• Title/Summary/Keyword: interface treatment

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EFFECT OF COBALT-CHROMIUM ALLOY SURFACE TREATMENT WHEN BONDING WITH 4-META/MMA-TBB RESIN (Cobalt-Chromium 합금의 표면처리가 4-META/MMA-TBB 레진과의 접착에 미치는 영향)

  • Jin, Jae-Sik;Kim, Kyo-Han;Lee, Cheong-Hee;Jo, Kwang-Hun
    • The Journal of Korean Academy of Prosthodontics
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    • v.38 no.4
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    • pp.510-525
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    • 2000
  • The effects of pretreatment of Co-Cr alloy, including two adhesive primers that contain either MDP or MAC-10, and silicoating on the bond The result sobtained as follows; o Strength of 4-META/MMA-TBB resin were investigated using FT-IR, SEM, and EDAX. o In the SEM observation of surface morphologies, the sandblasted specimen exibited a very rough surface, whereas the surfaces of the two groups primed with either MDP or MAC-10 were covered with a layer of primer, and the surface morphology of the silicoated specimen remained almost the same after sandblasting. o Before the thermocycling tests, the group treated with MDP demonstrated the highest mean tensile bond strength and the sandblasted group showed the lowest bond strength. o After 20,000 thermocyling, the mean tensile bond strength of the sandblasted group exhibited a 50% reduction in bond strength, while the others showed a $20\sim30%$ reduction. o Observation of the metal-resin interface revealed that in all groups the resin permeated the rough surface formed by sandblasting thereby producing a mechanical bond between the metal and the resin. It was also found that thermocycling resulted in a gap formation at the metal-resin interface of the specimens, and the sandblasted group exhibited a larger gap width than the other groups. o In fracture mode, all specimens indicated a cohesive fracture within the resin before thermocycling. However, thermocyling produced adhesive failure at the edge of the resin-metal interface in most specimens. The sandblasted group, which exhibited the lowest bond strength after thormocycling, also demonstrated the largest area of adhesive failure.

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The study of Ca $F_2$ films for gate insulator application (게이트 절연막 응용을 위한 Ca $F_2$ 박막연구)

  • 김도영;최유신;최석원;이준신
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1998.06a
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    • pp.239-242
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    • 1998
  • Ca $F_2$ films have superior gate insulator properties than conventional gate insulator such as $SiO_2$, Si $N_{x}$, $SiO_{x}$, and T $a_2$ $O_{5}$ to the side of lattice mismatch between Si substrate and interface trap charge density( $D_{it}$). Therefore, this material is enable to apply Thin Film Transistor(TFT) gate insulator. Most of gate oxide film have exhibited problems on high trap charge density, interface state in corporation with O-H bond created by mobile hydrogen and oxygen atom. This paper performed Ca $F_2$ property evaluation as MIM, MIS device fabrication. Ca $F_2$ films were deposited at the various substrate temperature using a thermal evaporation. Ca $F_2$ films was grown as polycrystalline film and showed grain size variation as a function of substrate temperature and RTA post-annealing treatment. C-V, I-V results exhibit almost low $D_{it}$(1.8$\times$10$^{11}$ $cm^{-1}$ /le $V^{-1}$ ) and higher $E_{br}$ (>0.87MV/cm) than reported that formerly. Structural analysis indicate that low $D_{it}$ and high $E_{br}$ were caused by low lattice mismatch(6%) and crystal growth direction. Ca $F_2$ as a gate insulator of TFT are presented in this paper paperaper

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Research of Historic Knowledge Based Traditional Korean Medicine(TKM) Database System (한의학지식정보자원 DB구축에 있어서 지식고고학적 가중치부여의 의의와 실제적용방안 연구)

  • Oh, Jun-Ho;Ahn, Sang-Woo;Kim, Nam-Il;Cha, Wung-Seok
    • Korean Journal of Oriental Medicine
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    • v.16 no.1
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    • pp.69-84
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    • 2010
  • It is the well-known truth that processing of raw information is needed to a certain extent during information search. Especially for Oriental Medical information, it becomes much clearer that even more complex processing is necessary. As a means of reducing such complexity, this study suggests a way to understand effectively the organic relationships among information found on the interface. In this process, 'knowledge-based archaeological' method has been used. A new concept of interface observed by this research is the study of a system which contains realistically considered knowledge-based archaeological and historical specificity. These models are organized so that search results could be materialized in different tree-structured interface models, which can help one understand the relationships among wanted search results at one glance and confirm the details of those results via mouse click. Strength of the vertical tree structure resides in its capability of suggesting its users clear historical relationship between separate Oriental medical information. The horizontal tree structure enables deeper understanding of sectional interrelationship of searched information. The strength of the prescription tree structure is that it helps one understand the lineage of prescriptions, as Oriental medicinal treatment is often summarized into changes in prescriptions.

