• Title/Summary/Keyword: interface treatment

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Direct treatment on live and cancer cells & process innovation of bio-sensor using atmospheric pressure plasma system with low-temperature arc-free unit

  • Lee, Keun-Ho;Lee, Hae-Ryong;Jun, Seung-Ik;Bahn, Jae-Hoon;Baek, Seung-J.
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.43-43
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    • 2010
  • We have characterized the parametric and functional properties of live cell and cancer cell according to plasma treatment conditions using Atmospheric Pressure (AP) Plasma with uniquely designed low temperature arc-free unit. AP plasma system showed very highly efficient capabilities of reacting and interfacing directly with live and cancer cells. The parametric results with the types of gases, applied power, applied gap, and process times on cells will be presented in accordance with functional studies of the works. The growth of cancer cells is directly influenced by AP plasma exposure with evaluating plasma conditions in several human cancer cells and understanding how plasma exposure alters molecular signaling pathways. The cells exhibit a slower or faster growth rates compared with untreated cells, depending on the cell types. These results strongly support the conclusion that alterations in one or more of each gene are responsible, at least in part, for plasma-induced apoptosis in cancer cells. In addition, it also will be presented that AP plasma has an important role for the improvement of sensor performance due to excellent interface property between enzyme and metal electrode for bio sensor manufacturing process.

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Comparative Study on Microstructures of Hot-rolled STS 304L/A516-70N and STS 316L/A516-70N Clad Plates (열간압연으로 제조된 STS 304L/A516-70N과 STS 316L/A516-70N 클래드재들의 미세조직에 대한 비교 연구)

  • Jin, Ju-Chan;Cho, Soochul;Sim, Hoseop;Lee, Young-Kook
    • Journal of the Korean Society for Heat Treatment
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    • v.34 no.4
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    • pp.171-178
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    • 2021
  • In the present study, we comparatively investigated the microstructures of two hot-rolled stainless steel clad plates; STS 304L - low carbon steel A516-70N and STS 316L - A516-70N. The STS 304L/A516-70N clad plate (Clad_304L_Ni) had a Ni-interlayer between stainless steel and carbon steel and a 90 ㎛ thick deformation band of unrecrystallized austenite grains on the stainless steel. The STS 316L/A516-70N clad plate (Clad_316L) had no interlayer and almost fully recrystallized austenite grains. Clad_304L_Ni exhibited the thinner a decarburized layer in carbon steel and a total carburized layer in stainless steel than Clad_316L. However, a severely carburized layer in stainless steel was thicker for Clad_304L_Ni than Clad_316L. Hardness profiles near the interface of clad plates matched well with microstructures at locations where the hardness values were measured.

Mechanical and Electrical Properties of Cu-15wt.%Ag Microcomposites Processed by Equal Channel Angular Pressing (등통로각압축공정을 이용하여 제작된 Cu-15wt.%Ag 미세복합재료의 미세구조 및 기계적, 전기적 특성)

  • Cho, Kyu Jin;Hong, Sun Ig
    • Korean Journal of Metals and Materials
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    • v.49 no.2
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    • pp.128-136
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    • 2011
  • Equal channel angular pressing (ECAP) with intermediate heat treatment was employed to optimize the strength of Cu-15 wt.%Ag. Changes in microstructure, electrical properties and mechanical properties were studied as a function of pressing methods and heat treatment. ECAPed Cu-15wt.%Ag exhibited ultrafine-grained microstructures with the shape and distribution of Ag-rich lamellae dependent on the processing routes. For route A in which the sample was pressed without rotation between each pass, the initial dendrites of Ag-rich phase were elongated along the shear direction and developed into elongated filaments. For route C in which the sample was rotated by 180 degree after each pass, the morphology of initial dendrites of Ag-rich phase was not much modified and the networked structure remained even after 8 passes of ECAP. For route Bc in which the sample was rotated by 90 degree after each pass, the initial dendrites became finer by fragmentation with no pronounced change of the shape and distribution of Ag-rich lamellae. The strength of Cu-15wt.%Ag ECAPed using route Bc was found to be greater than those ECAPed using route A, suggesting that the substructural strengthening is more effective in strengthening than the interface strengthening.

