• Title/Summary/Keyword: laboratory measurement

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Monitoring of Particulate Matter and Analysis of Black Carbon and Some Particle Containing Toxic Trace in the City of Yaoundé, Cameroon

  • Tchuente, Siaka Y.F.;Saidou, Saidou;Yakum, N.Y.;Kenmoe, N.X.;Abdourahimi, Abdourahimi
    • Asian Journal of Atmospheric Environment
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    • v.7 no.2
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    • pp.120-128
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    • 2013
  • The concentration and composition of particulate matter (PM) in the atmosphere can directly reflect the environmental pollution. The atmospheric pollution in some Cameroonian cities is increasing with the industrial development and urbanization. Air pollution is inherently complex, containing PM of varied size and composition. This PM exists as a dynamic cloud interacting with sunlight and is modified by the meteorology. The reflectometer and the EDXRF spectrometry are applied to determine the concentration of some specific elements at four sites in the city of Yaound$\acute{e}$. The particular aim of the present work is to put in place data base on air pollution in urban area and elaborate regulations on the emissions issued to industrial and vehicle activities. This study provides an overview of the concentration of black carbon and some specific elements in the air, which have impacts on human health. The measurement was done by distinguishing the size of particle. So that, the particle with aerodynamic diameter between $2.5-10{\mu}m$ (so-called coarse particle) and aerodynamic diameter < $2.5{\mu}m$ (so-called fine particle) were considered to obtain more information about levels of the inhalable fraction of the location. The results obtained in four locations of the city of Yaound$\acute{e}$ show that the black carbon concentration is very considerable, the element sulfur is a major pollutant and the concentration of fine particle is very greater. The results obtained of fine and coarse filters range from $5-17{\mu}g/m^3$ and $10-18{\mu}g/m^3$ for the black carbon. S, Cu, Zn, Pb, Cd, As, Se and Hg are the specific findings of this work. The pollutants with a greater concentration are S, Pb, and Zn. These later seem to be non-uniformly, non-regular in some location and high compared to other countries. This work allows us to make a potential relation between pollutants and emission sources. In this framework, some suggestions have been proposed to reduce emissions for an improvement of the air quality in the environment and thus, the one of the city of Yaound$\acute{e}$.

A Study for Qualitative Performance of Asbestos Inspection/Analysis Labs in Korea (국내석면조사기관의 질적 수준 평가를 위한 현황조사)

  • Choi, Sungwon;Kwon, Jiwoon;Baek, Jung Eun;Jang, Kwang Myong;Kim, Dae Jong;Kim, Hyunwook
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.24 no.4
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    • pp.501-508
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    • 2014
  • Objectives: This study identified the general characteristics of asbestos inspection/analysis laboratories in Korea and confirmed the actual situations in terms of technical aspects from these characteristics. In addition, given the background of the current problem, it offers preliminary data for determining future plans for improvement. Methods: A questionnaire was developed and distributed to the asbestos inspection/analysis laboratories that used the ISO/IEC 17025 for asbestos sampling and testing by UKAS(United Kingdom Accreditation Service) and the Korea Laboratory Accreditation Scheme(KOLAS). A total of 202 institutions in Korea were selected for the study and 145(71.8%) questionnaires were returned. Results: The number of personnel of the surveyed institutions averaged $4.2{\pm}2$ and 79.3% operated with less than five persons. In terms of education, the capital and other densely populated areas showed a high level of education(p<0.05). The level of education and facilities were determined by the magnitude of the institution(p<0.05). Institutions managed by highly educated directors were well-stocked with education and facilities(p<0.05). Institutions which had directors with considerable experiences received high scores overall and in particular higher scores in terms of education and facilities(p<0.05). At the level of the bottom five percent, the factor of education was 40.4% while the factor of measurement 49%, the factor of analysis 59%, the factor of facilities 61%, and the factor of survey 81%, respectively. Conclusions: To improve the quality of the institutions, in the short term, the problems identified in this study can be used to revise the related regulations. In the long term, a grading system of survey institutions needs to be established through the introduction of an accreditation system. However, the ongoing support of a government agency is required, including holding seminars and open education, suggesting guidelines for operation of asbestos inspection/analysis labs, and other means.

