• 제목/요약/키워드: laboratory measurement methods

검색결과 435건 처리시간 0.033초

Role of span length in the adaptation of implant-supported cobalt chromium frameworks fabricated by three techniques

  • Zhou, Ying;Li, Yong;Ma, Xiao;Huang, Yiqing;Wang, Jiawei
    • The Journal of Advanced Prosthodontics
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    • 제9권2호
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    • pp.124-129
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    • 2017
  • PURPOSE. This study evaluated the effect of span length on the adaptation of implant-supported cobalt chromium frameworks fabricated by three techniques. MATERIALS AND METHODS. Models with two solid abutment analogs at different inter-abutment distances were digitized using a laboratory scanner. Frameworks of two-, three-, and four-unit fixed prostheses were designed by a computer. Six dots with a diameter of 0.2 mm were preset on the surface of each framework. A total of 54 implant-supported cobalt chromium frameworks were fabricated by milling, selective laser melting (SLM), and cast techniques. The frameworks were scanned and exported as Stereolithography files. Distances between two dots in X, Y, and Z coordinates were measured in both the designed and fabricated frameworks. Marginal gaps between the framework and the abutments were also evaluated by impression replica method. RESULTS. In terms of distance measurement, significant differences were found between three- and four-unit frameworks, as well as between two- and four-unit frameworks prepared by milling technique (P<.05). Significant differences were also noted between two- and three-unit frameworks, as well as between two- and four-unit frameworks prepared by cast technique (P<.05). The milling technique presented smaller differences than the SLM technique, and the SLM technique showed smaller differences than the cast technique at any unit prostheses (P<.05). Evaluation with the impression replica method indicated significant differences among the span lengths for any fabrication method (P<.05), as well as among the fabrication methods at any unit prostheses (P<.05). CONCLUSION. The adaptation of implant-supported cobalt chromium frameworks was affected by the span length and fabrication method.

Tag 개방식 장치를 이용한 tert-Pentanol+n-Decane 계의 하부인화점 측정 (The Measurement of Lower Flash Point for tert-Pentanol+n-Decane System Using Tag Open-Cup Tester)

  • 하동명;이성진
    • 한국가스학회지
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    • 제16권5호
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    • pp.41-46
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    • 2012
  • 인화점은 공기 속 가연성 증기의 농도가 연소하한계(lower flammability limit)에 도달할 때의 최저 온도이며, 산업현장에서 사용하는 물질들의 화재와 폭발의 위험성을 결정하는 중요한 물성치이다. 단일 성분의 인화점 정보는 여러 문헌에서 얻을 수 있으나, 이성분계 혼합물의 인화점은 충분히 제공되어 있지 않다. 본 연구에서는 tert-pentanol+n-decanel 계의 인화점을 Tag 개방식 장치를 이용하여 측정하였다. 실험값은 Raoult의 법칙과, Wilson 식과 NRTL 식을 활용한 최적화 기법에 의해 계산된 값들과 비교되었다. 최적화 기법에 의한 계산값이 Rauolt의 법칙에 의한 계산값 보다 실험값에 더욱 근접하였다.

NIOSH5040, IMPROVE_A, EUSAAR2을 이용한 탄소 분석 결과 비교 (Intercomparison of Carbonaceous Analytical Results using NIOSH5040, IMPROVE_A, EUSAAR2 Protocols)

  • 오세호;박다정;조지혜;한영지;배민석
    • 한국대기환경학회지
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    • 제34권3호
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    • pp.447-456
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    • 2018
  • Elemental carbon (EC) and organic carbon (OC) thermal/optical methods for the analysis of ambient particulate matter were used to analyze twenty-two $PM_{2.5}$ samples along collected from May 28 to June 20 of 2016 at the Anmyeon measurement site ($36.32^{\circ}N$; $126.19^{\circ}E$). The three laboratory OCEC protocols, which are the National Institute of Occupational Safety and Health (NIOSH5040), the Interagency Monitoring of Protected Visual Environments_A(IMPROVE_A), and European Supersites for Atmospheric Aerosol Research2 (EUSAAR2), were utilized for the aerosol characterization experiment as in intercomparisons between three protocols. There are excellent agreement for total carbon (i.e. sum of EC and OC), but statistically significant differences were observed in the split between the measured EC and OC. IMPROVE_A EC values were always larger than both NIOSH5040 and EUSAAR2 protocols. These methods exhibited significantly different temperature-distributions based on thermogram analysis, which is normalized to total carbon. In this study, a protocol for carbonaceous analysis is suggested for the Korean Peninsula.

