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Color Variation in Color-shade Polycrystalline Zirconia Ceramics by the Atmosphere Controlled Firing

  • Chang, Myung Chul
    • Journal of the Korean Ceramic Society
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    • v.55 no.2
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    • pp.116-125
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    • 2018
  • Color shade variation was investigated in zirconia dental blocks, prepared using commercial powders. As a reference color-shade block we used the color indexes of A2, A3.5, A4 and B3, according to the VITA classical color scale. The zirconia powders for color shade blocks showed colors of white, yellow, pink and grey, respectively, after firing at $1530^{\circ}C$. The zirconia powders were mixed according to the recipe of color shade blocks and shaped at lower pressure using a uniaxial hydrostatic press. The shaped sample was inserted into a vinyl pack and sealed in a vacuum form machine. The shaped block samples were reshaped at 450 bar using an isostatic cold press and fired at $1530^{\circ}C$ for three hours. In order to investigate the atmospheric color variation with firing temperature, the A2, A3.5, A4 and B3 sintered blocks were fired between $700^{\circ}C$ and $1300^{\circ}C$ under controlled atmosphere of $pN_2$ and $pO_2$. The surface color picture was taken using a smart phone camera and compared with the results obtained using the VITA classical color scale. Quantitative color index value, CIELAB, was measured using a color-meter. Above $800^{\circ}C$, the color darkness greatly increased with the increase of the reduction temperature and keeping time.

A Study on the Degradation Analysis of PVC Hose for Gas (가스용 저압염화비닐호스 경년열화분석에 관한 연구)

  • Kim, Wan-Jin;Yi, Young-Seop;Ryu, Keun-Jun;Kim, Hyun-Ki
    • Journal of the Korean Society of Safety
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    • v.24 no.2
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    • pp.37-41
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    • 2009
  • PVC hose for gas is used widely in many of places which is used for connector between combustor and gas cock. In this study, it is collected by 5 regional area as Gyeonggi, Jeonnam, Gyeongbuk, Jeju and Gangwon and tested in leakage, hardness, anti-low temperature. As a result, the color on it is started to change rapidly when it is installed. Some of specimen are broken in bending test after keeping in $-25^{\circ}C$, 24hours. It's hardness has a tendency to increase gradually. If hardness of hose is increased, PVC hose is separated easily from cock or combustor so that LP gas or city gas can be escaped. For prevention of gas leakage accidents of PVC hose, the available period of it should be presented.

A COMPARISON OF JERSEY CROSSBRED AND LOCAL OXEN AS DRAUGHT ANIMALS IN THE EASTERN HILLS OF NEPAL

  • Pearson, R.A.
    • Asian-Australasian Journal of Animal Sciences
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    • v.4 no.1
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    • pp.31-40
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    • 1991
  • Four pairs of draught oxen (two local and two Jersey crossbred) were studied when they ploughed dry land on local farms. Work done, distance traveled and body temperature of each ox were measured continuously over a 5 h working day. A different team worked each day, completing at least six days work each. Individual food intakes and digestibility of feed were measured when the animals were given rice straw and tree fodder, and housed and fed according to local husbandry practices. The Jersey crossbreds, particularly the longer legged type, had a higher rate of work than the local oxen in this study. They did significantly more work and covered a greater distance during the day. The absence of a hump in the crossbred oxen had no effect on the position of the yoke or the way the oxen pulled when ploughing. The longer legged type of Jersey crossbred tended to work more erratically than any of the other teams. A fast rate of work made the oxen more liable to heat stress. When fed according to local practices and given the same amount of feed as local oxen, Jersey crossbreds tended to do less well. During the ploughing months, the local oxen gained weight, while the crossbreds remained at the same or lost some weight. Although there were some disadvantages to keeping Jersey crossbreds for work, their favourable work output suggests that the introduction of the Jersey crossbred in the hills of Nepal is unlikely to be detrimental to the performance of the work oxen population.

Ultrasonic ACF Bonding Technique for Mounting LCD Driver ICs (LCD 구동 IC의 실장을 위한 초음파 ACF접합 기술)

  • Joung, Sang-Won;Yun, Won-Soo;Kim, Kyung-Soo
    • Journal of Institute of Control, Robotics and Systems
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    • v.14 no.6
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    • pp.543-547
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    • 2008
  • In the paper, we develop the ultrasonic bonding technique for LCD driver chips having small size and high pin-density. In general, the mounting technology for LCD driver ICs is a thermo-compression method utilizing the ACF (An-isotropic Conductive Film). The major drawback of the conventional approach is the long process time. It will be shown that the conventional ACF method based on thermo-compression can be remarkably enhanced by employing the ultrasonic bonding technique in terms of bonding time. The proposed approach is to apply the ultrasonic energy together with the thermo-compression methodology for the ACF bonding process. To this end, we design a bonding head that enables pre-heating, pressure and ultrasonic excitation. Through the bonding experiments mainly with LCD driver ICs, we present the procedures to select the best combination of process parameters with analysis. We investigate the effects of bonding pressure, bonding time, pre-heating temperature before bonding, and the power level of ultrasonic energy. The addition of ultrasonic excitation to the thermo-compression method reduces the pre-heating temperature and the bonding process time while keeping the quality bonding between the LCD pad and the driver IC. The proposed concept will be verified and demonstrated with experimental results.

