• 제목/요약/키워드: inorganic particle

검색결과 302건 처리시간 0.026초

Particle Growth in Oxalate Process II; Control of Barium Titanyl Oxalate Particle Size

  • Hyo-Soon Shin;Zee Hoon Park;Chang Hyun Kim;Byung Kyo Lee
    • The Korean Journal of Ceramics
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    • 제2권2호
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    • pp.70-75
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    • 1996
  • On the basis of growth mechanism proposed by recent work, partile of barium titanyl oxalate was controlled by aging in water. From aging at $25^{\circ}C$ for 3 hours, uniform particles of 0.3 ${\mu}$m were obtained. During aging, abnormal particle growth was observed, which were thought to be caused by impurities in water. With increase of aging time and temperature, particle grows more, and differential growth was promoted. In aging for long time, grown particles were cracked.

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마이크로파 가열에 의하여 합성된 알루미나 입자의 특성 (Characteristics of Alumina Particles Synthesized by Microwave Heating)

  • 김성완;이성환;박재현;김준호;박성수;박희찬
    • 한국세라믹학회지
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    • 제39권10호
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    • pp.1007-1010
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    • 2002
  • 마이크로파 가열을 이용하여 ${\gamma}-Al_2O_3와\;Na_2SO_4$ 분말 혼합물로부터 알파 알루미나 판상체 입자를 합성하였다. 마이크로파를 이용하여 합성된 알루미나 입자의 크기와 입자분포를 마이크로파 이용 없이 동일한 혼합물로부터 합성된 분말과 비교하였다. 마이크로파를 이용하여 합성된 시료는 마이크로파 사용 없이 합성된 시료에 비하여 입자크기가 작고 입자분포가 좁음을 알 수 있었다.

New Retention System Using Branched Polymer

  • Son, Dong-Jin;Kim, Bong-Yong
    • 한국펄프종이공학회:학술대회논문집
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    • 한국펄프종이공학회 2006년도 PAN PACIFIC CONFERENCE vol.2
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    • pp.251-256
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    • 2006
  • The purpose of this study was to confirm multiple retention system of C-PAM, A-PAM and Inorganic micro particles vs. traditional micro particle system and dual polymer system by measuring retention, drainage and formation using RDA HSF and Techpap 2D -F Sensor The benefits of dual polymer system were easy to use, low chemical consumption and good retention property but defect was worse drainage property than inorganic microparticle systems. On the other hand, Inorganic microparticle system had benefit of good drainage effect but defects were difficult to use, high chemical consumption. Therefore, we tried to find optimal morphology of polyacrylamide and applied to multiple retention system of C-PAM, A-PAM and inorganic microparticles to compensate defects of both of retention systems. As a result, we found the performance of branched C-PAM, branched A-PAM and inorganic micro particle triple system was more appropriate than traditional inorganic mircoparticle systems or dual polymer systems by comparing retention, drainage and formation.

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Particle Size Effects on Microstructure Evolution and Microwave Dielectric Characteristics in $0.93MgTiO_3-0.07CaTiO_3$Ceramics

  • Lee, Jung-A;Kim, Jeong-Joo;Kim, Nam-Kyong;Cho, Sang-Hee;Hahn, Jin-Woo
    • The Korean Journal of Ceramics
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    • 제5권3호
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    • pp.260-264
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    • 1999
  • Effect of the particle size of $MgTiO_3$ and $CaTiO_3$ on the microstructural evolution during sintering of $0.93MgTiO_3-0.07CaTiO_3$ system was investigated. Microwave dielectric characteristics of the sintered ceramics were also measured. The microstructural evolutions were explained with an emphasis on the entrapping behavior of $CaTiO_3$ grain into the $MgTiO_3$ grain and were correlated with microwave dielectric characteristics. With an increasing particle size ratio between $CaTiO_3$and $MgTiO_3$, the fraction of entraped $CaTiO_3$ grains increased, which grain growth of $MgTiO_3$were concurrently accelerated due to decreasing drag force of its boundary migration. Besides, $CaTiO_3$-grain entrapment into the $MgTiO_3$grain interior led to decreaseing quality factor values.