Fluoroscopic the equipment study in accordance with the entrance surface dose study of patients and practitioners (투시 검사 시 장비에 따른 환자와 시술자의 입사표면선량 연구)

  • Yang, Hae-Doo;Hong, Seon-Sook;Seong, Min-Sook;Ha, Dong-Yoon
    • Korean Journal of Digital Imaging in Medicine
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    • v.15 no.2
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    • pp.13-18
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    • 2013
  • Purpose : Fluoroscopy equipment, depending on the type of changes that occur in the patient's position ESD and study the patient's scatter ray of ESD Practitioners considered a comparative analysis was to evaluate the correct dose. Materials and Methods : HITACHI four overtube type TU-8000 Flat Detector and Under tube C-Arm Philips' Multi Diagnost Eleva with Flat Detector type were measured by. Each devices is a measure of the patient's esd randophantom position in tabel unfors Xi multi funtion then fixed to the abdomen fluoroscopy and 10 seconds, spot was measured three times, practitioners of the incident surface dose by considering the patient's scatter ray of the table for each device in the average human stomach 21cm thickness acrylic phantom ($25cm{\times}25cm$) Place the practitioner position after position randophantom unfors Xi multi funtion in the thyroid and stomach 1 minute by a fixed one-time fluoroscopy and measured. Results : 10 seconds and the patient perspective of the c-arm ESD 1.2 times smaller on the AP and oblique measurements were measured in the 6-13 times smaller. spot positions to changes in the measured three times on the AP of the abdomen, ESD is 18 times smaller c-arm measurements and the oblique measurement was 19-30 times smaller. And 1 minute at practitioners fluoroscopy esd in the thyroid 2.12 times the c-arm, chest 1.75 times less the dose was measured. On the AP, depending on the device, but the lack of dose difference oblique positions of the two devices depending on changes in the area due to changes in both the AP than on the dose increased, the difference in dose between the two devices, the maximum difference was approximately 27 times. Conclusion : Fluoroscopic equipment at the time of inspection in accordance with changes in dose according to the patient and the patient's positions changes, because the area of the scatter ray considering the change of dose measurements be made, and study of the equipment according to the characteristics of the efficiency and the exposure of the patient and practitioner is considered smooth study equipment manufacturers that can be done is to build the system and think that is also important. Various fluoroscopy when you check future changes in many factors of change in dose for the equipment in the laboratory system by considering the scatter ray radiation shielding for the management to take advantage of reckless undertube have been utilized as more exposure Reduction activities can help is considered as the direction.

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Physical Properties of Rocks at the Gagok Skarn Deposit (가곡 스카른광상 암석의 물리적 특성)

  • Shin, Seungwook;Park, Samgyu;Kim, Hyoung-Rae
    • Geophysics and Geophysical Exploration
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    • v.16 no.3
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    • pp.180-189
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    • 2013
  • Geophysical exploration is widely used to develop strategic mineral resources in the world because of its efficient method in detecting mineralized zones in the metallic ore deposit. It is important to understand the physical properties of the stratum so that geophysical data can be more accurately interpreted. This paper is to comprehend physical properties of the rock at the Gagok mine, a typical skarn deposit in Korea. Thus, laboratory tests were conducted on specimens of ore and host rocks which were collected from rock outcrops and drill cores at the Gagok mine. Using the measurement system of rock physical property, we investigated the density, magnetic susceptibility, resistivity, and spectral induced polarization. According to the results, all physical properties of specimens had wide differences depending on contents of ore minerals, which are formed by skarnization. Especially, using the chargeability and time constant from the calculated spectral induced polarization data by the Cole-Cole inversion, we could estimate the volume contents as well as the grain size of the sulfide minerals. Therefore, the spectral induced polarization technique may be considered a useful method when exploring metallic ore deposit with sulfide minerals.

Measurement and Comparison of Morphology of Developmental Stages of Chestnut Weevil, Curculio sikkimensis(Coleoptera: Curculionidae) (밤바구미 (Curculio sikkimensis)의 발육단계별 형태측정 및 비교)

  • Kim, Young-Jae;Moon, Sang-Rae;Yoon, Chang-Mann;Kim, Gil-Hah
    • Korean journal of applied entomology
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    • v.49 no.1
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    • pp.11-16
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    • 2010
  • Measurements were made on morphology of each developmental stages of the chestnut weevil, Curculio sikkimensis, reared in the laboratory and field from 2003 to 2006. The size of egg was 0.8${\pm}$0.03 mm. The escaping larvae were measured, in average, as 98 mg in body weight, 10.65 and 3.99 mm in body length and width, and 1.70 mm in head width. Pupal size of female and male was 7.01 and 6.53 mm, respectively. The fresh weight (0.343 g), body length (7.76 mm) and width (3.38 mm), and head width (1.60 mm) of female adults were significantly bigger than those (0.268 g, 7.14 mm, 3.01 mm and 1.37 mm, respectively) of male adults. Proboscis length (6.53 mm) and antennal length (5.47 mm) of female was also significantly longer than those (3.56 and 4.63 mm, respectively) of male. The larvae of C. sikkimensis overwintered for 1~3 years and their body weight, body length, and body width were decreased. The ratio between proboscis length and body length, the basipodite position attached to the proboscis, and shape of the sex organ on the abdominal end could be used to discriminate sexes.