Interfacing between MAAP and MACCS to perform radiological consequence analysis

  • Kim, Sung-yeop;Lee, Keo-hyoung;Park, Soo-Yong;Han, Seok-Jung;Ahn, Kwang-Il;Hwang, Seok-Won
    • Nuclear Engineering and Technology
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    • v.54 no.4
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    • pp.1516-1525
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    • 2022
  • Interfacing the output of severe accident analysis with the input of radiological consequence analysis is an important and mandatory procedure at the beginning of Level 3 PSA. Such interfacing between the severe accident analysis code MELCOR and MACCS, one of the most commonly used consequence analysis codes, is relatively tractable since they share the same chemical groups, and the related interfacing software, MelMACCS, has already been developed. However, the linking between MAAP, another frequently used code for severe accident analyses, and MACCS has difficulties because MAAP employs a different chemical grouping method than MACCS historically did. More specifically, MAAP groups by chemical compound, while MACCS groups by chemical element. An appropriate interfacing method between MAAP and MACCS has therefore long been requested by users. This study suggests a way of extracting relevant information from MAAP results and providing proper source term information to MACCS by an appropriate treatment. Various parameters are covered in terms of magnitude and manner of release in this study, and special treatment is made for a bypass scenario. It is expected that the suggested approach will provide an important contribution as a guide to interface MAAP and MACCS when performing radiological consequence analyses.

A Case Report of 2 Cases of Severe Sacral Stage IV Pressure Ulcer in the Elderly Who Were Cured by Treatment with Jaungo and Acupuncture and Debridement (자운고와 침 치료 및 변연절제술로 완치된 고령자의 천골부위 4기 중증욕창 2례에 대한 증례보고)

  • Seo, Jung Bok;Lee, Tae Jong;Lee, Ji Won;Kim, Kyoung Ah;Yoon, Jung Jeh
    • Journal of Physiology & Pathology in Korean Medicine
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    • v.36 no.1
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    • pp.35-39
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    • 2022
  • The purpose of this study is to report the effect of Jaungo and acupuncture and debridement for severe pressure ulcer in the elderly. Two Elderly patients with stage 4 pressure ulcer in the sacral region were eligible to participate in this study. Dressing using Jaungo was applied twice a day, and acupuncture was applied 4 times a week along the boundary between the normal epidermis and the pressure ulcer granulation tissue in contact with the pressure ulcer interface. Debridement was performed after partial or total removal, if necessary, under the judgment of the attending physician.In both cases, stage 4 pressure sores in the sacrum covered with crusts were cured in 193 days and 223 days, respectively, and no side effects were reported during treatment. This study shows that Jaungo and acupuncture and debridement may represent effective to treat pressure ulcer. but further studies are needed.

MECHANICAL PROPERTIES AND CORROSION BEHAVIORS OF AGED Ti-4Mo-4Cr-X (X = Sn, V, Zr) ALLOYS FOR METALLIC BIOMATERIALS

  • KWANGMIN LEE;GUNHEE LEE
    • Archives of Metallurgy and Materials
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    • v.65 no.4
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    • pp.1297-1301
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    • 2020
  • The purpose of this study was to investigate the mechanical properties of beta type aged Ti-4Mo-4Cr-X (X = V, Sn, Zr) quaternary alloy for use as a cardiovascular stent. Titanium (Ti) alloys were fabricated using a vacuum arc remelting furnace process. To homogenize the specimens of each composition and remove the micro segregation, all cast specimens were subjected to homogenization at 850℃ for 4 h, which was 100℃ higher than the β-transus temperature of 750℃. The tensile strength and elongation of the aged Ti-4Mo-4Cr-X (X = V, Sn, Zr) alloys were increased as compared to the homogenized alloys. In addition, many α/β interface boundaries formed after aging treatment at 450℃, which acted as inhibitors of strain and caused an increase in tensile strength. The elongation of Ti-4Mo-4Cr-X alloys consisting of α + β phases after aging treatment was improved by greater than 30%. Results of a potentiodynamic polarization test showed that the lowest current density of Ti-4Mo-4Cr-4Sn with 1.05 × 10-8 A/cm2 was obtained. The present Ti-4Mo-4Cr-X alloys showed better corrosion characteristics as compared to the 316L stainless steel and L605 (Co-Cr alloy) cardiovascular stent alloys.

