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A STUDY ON THE ADHESION OF A SOFT LINER CONTAINING 4-META TO THE BASE METAL ALLOY AND ITS VISCOELASTIC PROPERTY

  • Park Hyun-Joo;Kim Chang-Whe;Kim Yung-Soo
    • The Journal of Korean Academy of Prosthodontics
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    • v.41 no.6
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    • pp.732-746
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    • 2003
  • Statement of problem. Soft lining materials, also referred to as tissue conditioning materials, tissue heating materials, relining materials, soft liners or tissue conditioners, were first introduced to dentistry by a plastic manufacturer in 1959. Since the introduction of the materials to the dental field, their material properties have been continually improved through the effort of many researchers. Soft lining materials have become widely accepted, particularly by prosthodontists, because of their numerous clinical advantages and ease of manipulation. Unfortunately, few reports have been issued upon the topic of increasing the bond strength between the base metal alloy used in cast denture bases and PMMA soft liner modified with 4-META, nor upon the pattern of debonding and material change in wet environment like a intra oral situation. Purpose. The purposes of this study were comparing the bond strength between base metal alloy used for the cast denture bases and PMMA soft liner modified with 4-META, and describing the pattern of debonding and material property change in wet environment like the intraoral situation. Material and Methods. This study consisted of four experiments: 1. The in vitro measurement of shear bond strength of the adhesive soft liner. 2. The in vitro measurement of shear bond strength of the adhesive soft liner after 2 weeks of aging. 3. A comparison of debonding patterns. 4. An evaluation the Relation time of modified soft liner. The soft liner used in this study was commercially available as Coe-soft (GC America.IL.,USA), which is provided in forms of powder and liquid. This is a PMMA soft liner commonly used in dental clinics. The metal primer used in this study was 4-META containing primer packed in Meta fast denture base resin (Sun Medical Co., Osaka, Japan). The specimens were formed in a single lap joint desist which is useful for evaluating the apparent shear bond strength of adhesively bonded metal plate by tensile loading. Using the $20{\times}20mm$ transparent grid, percent area of adhesive soft liner remaining on the shear area was calculated to classify the debonding patterns. To evaluate the change of the initial flow of the modified adhesive soft liner, the gelation time was measured with an oscillating rheometer (Haake RS150W/ TC50, Haake Co., Germany). It was a stress control and parallel plate type with the diameter of 35mm. Conclusion. Within the conditions and limitations of this study, the following conclusions were drawn as follows. 1. There was significant increase of bond strength in the 5% 4-META, 10% 4-META containing groups and in the primer coated groups versus the control group(P<0.05). 2. After 2 weeks of aging, no significant increase in bond strength was found except for the group containing 10% 4-META (P<0.05). 3. The gelation times of the modified soft liner were 9.3 minutes for the 5% 4-META containing liner and 11.5 minutes for the 10% 4-META liner. 4. The debonding patterns of the 4-META containing group after 2 weeks of aging were similar to those of immediaely after preparation, but the debonding pattern of the primer group showed more adhesive failure after 2 weeks of aging.

Design Approach for Boundary Element of Flexure-Governed RC Slender Shear Walls Based on Displacement Ductility Ratio (휨 항복형 철근콘크리트 전단벽의 경계요소설계를 위한 변위연성비 모델제시)

  • Mun, Ju-Hyun;Yang, Keun-Hyeok
    • Journal of the Korea Concrete Institute
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    • v.26 no.6
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    • pp.687-694
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    • 2014
  • This study established a displacement ductility ratio model for ductile design for the boundary element of shear walls. To determine the curvature distribution along the member length and displacement at the free end of the member, the distributions of strains and internal forces along the shear wall section depth were idealized based on the Bernoulli's principle, strain compatibility condition, and equilibrium condition of forces. The confinement effect at the boundary element, provided by transverse reinforcement, was calculated using the stress-strain relationship of confined concrete proposed by Razvi and Saatcioglu. The curvatures corresponding to the initial yielding moment and 80% of the ultimate state after the peak strength were then conversed into displacement values based on the concept of equivalent hinge length. The derived displacement ductility ratio model was simplified by the regression approach using the comprehensive analytical data obtained from the parametric study. The proposed model is in good agreement with test results, indicating that the mean and standard deviation of the ratios between predictions and experiments are 1.05 and 0.19, respectively. Overall, the proposed model is expected to be available for determining the transverse reinforcement ratio at the boundary element for a targeted displacement ductility ratio.