Ultra-fine Grained Aluminum Alloy Sheets fabricated by Roll Bonding Process

  • Kim, Hyeong-Uk;Tsuji, Nobuhiro
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.05a
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    • pp.6.2-6.2
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    • 2009
  • Ultra-fine grained (UFG) Al alloys, which have submicron grain structures, are expected to show outstanding high strength at ambient temperature and excellent superplastic deformation at elevated temperatures and high strain rate. In order to get the UFG microstructure, various kind of severe plastic deformation (SPD) processes have been developed. Among these processes, accumulative roll bonding (ARB) process is a promising process to make bulky Al sheets with ultrafine grained structure continuously. The purpose of the present study is to clarify the grain refinement mechanism during the ARB process and to investigate on the effects of ultra-fine grained structure on the mechanical properties. In addition, UFG AA8011 alloy (Al-0.72wt%Fe-0.63wt%Si) manufactured by the ARB had fairly large tensile elongation, keeping on the strength. In order to clarify the reason for the increase of elongation in the UFG AA8011 alloy, detailed microstructural and crystallographic analysis was performed by TEM/Kikuchi-line and SEM/EBSP method. The unique tensile properties of the UFG AA8011 alloy could be explained by enhanced dynamic recovery at ambient temperature, owing to the large number of high angle boundaries and the Al matrix with high purity.

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A Feasibility Analysis of Rapid Acquisition Test for Cement Fineness using Hydrometer (시멘트 인수검사 시 액체밀도계법에 의한 분말도 품질 신속평가 가능성 분석)

  • Han, Cheon-Goo;Kim, Young-Tae
    • Journal of the Architectural Institute of Korea Structure & Construction
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    • v.34 no.6
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    • pp.29-34
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    • 2018
  • In this research, regarding the cement supplied to ready mixed concrete plant, the feasibility of rapid acquisition test for cement fineness using hydrometer which used for early strength evaluation of concrete was analyzed. Additionally, regarding the rapid test with hydrometer control factors were provided. As a result of analysis, quality control using hydrometer was possible with the regressive equation obtained in five minute between density of suspension and fineness of cement powder. As the control factors, dispersing admixture, replacing kerosene as a medium, and temperature of cement and water were evaluated. According to the control factor evaluation, the tap water was optimum as a medium and calibration of keeping the temperature of water to $20^{\circ}C$ or correction factor was needed for density results. Finally, it is considered that the suggested rapid quality evaluation method using hydrometer is cheaper and easier method than currently used Blaine test.

Effects of Storage Containers and Storage Temperatures on Kimchi Quality (저장용기 및 저장온도에 따른 김치의 품질변화)

  • 송주은
    • Journal of the East Asian Society of Dietary Life
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    • v.5 no.2
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    • pp.39-48
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    • 1995
  • The effects of storage containers and storage temperatures on Kimchi quality were investigated. The results were summarized as follows : 1. Pabix, poly ethylene-back+plastic container, tupper-ware were much better than crock, stainless steel, and plastic container in keeping a Kimchi. However, there was no significant differences between containers in the sensory test for Kimchi. 2. Kimchi stored at 18$\pm$2$^{\circ}C$ was the most delicious, which revealed pH 4.30, acidity 0.45-0.50%, and salt concentration 3.10wt% in the 4th days after storage whereas sensory score for Kimchi quality was very low in the 12th days after storage. 3. pH in Kimchi stored at 5$^{\circ}C$ after fermentation at 18$\pm$2$^{\circ}C$ was slowly decreased as compared to the Kimchi stored at 18$\pm$2$^{\circ}C$, but texture score of Kimchi stored at -5$^{\circ}C$ or -8$0^{\circ}C$ after fermentation at 18$\pm$2$^{\circ}C$, but texture score of Kimchi stored at -5$^{\circ}C$ or -8$0^{\circ}C$ were compared to that of the Kimchi stored at 18$\pm$2$^{\circ}C$ after fermentation. 5. In the group of Kimchi stored at 1$0^{\circ}C$, immediately after picking it took 48days until the best conditions which were pH 4.30 and acidity 0.45-0.50% were matched. 6. The most promising method in keeping good taste and good quality of Kimchi was to store Kimchi at 5$^{\circ}C$ after 4days fermentation at 18$\pm$2$^{\circ}C$. And, for long period preservation of Kimchi, it took would be effective to store at -8$0^{\circ}C$ after fermentation at 18$\pm$2$^{\circ}C$.