비파괴기법을 이용한 철근 콘크리트 벽체 철근의 부식률 예측기법 (Corrosion Level Measurement Technique for RC Reinforcement Using Non-Destructive Test Methods)

  • 노영숙
    • 비파괴검사학회지
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    • 제31권1호
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    • pp.24-31
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    • 2011
  • 콘크리트 벽체 구조물에 매입된 철근의 정량적인 부식률을 측정하기 위하여 자연전위 측정법과 적외선 열화상법을 이용하였다. 벽체 실험체는 부식률(0, 1, 3, 5, 7%)과 피복 두께(30 mm, 40 mm), 그리고 철근 배근 간격에 변수를 주어 콘크리트 표면에서 저항 및 전류를 측정하고 온도를 측정하였으며, 콘크리트 표면 상태에서 얻은 결과를 분석하여 다음과 같은 결론을 얻었다. 전류밀도 분포는 부식률이 증가할수록 그값이 증가하였으며 피복 두께가 클수록 분포도가 넓게 나타났다. 적외선 촬영으로 얻어진 열화상 정보는 서로 다른 부식률과 피복 두께에서는 현저한 차이를 보였으며 주변 온도 및 철근 배근 간격에 대해서는 그 영향이 미비하게 나타났다. 제시된 부식 모델을 통해서 콘크리트 표면의 전류나 온도를 측정하여 내부에 매입되어 있는 철근의 부식률을 정량적으로 측정할 수 있는 것으로 나타났다.

1액형 광촉매를 아스팔트 포장에 적용하기 위한 기초연구 (Fundamental Study on Applying an Integral TiO2 Solution to Asphalt Pavement)

  • 박재영;김영;김혁중;황용경;이재준
    • 한국도로학회논문집
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    • 제19권1호
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    • pp.53-62
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    • 2017
  • PURPOSES : This research was a fundamental study on the application of an integral $TiO_2$ solution to asphalt concrete pavement. The integral $TiO_2$ solution was produced in pilot production equipment; application of the integral $TiO_2$ solution to asphalt pavement was conducted to examine the pollution-reducing capability of photocatalytic compounds such as $TiO_2$. The photocatalytic $TiO_2$ reacted with air pollutants, converting them into small amounts of relatively benign molecules. METHODS : In this study, laboratory experiments were conducted using five various testing methods. Tensile strength ratio (TSR) and British pendulum test (BPT) were conducted in order to evaluate the properties of asphalt pavement subsequent to the integral $TiO_2$ solution coating. In addition, methylene blue testing, a measurement of nitrate on the coated pavement, and nitrogen oxide (NOx) reduction testing were conducted in order to evaluate photocatalytic reaction. Lastly, a UV-A lamp was used as a light source for photocatalytic reactions. RESULTS : Test results indicated no change in the properties of asphalt pavement following the integral $TiO_2$ solution coating. In order to evaluate the performance of asphalt pavement as a function of $TiO_2$, the moisture susceptibility and skid resistance were investigated. The moisture susceptibility and skid resistance satisfied there quirements related to pavement quality and safety specification. Furthermore, the effects of reduction of air pollution were significantly improved as determined via the methylene blue test and NOx reduction test. The $TiO_2$-paved asphalt specimen exhibited approximately 43% reduction of NOx. CONCLUSIONS : This study has suggested that applying $TiO_2$ rarely impacts asphalt pavement performance measures such as moisture susceptibility and skid resistance, and that its application may be a better means of reducing air pollution. Further studies, such as proper $TiO_2$ dosage rates and compatibility with various pavement types, are required to broaden and generalize its application.