Properties of Engineering and Durability Concrete with Fly-ash and Blast Furnace Slag in Normal Strength Level (플라이애시 및 고로슬래그 첨가율에 따른 일반강도영역 콘크리트의 공학적 특성 및 내구성)

  • Kim, Gyu-Yong;Shin, Kyoung-Su;Lim, Chang-Hyuk;Nam, Jeong-Soo;Kim, Moo-Han
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.5 no.1
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    • pp.103-110
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    • 2010
  • Recently, reducing usage of cement and using by-product of industry such as blast furnace slag and fly-ash have been increased to reduce $CO_2$ gas emission. That apply to construction. As a result, reduction of environmental stress and recycling of resources are expected. In this study, as basic study to the reuse of resources and reduce Environmental Load, comparing and analyzing hardening characteristics and durability as using the blast furnace slag and fly-ash, examining concrete characteristics substituted the three elements for the blast furnace slag and fly-ash and evaluating the relationship as binder. Through this, it want to provide the basic data for mass utilization. Blast furnace slag powder and replaced at fly-ash compressive strength of concrete in the strength of the initial seven days material age lower level of expression significantly compared to the concrete, but, 28 days after the similar or higher compressive strength than the concrete expression of the was. In addition, the reserves replacement of blast furnace slag powder salt injury increasing resistance are seen improvements, according to the conventional blast furnace slag powder study by the chloride ions on the surface of the concrete are improved being fixation salt injury resistance is considered.

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Review of the Structural Shape for Aft Transition Ring of Submarine (잠수함 함미 트랜지션 링 구조 형상에 대한 고찰)

  • Oh, Dohan;Ahn, Namhyun
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.25 no.7
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    • pp.936-944
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    • 2019
  • Submarines, which have been called an invisible force, are strategic underwater weapon systems that perform missions such as anti-surface warfare, anti-submarine warfare, and high payoff target strikes with the advantage of underwater covertness. A submarine should be able to withstand the hydrostatic pressure of the deep sea. In this respect, the submarine pressure hull, as the main structural system to resist the external pressure corresponding to the submerged depth, should ensure the survivability from hazards and threats such as leakage, fires, shock, explosion, etc. To do this, the initial scantling of the submarine pressure hull must be calculated appropriately in the concept design phase. The shape of the aft transition ring varies according to its connection with the submarine aft end conical structure, pressure hull cylindrical part, and non-pressure hull of the submarine; the design of the aft transition ring should not only take into account stress flow and connectivity but also the cost increase due to the increased man-hours of its complex geometry. Therefore, trade-off studies based on the four different shapes of the aft transition ring are carried out considering both the review of the structural strength through nonlinear finite element analysis (FEA) and economic feasibility by reviewing the estimations of the manufacturing working days and material costs. Finally, the most rational structural aft transition ring shape for a submarine amongst four reviewed types was proposed.

FRACTURE STRENGTH BETWEEN DIFFERENT CONNECTOR DESIGNS OF ZIRCONIA CORE FOR POSTERIOR FIXED PARTIAL DENTURES MANUFACTURED WITH CAD/CAM SYSTEM (CAD/CAM을 이용한 구치부 전부도재 고정성 국소의치 지르코니아 코어의 연결부 설계에 따른 파절강도)