Effects of $N_2/H_2$ plasma treatments on enhancement of neuronal cell affinity on single-walled carbon nanotube paper scaffolds

  • Yoon, Ok-Ja;Lee, Hyun-Jung;Jang, Yeong-Mi;Kim, Hyun-Woo;Lee, Won-Bok;Kim, Sung-Su;Lee, Nae-Eung
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.393-393
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    • 2010
  • The biocompatibility of materials used for biomedical applications depends on chemical composition, mechanical stiffness, surface energy, and roughness. The plasma treatment and etching process is a very important technology in the biomedical fields due to possibility of controlling the surface chemistry and properties of materials. In this work, $N_2/H_2$ plasma were treated on single-walled carbon nanotubes (SWCNTs) paper and characterization of treated SWCNTs paper was carried out. Also we investigated neurite outgrowth from SH-SY5Y on treated SWCNTs paper. The results indicated that $N_2/H_2$ plasma-modified SWCNTs paper enhanced neuronal cell adhesion, viability, neurite outgrowth and branching in vitro and exerted a positive role on the health of neural cells.

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Effect of Thermal Aging on Intermetallic Compound Growth Kinetics of Au Stud Bump (Au stud 범프의 금속간화합물 성장거동에 미치는 시효처리의 영향)

  • Lim, Gi-Tae;Lee, Jang-Hee;Kim, Byoung-Joon;Lee, Ki-Wook;Lee, Min-Jae;Joo, Young-Chang;Park, Young-Bae
    • Korean Journal of Materials Research
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    • v.18 no.1
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    • pp.45-50
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    • 2008
  • Microstructural evolution and the intermetallic compound (IMC) growth kinetics in an Au stud bump were studied via isothermal aging at 120, 150, and $180^{\circ}C$ for 300hrs. The $AlAu_4$ phase was observed in an Al pad/Au stud interface, and its thickness was kept constant during the aging treatment. AuSn, $AuSn_2,\;and\;AuSn_4$ phases formed at interface between the Au stud and Sn. $AuSn_2,\;AuSn_2/AuSn_4$, and AuSn phases dominantly grew as the aging time increased at $120^{\circ}C,\;150^{\circ}C,\;and\;180^{\circ}C$, respectively, while $(Au,Cu)_6Sn_5/Cu_3Sn$ phases formed at Sn/Cu interface with a negligible growth rate. Kirkendall voids formed at $AlAu_4/Au$, Au/Au-Sn IMC, and $Cu_3Sn/Cu$ interfaces and propagated continuously as the time increased. The apparent activation energy for the overall growth of the Au-Sn IMC was estimated to be 1.04 eV.

Comparative analysis of turbulence models in hydraulic jumps

  • Lobosco, Raquel J.;da Fonseca, David O.;Jannuzzia, Graziella M.F.;Costa, Necesio G.
    • Coupled systems mechanics
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    • v.8 no.4
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    • pp.339-350
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    • 2019
  • A numerical simulation of the incompressible multiphase hydraulic jump flow was performed to compare the interface prediction through the use of the three RANS turbulence models: $k-{\varepsilon}$, $RNGk-{\varepsilon}$ and SST $k-{\omega}$. A three dimensional no submerged hydraulic jump and a two dimensional submerged hydraulic jump were modeled. Both the geometry and the mesh were created using the open source Gmsh code. The project's geometry consists of a rectangular channel with length and height differences between the two dimensional and three dimensional simulations. Uniform hexahedral cells were used for the mesh. Three refining meshes were constructed to allow to verify simulation convergence. The Volume of Fluid (abbr. VOF) method was used for treatment of the air-water surface. The turbulence models were evaluated in three distinct set up configurations to provide a greater accuracy in the flow representation. In the two-dimensional analysis of a submerged hydraulic jump simulation, the turbulence model RNG RNG $k-{\varepsilon}$ provided a better interface adjust with the experimental results than the model $k-{\varepsilon}$ and SST $k-{\omega}$. In the three-dimensional simulation of a no-submerged hydraulic jump the k-# showed better results than the SST $k-{\omega}$ and RNG $k-{\varepsilon}$ capturing the height and length of the ledge with a better fit with the experimental results.