Development and evaluation of standard samples for quality control of automated total bacterial counter in raw milk (원유 세균수 검사장비의 정도관리를 위한 표준시료의 개발 및 평가)

  • Kang, Hye Jeong;Kim, Jin Hwan;Byun, Yeong Seob;Lee, Hana;Lee, Hye Young;Kim, Jihyeon;Hong, Serim;Kim, Ha-Young;Yoon, Soon-Seek;Moon, Jin-San
    • Korean Journal of Veterinary Service
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    • v.43 no.3
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    • pp.147-154
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    • 2020
  • Standard samples were prepared for this study, and applied for BactoScanTM and BactoCountTM in order for quality control evaluation for total bacterial count in raw milk. Accordingly, the preparation of two lots of standard samples for quality control were lyophilized, which contain Lactobacillus lactis. The standard samples were prepared into three different levels of bacterial counts, those were Low 30,000~40,000, Medium 70,000~90,000, High 150,000~220,000 CFU/mL, respectively. Then, the proficiency tests were performed in total 19 laboratories for measuring total bacterial counts. The total bacterial counts in the standard samples showed 37~42, 82~105, 214~240 CFU/mL in the first lot, and it showed 30~36, 67~75, 131~163 CFU/mL in the second lot in low, medium and high levels, respectively. Based on these results, the absolute values of z-scores of six standard samples in 18 laboratories were ≤2, which means the samples are satisfactory. However, z-score in one laboratory was ≤3, which means the sample is questionable. Using two standard samples, the correlation between BactoScanTM and BactoCountTM was 0.9982, which means the results of total bacterial count measurement of both equipment were equivalent. Therefore, the standard samples manufactured in this study for quality control of total bacterial count using BactoScanTM and BactoCountTM in the raw milk could be applied to proficiency tests.

Reaction Characteristics of Kaolinite-based Additives and Alkali Salts (Kaolinite 계열의 첨가제와 알칼리염의 반응 특성)

  • Jun, HyunJi;Choi, Yujin;Shun, Dowon;Han, Keun-Hee;Bae, Dal-Hee;Rhee, Young-Woo
    • Clean Technology
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    • v.26 no.3
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    • pp.221-227
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    • 2020
  • When the waste solid fuel (SRF, Bio-SRF) is burnt in a boiler, a problem occurs in the combustion process involving the alkali components (Na, K) contained in large amounts in the fuel. The alkaline component has a low melting point, which usually forms low melting point salt in the temperature of the furnace, with the resulting low melting point salts attaching to the heat pipe to form a clinker. Various additives are used to suppress clinker generation, and the additive based on the kaolinite has alkali-aluminum-silica to inhibit the clinker. In this study, the reactivity of the additives based on the kaolinite was compared. The additives utilized were R-kaolinite, B-kaolinite, and A-kaolinite. Also silica and MgO were sourced as the comparison group. The experimental group was employed as a laboratory-scale batch horizontal reactor. The additive and alkaline salts were reacted at a weight ratio of 1 : 1, and the reaction temperature was performed at 900 ℃ for 10 hours. The first measurement of HCl occurring during the experiment was performed 30 minutes after the detection tube was used, and the process was repeated every hour after the experiment. After the reaction, solid residues were photographed for characterization analysis by means of an optical microscope. The reaction characteristics of the kaolinite were confirmed based on the analysis results.

The Strategy for Diagnosis and Treatment of Isovaleric Acidemia (아이소발레릭산혈증의 신생아선별검사 후 진단 및 치료 전략)

  • Ko, Jung Min;Lee, Kyung-A
    • Journal of The Korean Society of Inherited Metabolic disease
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    • v.16 no.2
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    • pp.57-61
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    • 2016
  • Isovaleric acidemia (IVA) is an autosomal recessively inherited organic acid disorder due to a defect of the enzyme isovaleryl-CoA dehydrogenase in the leucine metabolic pathway. Deficiency of this enzyme results in the accumulation of derivatives of isovaleryl-CoA. In acute illness in IVA, isovaleric acid and its derivatives accumulate and profound metabolic acidosis with ketosis, characteristic pungent body odor, hypoglycemia, and hyperammonemia can be developed. Additionally, recurrent vomiting, failure to thrive, developmental delay, epilepsy and mental retardation are chronic presenting symptoms and signs for IVA. On the result of newborn screening for inherited metabolic disorders, increased levels of isovalerylcarnitine (C5) are shown. However, C5 elevation can be accompanied with short/branched-chain acyl-CoA dehydrogenase (SBCAD) and therapy with certain antibiotics containing pivalic acid. Quantitative measurement of organic acids in urine and acylcarnitine profiles in plasma are necessary to differential diagnosis. Molecular genetic analysis of the IVD gene for IVA and ACADSB is also helpful to confirm IVA and SBCAD deficiency, respectively. Considering that IVA can be associated with significant morbidity and mortality at acute presentation of metabolic crisis, early diagnosis prior to the onset of symptoms by newborn screening enable to introduction of early treatment and prevention of acute and chronic complications.