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Market Quality Changes of 'Fuji' Apples Influenced by the Duration of Preshipment Storage and Packaging during Simulated Export (수출 전 저장기간과 모의 수출에 따른 '후지' 사과의 상품성 변화)

  • Piao, Yi-Long;Lee, Jae-Chang;Hwang, Yong-Soo
    • Korean Journal of Agricultural Science
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    • v.29 no.1
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    • pp.15-23
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    • 2002
  • The percentage of watercore occurrence harvested on Nov. 6 (commercial harvest season) was over 80% but fruits seemed not to reach climacteric stage on the basis of ethylene evolution. The occurrence ratio and severity of watercore gradually decreased with the increase of preshipment storage for 2 months. The level of soluble solids did not show a clear tendency during preshipment storage but flesh firmness, fresh weight, and acidity gradually decreased. Although the overall quality of fruit reduced along with the increase of preshipment storage duration after exposure to retail condition at ambient temperature for 1 week, plastic film wrapping (PE 30 um) as well as plastic film wrapping plus ethylene scrubbing had a benefit on keeping freshness of fruit even after retail condition. Waxed fruit showed excellent appearance but browning disorder was developed. Results indicated that moisture barrier such as plastic film wrapping and ethylene removal have a great potential on keeping freshness of fruit during export which required long-term transport under low humidity environment.

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Fabrication of the Wafer Level Packaged LED Integrated Temperature Sensor and Configuration of The Compensation System for The LED's Optical Properties (온도센서가 집적된 WLP LED의 제작과 이를 통한 광 특성 보상 시스템의 구현)

  • Kang, In-Ku;Kim, Jin-Kwan;Lee, Hee-Chul
    • Journal of the Institute of Electronics Engineers of Korea SD
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    • v.49 no.7
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    • pp.1-9
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    • 2012
  • In this paper, resistance temperature detector (RTD) integrated into the LED package is proposed in order to solve the temperature dependence of LED's optical properties. To measure the package temperature in real time, the RTD type temperature sensor having excellent accuracy and linearity between temperature change and resistance change was adopted. A stable metallic film is required for long term reliability and stability of the RTD type temperature sensor. Therefore, deposition and annealing condition for the film were determined. Based on the determined condition, the RTD type temperature sensor with the sensitivity of about $1.560{\Omega}/^{\circ}C$ was fabricated inside the LED package. In order to configurate the LED package system keeping the constant brightness regardless of the temperature, additional conversion circuit and control circuit boards were fabricated and added to the fabricated LED package. The proposed system was designed to compensate the light intensity caused by temperature change using the variable duty rate of driving current. As a result, the duty rate of PWM signal which is the output signal of the configurated system was changed with the temperature change, and the duty rate was similarly varied with the target duty rate. Consequently, it was focused the fabricated RTD can be used for compensating the optical properties of LED and the LED package which exhibits constant brightness regardless of the temperature change.

On response of Surface Equilibrium Temperature for Change of Surface Characteristics : An EBM Study (지표 특성 변화에 대한 평형온도의 반응 연구 : EBM 연구)

  • Seo, Ye-Won;Chu, Jung-Eun;Ha, Kyung-Ja
    • The Korean Journal of Quaternary Research
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    • v.24 no.2
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    • pp.1-11
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    • 2010
  • Energy Balance Model (EBM) was used to experiment the distribution of surface equilibrium temperature which responds to external forcing associated with the surface characteristics. Surface equilibrium temperature is calculated as sum of incoming solar radiation and latitudinal transport is balanced with outgoing infrared radiation. To treat incoming solar radiation, the source of the earth energy, significantly for energy balance, the experiment for surface equilibrium temperature distribution was performed considering the energy balance with the latitudinal albedo change as well as land and sea distribution. In addition, linear albedo change experiment, arctic albedo 5%, 10%, 15% change experiments and the opposite albedo change experiments between arctic and mid-latitudes were performed using incoming solar radiation as an external forcing. Moreover, with and without ice-albedo feedback experiments were performed. Increasing of arctic albedo is blocked out the incoming solar radiation so that it induces decreasing of latitudinal heat transport. It is strengthened energy transport from low latitudes by keeping arctic low energy states. Therefore the temperature change in the mid-latitudes exhibits larger response than that of arctic due to the difference of transport. The land which has lower heat capacity than sea can be reach to equilibrium temperature shortly. Also land is more sensitive to temperature change with respects to albedo. Thus it induces the thermal difference between land and sea. As a result, the equilibrium temperature exhibits differently as the difference of albedo and heat capacity which are the one of surface characteristics. Surface equilibrium temperature decreases as albedo increase and the ratio of temperature change is large as heat capacity is small. The decreasing of surface equilibrium temperature with respects to increasing of linear albedo is accelerated by ice-albedo feedback. However local change of surface equilibrium temperature decreases non-linearly.

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