SHEAH BOND STRENGTH OF VENEERING CERAMIC TO ELECTROFORMED GOLD WITH THREE DIFFERENT SURFACE TREATMENT (표면처리방법에 따른 전기성형금속의 도재결합강도)

  • Kim Cheol;Lim Jang-Seop;Jeon Young-Chan;Jeong Chang-Mo;Jeong Hee-Chan
    • The Journal of Korean Academy of Prosthodontics
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    • v.43 no.5
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    • pp.599-610
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    • 2005
  • Purpose: The success of the bonding between electroformed gold and ceramic is dependent on the surface treatment of the pure gold coping. The purpose of this study was to evaluate the bonding strength between the electroformed gold and ceramic with varying surface treatment. Materials and methods: A total of 32 disks,8 were using conventional ceramometal alloy, 24 were using electroforming technique as recommended by manufacturer, were prepared. 24 electroformed disks were divided 3 groups according to surface treatment, i.e. 50 microns aluminium oxide sandblasting(GES-Sand), gold bonder treatment(GES-Bond) and $Rocatec^{TM}$ system(GES-Rocatec). For control group of conventional alloy 50 microns aluminium oxide treatment was done(V-Supragold). Energy dispersive x-ray analysis and scanning electron microscope image were observed. Using universal testing machine, shear bond strength and bonding failure mode at metal-porcelain interface were measured. Results and Conclusion: The following conclusions were drawn: 1. In the energy dispersive x-ray analysis, the Au was main component in electroformed gold(99.9wt%). After surface treatment, a little amount of $Al_2O_3(2.4wt%)$ were found in GES-Sand, and $SiO_2(4wt%)$ in GES-Bond. In GES-Rocatec, however, a large amount of $SiO_2(17.4wt%)$ were found. 2. In the scanning electron microscopy, similar pattern of surface irregu larities were observed in V-Supragold and GES-Sand. In GES-Bond, surface irregularities were increased and globular ceramic particles were observed. In GES-Rocatec, a large amount of silica particles attached to metal surface with increased surface irregularities were observed. 3. The mean shear bond strength values(MPa) in order were $22.9{\pm}3.7(V-Supragold),\;22.1{\pm}3.8(GES-Bond),\;20.1{\pm}2.8(GES-Rocatec)\;and\;13.0{\pm}1.4(GES-Sand)$. There was no significant difference between V-Supragold, GES-Bond, and GES-Rocatec. (P>0.05) 4. Most bonding failures modes were adhesive type in GES-Sand. However, in V-Supragold, GES-Bond and GES-Rocatec, cohesive and combination failures were commonly observed. From the result, with proper surface treatment method electroformed gold may have enough strength compare to conventional ceramometal alloy.

EFFECTS OF ACID TREATMENT OF FLUORIDE APPLIED DENTIN SURFACE ON DENTIN BONDING (불소도포한 상아질면의 산처리가 상아질접착에 미치는 영향)