  • Seo Jun-Yong;Park In-Nim;Lee Keun-Woo
    • The Journal of Korean Academy of Prosthodontics
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    • v.44 no.1
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    • pp.29-39
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    • 2006
  • Statements of problem: Zirconia core is used for posterior fixed partial dentures because it's good mechanical properties. Stress is concentrated on connectors in fixed partial dentures, so the proper design of connector areas is needed for adequate mechanical long-term properties of any prosthesis. The area of connector is critical, but tooth size and surrounding soft tissue limit the connector design. Purpose: The purpose of this study is to compare fracture strengths between different connector designs of zirconia core for posterior fixed partial dentures manufactured with CAD/CAM system and determining the optimal connector design satisfying strength and hygiene. Material and method: The following four groups of 40 posterior fixed partial denture specimens(each group 10) were fabricated as followed; group 1 vertical height of connector is 3mm (control group, all groups have the same condition); group 2, lingual vertical 1mm reinforcement on connector; group 3, lingual vertical 2mm reinforcing on connector and group 4, lingual vertical 3mm reinforcing on connector. Specimens were subjected to compressive loading on the central fossa of pontic by instron. SEM was used to identify the initial crack and characterize the fracture mode. Results: The results were as follows: 1. The mean fracture load of the non-lingual reinforcing group was 1212N and the lingual vertical 1mm reinforcing group was 1510N, the lingual vertical 2mm reinforcing group was 1882N, the lingual vertical 3mm reinforcing group was 1980N. 2. The reinforcing groups were statistically significant compared to non-reinforcing groups(P<0.001). 3. There were 2, 3mm reinforcing groups that were statistically significant compared to 1mm reinforcing groups(P<0.001), and the 3mm reinforcing group was not statistically significant compared to 2mm reinforcing groups(P>0.05) 4. Fractures were initiated in gingival embrasures of connectors and processed to the loading site. Conclusion: In this study, lingual reinforcement of connector for improved strength of zirconia based fixed partial denture is nessasary. And long-term study for clinical application is required

Structural Behavior of RC Roof Slab under Cyclic Temperature Load (반복 일사하중에 대한 철근콘크리트 지붕슬래브의 구조적 거동)

  • Seo, Soo-Yeon;Yoon, Seung-Joe;Cho, Yong-Man;Choi, Gi-Bong
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.14 no.2
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    • pp.67-74
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    • 2010
  • A variation of temperature acting on a RC roof slab causes a change of stress in concrete since it expands during summer and is compressed during winter. This behavior repeats annually and makes an affection to the structural capacity of member for both serviceability and ultimate level. In this paper, a cyclic temperature loading variation is calculated by analyzing the weather data of Korea for 20 years. In addition, an experimental work is planned to find the long term effect of temperature variation. Six RC slab are made with same dimension. Test parameters are loading duration (10, 20, 30 year) and whether it has pre-damage or not. Observation of stiffness variations according to cyclic loading period shows that the serious stiffness drop happens after 10 year's cyclic loading at summer while after 30 year's loading at winter. From the fracture test about slabs damaged by long term cyclic loading, however, the capacity of member such as initial stiffness and maximum strength were not changed except yield strength according to the period of long term cyclic loading. The yield strength tends to decrease after 20 year's cyclic loading.

Enhanced Nitrate Uptake by Enterobacter amnigenus GG0461 at Alkaline pH (염기성 pH에서 Enterobacter amnigenus GG0461의 질산이온 흡수증가)

  • Choi, Tae-Keun;Kim, Sung-Tae;Han, Min-Woo;Kim, Young-Kee
    • Applied Biological Chemistry
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    • v.51 no.1
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    • pp.1-5
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    • 2008
  • Salt accumulation in soils of greenhouse due to the massive application of nitrogen fertilizers causes salt stress on the various crops, a serious problem in domestic agriculture. Since the majority of the salinity is nitrate, the excess nitrate should be removed; therefore, a bacterial strain having high capacity of nitrate uptake and identified as Enterobacter amnigenus GG0461 was isolated from the soils of greenhouse. Optimum conditions for the bacterial growth and nitrate uptake were investigated. GG0461 was able to grow without nitrate; however, nitrate facilitated the growth. The rate of nitrate uptake increased at alkaline pH and both growth and nitrate uptake were maximal at pH 8-9. When the initial pH of culture medium was increased to pH 8 or 9, it was decreased to neutral upon bacterial growth and nitrate uptake. These results imply that the major factor mediating bacterial nitrate uptake is a nitrate/proton antiporter. The fact was supported by the effect of nitrate addition in the absence of nitrate, since the addition of nitrate greatly increased the nitrate uptake and rapidly decreased pH of media.