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SHS법에 의한 탄화텅스텐 분말 합성 (Synthesis of Tungsten Carbide Powders by SHS Method)

  • 전호병;조덕호;이형복;박성
    • 한국세라믹학회지
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    • 제31권10호
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    • pp.1159-1168
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    • 1994
  • We powders were synthesized from W powders in differnet particle sizes by Self-propagating High-temperature Synthesis process (SHS) using a chemical furnace. The effects of the mole ratio of chemical fuel content, pellet thickness and the mole ratio between carbon and tungsten (C/W Ratio) on synthesis were investigated with the tungsten powders have different particle size each other. Compositional and structural characterization of these powders was carried out by scanning electron microscope (SEM0 and x-ray diffractometer. Powder characterization was carried out by the measurement of particle size distribution with laser-particle size analyzer. The amounts of WC obtained by SHS process depend very much on the particle size of tungsten powder and heat contents given in a product, i.e. as the particle size of W powder is smaller, the amounts of WC produced increase. Also the more heat contents is given, the more amounts of WC increase. By optimizing the synthesis conditions, it is possible to fabricate WC powders which have little secondary phases (W2C, C).

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양이온성 고분자로 처리한 무기입자에 대한 플렉소그라피 잉크의 흡착 (Adsorption of Flexography Ink on Inorganic Particles Patched with Cationic Polymer)

  • 정영빈;김진우;오규덕;윤혜정;이학래
    • 펄프종이기술
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    • 제44권5호
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    • pp.8-13
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    • 2012
  • The flexography ink has disadvantage in a deinking process because it tends to form too fine particles in alkali condition to be removed in flotation deinking. The influence of pH conditions on the particle size of phthalocyanine cyan ink used for flexo-printing was investigated to see the effect of pH conditions on flexography ink dispersion. Flexography ink particles prepared by grinding dried ink films were used in this experiment. Greater reduction of the ink particle size was noticed under alkaline pH condition, which was attributed to dissolution of resin component of the ink. Adsorption behavior of flexography ink onto pigment particles was examined using clay and talc as substrate pigments. Pretreatment of inorganic pigments with a cationic poly-DADMAC increased the surface adsorption of flexography ink particles, which improved the removal of the inks by centrifugal sedimentation of inorganic pigments. Most efficient removal of the ink particles was achieved when an optimal addition level of the cationic polymer was used for pretreatment of inorganic pigments, and this optimal addition level corresponds to the surface saturation point of the polyelectrolyte. Adsorption of flexography ink particles onto inorganic pigments improved the ink removal in flotation deinking since the pigment particles has the optimal particle size for flotation deinking.

전기영동적층법을 통한 판상 알루미나 입자와 전기영동 수지의 배향 유무기 복합체 제조 및 물성평가 (Preparation and Characterization of a Layered Organic-inorganic Composite by the Electrophoretic Deposition of Plate-shaped Al2O3 Particles and Electrophoretic Resin)

  • 박희정;임형미;최성철;김영희
    • 한국세라믹학회지
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    • 제50권6호
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    • pp.460-465
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    • 2013
  • Plate-shaped inorganic particles are coated onto a stainless steel substrate by the electrophoretic deposition of a precursor slurry which includes the inorganic particles of $Al_2O_3$ and polymer resin in mixed solvents to mimic the abalone shell structure, which is a composite of plate-shaped inorganic particles and organic interlayer binding materials with a layered orientation. The process parameters of the electrophoretic deposition include the voltage, coating time, and conductivity of the substrate. In addition, the suspension parameters are the particle size, concentration, viscosity, conductivity, and stability. We prepared an organic-inorganic composite coating with a high inorganic solid content by arraying the plate-shaped $Al_2O_3$ particles and electrophoretic resin via an electrophoretic deposition method. We analyzed the effect of the slurry composition and the electrophoretic deposition process parameters on the physical, mechanical and thermal properties of the coating layer, i.e., the thickness, density, particle orientation, Young's modulus and thermogravimetric analysis results.