  • Hwang, Hea-Kyung;Ahn, Sik-Hwan;Kim, Sung-Kyo;Jo, Kwang-Hun;Park, Jin-Hoon
    • Restorative Dentistry and Endodontics
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    • v.21 no.2
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    • pp.602-618
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    • 1996
  • The purpose of this study was to investigate the effect of acid treatment of fluoride applied dentin surface with various concentrations of phosphoric acid for various periods of time on dentin bonding. Dentin specimens prepared from freshly extracted bovine mandibular anterior teeth were divided into fluoridated and nonfluoridated groups. Specimens of nonfluoridated group were pretreated with 10% phosphoric acid for 15 seconds. Those of fluoridated groups were treated with 2% sodium fluoride or 2% stannous fluoride solution for 5 minutes and stored in $37^{\circ}C$ distilled water for 3 days, followed by phosphoric acid treatment. The concentrations of phosphoric acid were 10%, 32% or 50% and the treatment periods of time were 15, 30 or 60 seconds. All the specimens were bonded with All Bond$^{(R)}$ 2 and Bisfil$^{TM}$ composite resin. After bonded specimens were stored in $37^{\circ}C$ distilled water for 24 hours, tensile bond strengths of each specimens were measured and the pretreated dentin and the fractured dentin surfaces were examined under the scanning electron microscope. The results were as follows : The tensile bond strengths from the fluoridated groups were significantly lower than those from the nonfluoridated group when the concentrations of phosphoric acid and the treatment periods of time were equal in all the groups (p<0.05). In general, the higher the concentration of phosphoric acid and the longer the treatment period of time for acid etching on the fluoride applied dentin surface, the higher were the bond strength values. Recovery of bond strength of the dentin bonding agent was better in the NaF applied group than in the $SnF_2$ applied one. SEM findings of NaF applied and $SnF_2$ applied dentin surfaces demonstrated reaction product-covered and partially or completely obstructed dentinal tubules. SEM findings of dentin surfaces fluoridated for 5 minutes followed by etching showed wider tubular openings and more clean dentin surfaces when dentin was etched with higher concentration of phosphoric acid for longer period of time. On the SEM observations of the fractured dentin-resin interface, the etched specimens of fluoridated group showed an adhesive failure mode when the concentration of phosphoric acid and the treatment period of time were same as in the nonfluoridated group. As the concentration of phosphoric acid and the treatment period of time increase during acid etching, the cohesive failure area increased. However, excessive acid etching caused adhesive failure.

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The Inhibitive Effect of Electrochemical Treatment Applied to Fresh/hardened Concrete (철근 부식 방식을 위한 굳지 않은/굳은 콘크리트의 전기방식 적용에 관한 연구)

  • Kim, Sung-Wook;Moon, Jae-Heum;Ann, Ki-Yong
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.17 no.5
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    • pp.67-76
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    • 2013
  • In this study, the inhibitive effect of electrochemical treatment subjected to fresh and hardened concrete and literature reviews in terms of the treatment were performed. In hardened concrete, chloride ions are mixed during casting to destroy the passivity of steel, and then the current was provided for 2 weeks with 250, 500 and $750mA/m^2$. After completion of electrochemical treatment, the extraction of chloride ions was quantified and repassivation of steel was observed. Simultaneously, the equated levels of current density for 2 weeks were applied to fresh concrete. Steel-concrete interface in concrete was observed by BSE image analysis and the concrete properties in terms of the diffusivity of chloride ions and the resistance of steel corrosion was measured. As the result, electrochemical treatment is very effectiveness to rehabilitate the passive film on the steel surface and 63-73% of chloride ions in concrete were extracted by the treatment. As the treatment was applied to fresh concrete, the resistance of steel corrosion was improved due to the densification of $Ca(OH)_2$ layers in the vicinity of steel. However, an increase in the current density resulted in an increase in surface chloride content of concrete.

Spectral Change and Surface Images of the Azobenzene Functionalized Dendrimer in LB Monolayers

  • Shin, Hoon-Kyu;Kwon, Young-Soo
    • KIEE International Transactions on Electrophysics and Applications
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    • v.11C no.4
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    • pp.146-149
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    • 2001
  • The functionalized dendrimer containing 48 azobenzene was synthesized. Many isolated featureless domains were explicitly observed even at the air/water interface. Also, these monolayers were representatively observed, showing the change of surface pressure with irradiation time and wavelength. In AFM images, larger domains irregularly shaped structures on the top, while smaller ones were free from such defects. In the optical absorption spectra of the monolayer films by UV irradiation and heat treatment, only the photoiosmerization of the G4-48 Azo monolayers was observed, revealing a decrease of absorbance peaks without any change of the spectral shape. This suggests that the functional group and the symmetric chain affect optical behavior and morphological change.

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