Investigation of the Gene Encoding Isotocin and its Expression in Cinnamon Clownfish, Amphiprion melanopus (Cinnamon clownfish Amphiprion melnaopus의 이소토신 유전자 구조와 삼투압 조절이 미치는 영향)

  • Noh, Gyeong Eon;Choi, Mi-Jin;Min, Byung Hwa;Rho, Sum;Kim, Jong-Myoung
    • Journal of Life Science
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    • v.26 no.2
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    • pp.164-173
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    • 2016
  • Isotocin (IT), a nonapeptide homolog of oxytocin in mammals, has been suggested to be involved in physiological processes including social behaviors, stress responses, and osmoregulation in teleost fish. To study its structure and function, the gene encoding the IT precursor was cloned from the genomic DNA and brain cDNA of the cinnamon clownfish, Amphiprion melanopus. The IT precursor gene consists of three exons separated by two introns, and encodes an open reading frame of 156 amino acid (aa) residues, comprising a putative signal peptide of 19 aa, a mature IT protein of 9 aa, a proteolytic processing site of 3 aa, and 125 aa of neurophysin. Tissue-specific analysis of the IT precursor transcript indicated its expression in the brain and gonads of A. melanopus. To examine its osmoregulatory effects, the salinity of the seawater (34 ppt) used for rearing A. melanopus was lowered to 15 ppt. Histological analysis of the gills indicated the apparent disappearance of an apical crypt on the surface of the gill lamella of A. melanopus, as pavement cells covered the surface upon acclimation to the lower salinity. The level of Na+/K+-ATPase activity in the gills was increased during the initial stage of acclimation, followed by a decrease to its normal level, suggesting its involvement in osmoregulation and homeostasis. The only slight increase in the level of IT precursor transcript in the A. melanopus brain upon low-salinity acclimation suggested that IT played a minor role, if any, in the process of osmoregulation.

Effect of water potential of culture solution on water uptake, transpiration and photosynthesis of Panax ginseng (배양액(培養液)의 수분장력(水分張力)이 인삼(人蔘)의 수분흡수(水分吸收) 증산(蒸散) 및 광합성(光合成)에 미치는 영향(影響))

  • Mok, Sung-Kyun;Park, Hoon;Lee, Chong-Hwa;Son, Suk-Yeong
    • Korean Journal of Soil Science and Fertilizer
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    • v.13 no.4
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    • pp.115-118
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    • 1981
  • Effect of water potential of culture solution on photosynthesis, transpiration and water uptake was investigated using polyethylene glycol 6000. 1. Even at -0.5 bar of culture solution phothosynthesis was decreased by 20% within 1 hour. Plant in control showed 3.26% loss of initial water for 13 hours suggesting very sensitive in water uptake. 2. Relation between water potential of culture solution (${\psi}$) and water uptake amount (W) 2-year root was ${\psi}=-2.890/e^{2.796W}$ indicating that permanent wilting point will be greater than -2.89 bar. 3. Transpiration considerably decreased with the decrease of water potential and thus by 23.9% at -0.5 bar after 4 hours. 4. From the above results ginseng plant appears to have high root water potential at permanent wilting point and thus very week to water stress due to drought or high salt content in soils.

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Study on Flexural Properties of Polyamide 12 according to Temperature produced by Selective Laser Sintering (선택적 레이저 소결 제작 폴리아미드 12 시편의 온도별 굴곡 특성 연구)

  • Kim, Moosun
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.11
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    • pp.319-325
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    • 2018
  • The use of 3D printing (Additive Manufacturing) technology has expanded from initial model production to the mass production of parts in the industrial field based on the continuous research and development of materials and process technology. As a representative polymer material for 3D printing, the polyamide-based material, which is one of the high-strength engineering plastics, is used mainly for manufacturing parts for automobiles because of its light weight and durability. In this study, the specimens were fabricated using Selective Laser Sintering, which has excellent mechanical properties, and the flexural characteristics were analyzed according to the temperature of the two types of polyamide 12 and glass bead reinforced PA12 materials. The test specimens were prepared in the directions of $0^{\circ}$, $45^{\circ}$, and $90^{\circ}$ based on the work platform, and then subjected to a flexural test in three test temperature environments of $-25^{\circ}C$, $25^{\circ}C$, and $60^{\circ}C$. As a result, PA12 had the maximum flexural strength in the direction of $90^{\circ}$ at $-25^{\circ}C$ and $0^{\circ}$ at $25^{\circ}C$ and $60^{\circ}C$. The glass bead-reinforced PA12 exhibited maximum flexural strength values at all test temperatures in the $0^{\circ}$ fabrication direction. The tendency of the flexural strength changes of the two materials was different due to the influence of the plane direction of the lamination layer depending on the type of stress generated in the bending test.