no.1
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• pp.1-8
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• 2006

To get the information of flue-cured leaf, the chemical constituents, quality indices, leaf color and the effects of climatic factors on the physicochemical properties of leaf produced from 2000 to 2004 crop years at 6 growing areas were analysed. The average leaf chemical contents for 5 years were as follows ; nicotine 2.22%, total sugar 28.0%, total nitrogen 1.89%, ether extracts 6.37% and chlorine 0.38%. The nicotine and total nitrogen contents were low while the total sugar were high as compared with KT&G recommended contents(nicotine ; $2.5{\sim}3.0%$, total nitrogen; $2.0{\sim}2.5%$, total sugar ; below 25.0%). The variations of physicochemical properties among crop years were high while those of growing areas relatively low. The nicotine content of leaf was negatively correlated to the rainfalls in June and July sugar content was negatively correlated to the average air temperature in June and July according to crop years. The orange colored leaves were produced under the drought and long sunshine weather condition while the lemon colored leaves were produced under the contrary condition according to crop years. Blending the different crop year's leaves in the proper way may be beneficial to produce of uniform and consistent cigarettes. It is considered that the increasing of nitrogen fertilizer or improving of nitrogen uptake may be available to increase the nicotine and nitrogen and decrease the total sugar contents of flue-cured leaf tobacco.

• Journal of the Korean Society of Tobacco Science
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• v.21 no.2
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• pp.128-135
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• 1999

This study was conducted to determine the sidestream smoke concentration, nicotine, tar, and CO, by the characteristics of tobacco leaves and their combinations. 20 kinds of tobacco leaves and 15 types of their combinations were selected for this study. After collecting the sidestream smoke by fishtail chimney, the concentrations of nicotine, tar, and CO in sidestream smoke were analyzed. Variation in nicotine concentration of sidestream smoke among tobacco leaves and their combinations was as much as 9-times. Heavy leaves and burley leaves were higher in nicotine concentration than light leaves and flue-cured leaves, respectively, the reconstituted tobacco leaf had the minimum concentration of nicotine. Tar concentration of sidestream smoke also was changed by the characteristics of tobacco leaves and their combinations. As the american C4F had the maximum concentration of tar in sidestream smoke, the reconstituted tobacco leaf showed the minimum concentration. Blending 50 % flue-cured B1-0 plus 50% burley B1-T grade showed the highest value in the nicotine concentration. Also, in case of adding B3K and izmir tobacco leaves, the nicotine concentration was decreased. The tar concentration in the sidestream smoke increased as increasing the amount of flue-cured heavy leaf. The CO concentration was not so much Changed by the characteristics of tobacco leaves and their combinations.

• Journal of the Korean Institute of Landscape Architecture
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• v.27 no.3
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• pp.109-113
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• 1999

The objective of this research was to develop growth media for artificial ground by blending calcined clay and coconut peat. To achieve this, aggregates of clay particles were mixed with disel oil and heated to high temperature(1150~120$0^{\circ}C$) to expand clays. The particle sizes of expanded clay were controlled to 2~5mm in diameter. Then expanded clayes were mixed with coconut peat and changes of soil physicochemical properties and their effect on plant growth of Hedera L. were determined. The infiltration rate of calcined clay was very high, but the water holding capacity, the cation exchange capacity(CEC), and the nutrient contents were low. The characteritics of coconut peat was vice verse to calcined clay. This indicates that the mixture of calcined clay and coconut peat have the better characteristics than each material. As compared to mineral soil, the infiltration rate, the water holding capacity, the CEC and the nutrient contents increased, but bulk density decreased to about 1/4. And, Hedera L. grown in the mixture of calcined clay and coconut peat(6:4, v/v) had higher plant height, longer leaf length, more total number of leaves per plant and fresh weight than that grown in mineral soil, but statistical differences were not observed between two treatments.