Review on Rice Flour Manufacturing and Utilization

  • Kim, Myoung Ho
    • Journal of Biosystems Engineering
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    • 제38권2호
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    • pp.103-112
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    • 2013
  • Background: The Korean government launched a project in 2008, where the amount of rice used as raw ingredient in rice-based foods in 2012 was planned to increase up to 10% (470,000 ton) of the total rice production through developing various new rice-based processed foods and their commercial manufacturing technology. Among the four major rice-based processed foods, rice cakes and noodles need rice flour as their main raw ingredient. Technology in rice flour utilization and manufacturing is far behind than the technology pertinent to wheat flour in many subject areas. Purpose: This review aims to provide information on rice flour utilization and manufacturing with some fundamental subjects in the area of size reduction. Results: A variety of food items including bread, noodle, cake, cookie, muffin, pre-mix, beverage, vinegar, surimi, and artificial meat have found rice flour as their raw ingredient. Rice bread made out of 100% rice flour has been developed and is now sold in retail stores. Various noodle products made from rice flour are also on the market. Issues on product definition and labeling regulation about rice flour content of the products were explored. Generalized grinding equations available in the literature were seldom used in practice; instead, it has been a general practice to develop empirical equations from test milling data. Introductory remarks on three popular particle size measurement methods (sieving, Coulter counter, light diffraction) were explained. Mathematical expressions frequently used to describe particle size distribution and to correlate cumulative quantity of particles with particle size were represented. Milling methods used in producing rice flour were described along with their advantages and disadvantages. Because of their profound effect on functional properties of the rice flour, four rice flour milling equipments used at both laboratory experiments and commercial manufacturing plants were discussed.

The detection of cavitation in hydraulic machines by use of ultrasonic signal analysis

  • Gruber, P.;Farhat, M.;Odermatt, P.;Etterlin, M.;Lerch, T.;Frei, M.
    • International Journal of Fluid Machinery and Systems
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    • 제8권4호
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    • pp.264-273
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    • 2015
  • This presentation describes an experimental approach for the detection of cavitation in hydraulic machines by use of ultrasonic signal analysis. Instead of using the high frequency pulses (typically 1MHz) only for transit time measurement different other signal characteristics are extracted from the individual signals and its correlation function with reference signals in order to gain knowledge of the water conditions. As the pulse repetition rate is high (typically 100Hz), statistical parameters can be extracted of the signals. The idea is to find patterns in the parameters by a classifier that can distinguish between the different water states. This classification scheme has been applied to different cavitation sections: a sphere in a water flow in circular tube at the HSLU in Lucerne, a NACA profile in a cavitation tunnel and two Francis model test turbines all at LMH in Lausanne. From the signal raw data several statistical parameters in the time and frequency domain as well as from the correlation function with reference signals have been determined. As classifiers two methods were used: neural feed forward networks and decision trees. For both classification methods realizations with lowest complexity as possible are of special interest. It is shown that two to three signal characteristics, two from the signal itself and one from the correlation function are in many cases sufficient for the detection capability. The final goal is to combine these results with operating point, vibration, acoustic emission and dynamic pressure information such that a distinction between dangerous and not dangerous cavitation is possible.

동영상 촬영방식의 구강스캐너로 채득된 전악치열 디지털모형의 정확도 분석 : CS-3600 시스템을 중심으로 (Accuracy of full arch digital model obtained from rendering-based intraoral scanner(IOS) : An example of CS-3600 system)

  • 김재홍
    • 대한치과기공학회지
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    • 제42권1호
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    • pp.17-25
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    • 2020
  • Purpose: The purpose of this study was to evaluate and compare the accuracy of definitive casts that are fabricated from digital intraoral impression and conventional impression technique. Methods: A master model(ANNA-4, Frasaco GmbH, Tettnang, Germany) with the prepared upper full arch tooth was used. Conventional impression and then stone model(n=10) were produced from this master model, and on the other hands, digital impressions were made with the CS-3600 intraoral scanner(n=10). Six linear measurements were recorded between landmarks, directly on each of the stone models on two occasions by a single examiner. Measurements were made with a digital caliper to the nearest 0.01mm from manual models and with the software(Delcam PowerSHAPE) from the virtual models. The t-student test for paired samples and intraclass correlation coefficient(ICC) were used for statistical analysis. Results: The measurement of two methods showed good reliability. The ICC of the two models were 0.88~0.91(stone model) and 0.94~0.99(digital model). The mean differences to master model for stone model and digital model were 0.10~0.14mm, and 0.14~0.20mm, respectively. Conclusion: The definitive casts obtained with digital intraoral technique model had significantly larger dimensions as compared to those of the stone model. However, the differences to the master model detected appear to provide enough accuracy and reliability for clinical application.