환경친화적인 무기/유기 Core-Shell의 제조에 관한 연구 (A Study on the Environmental Fraternized Preparation of Inorganic/organic Core-shell Binder)

  • 설수덕;임재길;임종민;권재범;이내우
    • 한국안전학회지
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    • 제19권1호
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    • pp.81-87
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    • 2004
  • Composite particles using inorganic and organic chemicals were synthesized and the results of those reaction were compared to variation of temperature and agitation speed in presence of $CaCO_3$ which was adsorbed SDBS. Also the synthesises were optimized according to conversion rate of composite particles. In inorganic/organic core-shell composite particle polymerization, $CaCO_3$ adsorbed by 0.5wt% surfactant SDBS was prepared initially and then core $CaCO_3$ was encapsulated by sequential emulsion polymerization using MMA at the addition of APS 3.16${\times}$$10^{-3}$mol/L to minimize the coagulated PMMA particle itself during MMA shell polymerization. Encapsulated PMMA on $CaCO_3$ as inorganic/organic core-shell particles was verified by FT-IR and DSC analysis. It was found that the $CaCO_3$ was very well encapsulated by PMMA as shell. The surfaces were distinctly found as spindle shape and broad particle distribution after capsulation.

춘천에서 2002년 봄철 황사 발생기간 동안에 채취된 미세분진 중 무기성분의 특성 (Characteristics of Inorganic Components in Fine Particles Collected at Chunchon during the Springtime Yellow Sand Occurrence Period in 2002)

  • 김희갑;정경미;김동진;이종태
    • Environmental Analysis Health and Toxicology
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    • 제17권4호
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    • pp.333-339
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    • 2002
  • Yellow sand (YS) storms were observed about ten times in the Korean peninsula during March and April in 2002. Twenty four hour fine particle (PM$\_$2.5/) samples were collected onto the 47 mm Teflon - coated quartz filters over 9 days during and after the events using the MiniVol Portable Air Sampler at a flow rate of 5 liters per minute. The highest PM$\_$2.5/ concentration measured during the YS period was 289 $\mu\textrm{g}$/㎥, which is 13 times higher than the lowest of the values for the samples collected during the non-yellow sand period. The filter samples were analyzed for inorganic ions using the IC, AAS and Autoanalyzer, and for metals using the ICP-MS. The results showed that the concentrations of some inorganic ions (e.g., Ca$\^$2+/ and SO$_4$$\^$2-/) and metals (e.g., Fe, Mn) of soil origin were elevated during the yellow sand events.

Effect of $Al_{2}O_{3}$ filler addition on sintering behavior of low-firing $BaO-B_{2}O_{3}-ZnO$ glass ceramic system

  • Kim, Young-Nam;Kim, Byung-Sook;Lee, Joon-Hyung;Kim, Jeong-Joo
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2003년도 International Meeting on Information Display
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    • pp.814-817
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    • 2003
  • The sintering behavior of $BaO-B_{2}O_{3}-ZnO$, which is Pb-free glass-ceramic system, was examined as functions of the composition and the amount and particle size of $Al_{2}O_{3}$ filler. Different kinds of modifiers were added and $Al_{2}O_{3}$ fillers with different particle sizes ($1.5{\mu}m$ and $4.5{\mu}m$) were added. The glass frit-filler composites were sintered in the temperature range $520{\sim}580^{\circ}C$. X-ray diffraction results revealed that some of the composites crystallized during sintering. Dielectric constant and thermal expansion coefficient the glass-ceramics were analyzed.

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