Effects of radiation therapy on the dislocation resistance of root canal sealers applied to dentin and the sealer-dentin interface: a pilot study

  • Pallavi Yaduka;Rubi Kataki;Debosmita Roy;Lima Das;Shachindra Goswami
    • Restorative Dentistry and Endodontics
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    • v.46 no.2
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    • pp.22.1-22.12
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    • 2021
  • Objectives: This study evaluated and compared the effects of radiation therapy on the dislocation resistance of AH Plus and BioRoot RCS applied to dentin and the sealer-dentin interface. Materials and Methods: Thirty single-rooted teeth were randomly assigned to 2 groups (n = 15 each): AH Plus (Dentsply DeTrey) and BioRoot RCS (Septodont). Each group was subdivided into control and experimental groups. The experimental group was subjected to a total radiation dose of 60 Gy. The root canals of all samples were cleaned, shaped, and obturated using the single-cone technique. Dentin slices (1 mm) were sectioned from each root third for the push-out test and scanning electron microscopy (SEM) was done to examine the sealer-dentin interface. The failure mode was determined using stereomicroscopy. Bond strength data were analyzed by the independent t-test, 1-way analysis of variance, and the Tukey post hoc test (α = 0.05). Results: Significantly lower bond strength was observed in irradiated teeth than non-irradiated teeth in the AH Plus group (p < 0.05). The BioRoot RCS group showed no significant reduction in bond strength after irradiation (p > 0.05) and showed a higher post-irradiation bond strength (209.92 ± 172.26 MPa) than the AH Plus group. SEM revealed slightly larger gap-containing regions in irradiated specimens from both groups. Conclusions: The dislocation resistance of BioRoot RCS was not significantly changed by irradiation and was higher than that of AH Plus. BioRoot RCS may be the sealer of choice for root canal treatment in patients undergoing radiation therapy.

Fabrication and Microstructure/Properties of Bulk-type Tantalum Material by a Kinetic Spray Process (Kinetic Spray 공정을 이용한 벌크형 탄탈륨 소재의 제조 및 미세조직/물성)

  • Lee, Ji-Hye;Kim, Ji-Won;Lee, Kee-Ahn
    • Journal of Powder Materials
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    • v.23 no.1
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    • pp.8-14
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    • 2016
  • A bulk-type Ta material is fabricated using the kinetic spray process and its microstructure and physical properties are investigated. Ta powder with an angular size in the range $9-37{\mu}m$ (purity 99.95%) is sprayed on a Cu plate to form a coating layer. As a result, ~7 mm-sized bulk-type high-density material capable of being used as a sputter material is fabricated. In order to assess the physical properties of the thick coating layer at different locations, the coating material is observed at three different locations (surface, center, and interface). Furthermore, a vacuum heat treatment is applied to the coating material to reduce the variation of physical properties at different locations of the coating material and improve the density. OM, Vickers hardness test, SEM, XRD, and EBSD are implemented for analyzing the microstructure and physical properties. The fabricated Ta coating material produces porosity of 0.11~0.12%, hardness of 311~327 Hv, and minor variations at different locations. In addition, a decrease in the porosity and hardness is observed at different locations upon heat treatment.

Laser Surface Treatment of Magnesium Alloy using ZrO2 for Corrosion Resistance (내식성 향상을 위한 마그네슘합금의 ZrO2 적용 레이저 표면 처리)

  • Yoon, Sangwoo;Kang, Dongchan;Kim, Joohan
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.15 no.4
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    • pp.93-100
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    • 2016
  • The laser surface treatment of magnesium alloy was studied. $ZrO_2$ was used as sintering ceramics, and its corrosion resistance was verified. Appropriate laser parameters were proposed for homogeneous solidification of the sintered layer. The chemical compositions of the sintered layer were analyzed with laser-induced breakdown spectroscopy. $Na_2SO_4$ was used for a corrosion test, and the resistance of the sintered sample was confirmed. The microstructures of the sintered parts were also examined. The solidified grains on the top sintered surface were observed; however, reasonable fusion was obtained at the interface between the baseline and the ceramics. Laser surface treatment using $ZrO_2$ on magnesium alloy showed an improvement in corrosion resistance.

The ESCA Analysis of Hydroxyapatite Thin Films Deposited by RF Sputtering (RF 스퍼터링으로 증착된 하이드록시아파타이트 박막의 ESCA 분석)

  • Jung, Chan-Hoi;Lee, Jun-Hee;Kim, Soon-Kook;Kim, Myung-Han;Yu, Jae-Keun;Kim, Seung-Eon
    • Korean Journal of Materials Research
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    • v.16 no.4
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    • pp.264-271
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    • 2006
  • RF sputtering process was applied to produce thin hydroxyapatite(HAp) films on Ti-6Al-4V alloy substrates. The effects of different heat treatment conditions on the chemical composites between HAp thin films and Ti-6Al-4V alloy substrates were studied. After deposition, the HAp thin films were heat treated for 1h at $400^{\circ}C,\;600^{\circ}C\;and\;800^{\circ}C$ under the atmosphere, and analyzed O/M, FESEM-EDX and ESCA, respectively. Experimental results represented that interface of HAp thin films and Ti-6Al-4V alloy substrates was composed Ti-OH, TiO, TiN, $Al_2O_3,\;V_2O_3,\;VO_2$. pyrophosphate and decreased carbide followed by the increase of heat treatment temperature.