에스트라디올 유도체의 합성, 표지 및 체내동태에 관한 연구 (A Study on the Synthesis, Labeling and Its Biodistribution of Estradiol Derivatives)

  • 김상욱;양승대;서용섭;전권수;안순혁;임수정;최창운;임상무;김영순;유국현
    • 대한핵의학회지
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    • 제34권5호
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    • pp.403-409
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    • 2000
  • 목적: 에스트로겐 수용체의 불균질 분포와 시간 변화에 따른 수용체 상태의 변화 때문에 조직검사를 통한 에스트로겐 수용체의 생화학적 측정은 유방암을 진단하기에 충분하지 못한 단점이 있다. 이런 단점을 개선하고 좀더 나은 유방암의 진단을 위하여 E-$[^{123}I]$IVE에 대하여 연구하였다. 본 연구에서는 에스트로겐 수용체 양성 유방암 환자의 영상을 얻기에 적합한 방사성 추적자를 개발 하였다. 대상 및 방법: 여러 가지 에스트라디올 유도체 중에서 $17{\alpha}$-ethynyl estradiol로부터 $17{\alpha}-[^{123}I]$iodovinyl estradiol ($[^{123}I]$IVE)을 합성하였다. E-$[^{123}I]$IVE는 peracetic acid와 $[^{123}I]$NaI를 이용하여 합성하였고, Z-$[^{123}I]$IVE는 chloramine-T/HCl과 $[^{123}I]$NaI로 합성하였다. 표지수율은 TLC-scanner를 이용해 측정하였으며, 방사 화학적 순도는 HPLC로 측정하였다. E-$[^{123}I]$IVE의 체내 동태 연구는 immature female Fisher rate를 사용해 60분, 120분 그리고 300분에 측정하였다. 결과: E-$[^{123}I]$IVE와 Z-$[^{123}I]$IVE의 표지수율은 각각 92%와 94%이었고, 정제 후 방사 화학적 순도는 98% 이상이었다. E-$[^{123}I]$IVE의 최고섭취는 uterus에서 주사 120분 후에 관찰되었다(3.11%ID/g). 결론: 이상의 결과를 종합해 볼 때 E-$[^{123}I]$IVE는 유방암환자의 에스트로겐 수용체의 존재를 평가하는 진단시약으로서의 사용 가능성을 확인하였다.

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전기비저항을 이용한 확률론적 암반분류 - RMR과 전기비저항 관계 이론 중심으로- (Probabilistic rock mass classification using electrical resistivity - Theoretical approach of relationship between RMR and electrical resistivity-)

  • 류희환;주건욱;조계춘;김경열;임영덕
    • 한국터널지하공간학회 논문집
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    • 제15권2호
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    • pp.97-111
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    • 2013
  • 성공적인 지하공간 건설을 위해서는 주변 암반의 상태를 정확히 파악하는 것이 매우 중요하다. 암반의 상태를 평가하는 방법 중에 대표적인 방법으로는 RMR 방법과 Q-system이 있으며, 설계, 시공, 유지관리 등에 적용되고 있다. 하지만 주관적인 시각과 측정 방법의 정확성 문제에 지속적으로 의문이 제기되어 많은 연구자들이 여러 방법을 통해 암반을 평가하고자 연구를 수행하고 있으나, 대부분의 방법이 국한적으로 지반조사 결과와 암반상태를 상관 맺거나 경향성만 보여주고 있다. 본 논문에서는 절리가 존재하는 암반에서 이론적으로 전기장 해석을 하여 유도된 이론식으로 부터 RMR과 전기비저항의 관계를 도출하였다. 또한, 확률론적 접근을 통해, 보다 신뢰성 있는 RMR과 전기비저항 관계를 획득하였다. 기존에 사용되고 있는 방법과 더불어 제시된 방법을 현장에 적용한다면, 현장에서 RMR을 평가하는데 도움을 줄 수 있을 것으로 판단된다.