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Behavior of Full Scaled Geobag Retaining Wall Structure by Field Pilot Test (현장실험을 통한 식생토낭 보강토벽의 거동특성에 관한 연구)

  • Shin, Eun-Chul;Park, Kyung-Won;Shin, Hui-su;Ham, Kyung-Won
    • Journal of the Korean Geosynthetics Society
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    • v.16 no.4
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    • pp.21-31
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    • 2017
  • Geobag method is an eco-friendly method to minimize the impact on the environment in the construction of retaining wall structure as a kind of geosynthetic reinforced retaining walls. In this study, evaluated behavior of full scaled geobag retaining wall about four different types of geobag retaining walls, that is, non-compacted geobags wall, compacted geobag wall, combination of longitudinal and transversal laied geobags wall, gabion and geobag wall were constructed in the field with instrumentation. Based on the results of field measurement, transversal layered geobag wall for non-compacted case was displaced 30% more than that of mixed gabion wall. Also, the more than 2m geobag walls without reinforcement at the backfill area are turned out to be unstable in terms of wall displacement. On the one hand, the distribution of the earth pressure for all geobag retaining walls sites show within the range of Rankine's and Coulomb's earth pressure after construction. But after intensity rainfall, the transversal laied geobag walls significantly increment of soil pressure. The geobag walls which constructed in the way of mixed wall systems such as gabion and geobag, longitudinal and transversal laied geobags are much stable with comparison of transversal laied geobag wall.

Study on the effect of p-type doping in mid-infrared InAs/GaSb superlattice photodetectors

  • Han, Im-Sik;Lee, Yong-Seok;Nguyen, Tien Dai;Lee, Hun;Kim, Jun-O;Kim, Jong-Su;Gang, Sang-U;Choe, Jeong-U;Kim, Ha-Sul;Ku, Zahyun;Lee, Sang-Jun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2015.08a
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    • pp.170.1-170.1
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    • 2015
  • 안티모니 (Sb)를 기반으로 한 제2형 초격자 (Type II superlattice, T2SL)구조 적외선 검출기 연구는 2000년대 들어 Sb 계열의 화합물 반도체 성장 기술이 발전함에 따라 HgCdTe (MCT), InSb, 양자우물 적외선 검출기 (QWIP)를 대체할 수 있는 고성능의 양자형 적외선 검출 소재로 부상하였으며, 현재 전 세계적으로 활발한 연구가 진행되고 있다. 특히, 기존의 양자형 적외선 검출소자에 비해 전자의 유효질량이 상대적으로 커서 밴드 간의 투과전류가 줄어들 뿐만 아니라, 전자와 정공이 서로 다른 물질 영역에 분포하여 Auger 재결합률을 효과적으로 줄일 수 있어 상온 동작이 가능한 소재로 주목을 받고 있다. 또한, T2SL 구조는 초격자를 구성하는 물질의 두께나 조성 변화를 통한 밴드갭 변조가 용이하여 단파장에서 장파장 적외선에 이르는 광범위한 파장 대역에서 동작이 가능할 뿐만 아니라 구조적 변화를 통해 이중 대역을 동시에 검출 할 수 있는 차세대 적외선 열영상 소자로 알려져 있다. 본 연구에서는 분자선 에피택시(MBE)법을 이용하여 300 주기의 InAs/GaSb (10/10 ML) 제2형 초격자 구조를 성장하여 적외선 검출소자를 제작하였다. 제2형 초격자 구조를 구성하는 물질계에 p-type dopant인 Be을 이용하여 각각 도핑 농도가 다른 시료를 성장하였다. 이때 p-type 도핑 농도는 각각 $1/5/10{\times}10^{15}cm^{-3}$로 변화를 주었다. 성장된 시료의 구조적 특성 분석을 위해 고분해능 X선 회절 (High resolution X-ray diffraction, HRXRD)법을 이용하였으며, 초격자 한 주기의 두께가 6.2~6.4 nm 로 설계된 구조와 동일하게 성장됨을 확인 하였으며, 1차 위성피크의 반치폭은 30~80 arcsec로 우수한 결정성을 가짐을 확인하였다. 적외선 검출을 위한 $410{\times}410{\mu}m^2$ 크기의 단위 소자 공정을 진행하였으며 이때 적외선의 전면 입사를 위해 소자 위에 $300{\mu}m$의 윈도우 창을 제작하였다. 단위 소자의 측벽에는 표면 누설 전류가 흐르는데 이를 방지하기 위해서 표면보호막을 증착하였다. 적외선 검출 소자의 전기적 특성 평가를 위해 각각의 시료의 암전류 (dark current)와 파장별 반응 (spectral response)을 온도별로 측정하여 비교 및 분석하였다.

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