• Title/Summary/Keyword: infiltration method

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RBSC Prepared by Si Melt Infiltration into the Y2O3 Added Carbon Preform (Y2O3 첨가 탄소 프리폼에 Si 용융 침투에 의해 제조한 반응 소결 탄화규소)

  • Jang, Min-Ho;Cho, Kyeong-Sik
    • Journal of Powder Materials
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    • v.28 no.1
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    • pp.51-58
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    • 2021
  • The conversion of carbon preforms to dense SiC by liquid infiltration is a prospectively low-cost and reliable method of forming SiC-Si composites with complex shapes and high densities. Si powder was coated on top of a 2.0wt.% Y2O3-added carbon preform, and reaction bonded silicon carbide (RBSC) was prepared by infiltrating molten Si at 1,450℃ for 1-8 h. Reactive sintering of the Y2O3-free carbon preform caused Si to be pushed to one side, thereby forming cracking defects. However, when prepared from the Y2O3-added carbon preform, a SiC-Si composite in which Si is homogeneously distributed in the SiC matrix without cracking can be produced. Using the Si + C → SiC reaction at 1,450℃, 3C and 6H SiC phases, crystalline Si, and Y2O3 were generated based on XRD analysis, without the appearance of graphite. The RBSC prepared from the Y2O3-added carbon preform was densified by increasing the density and decreasing the porosity as the holding time increased at 1,450℃. Dense RBSC, which was reaction sintered at 1,450℃ for 4 h from the 2.0wt.% Y2O3-added carbon preform, had an apparent porosity of 0.11% and a relative density of 96.8%.

Effect of Y2O3 Additive Amount on Densification of Reaction Bonded Silicon Carbides Prepared by Si Melt Infiltration into All Carbon Preform (완전 탄소 프리폼으로부터 Si 용융 침투에 의해 제조한 반응 소결 탄화규소의 치밀화에 미치는 Y2O3 첨가량의 영향)

  • Cho, Kyeong-Sik;Jang, Min-Ho
    • Korean Journal of Materials Research
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    • v.31 no.5
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    • pp.301-311
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    • 2021
  • The conversion of all carbon preforms to dense SiC by liquid infiltration can become a low-cost and reliable method to form SiC-Si composites of complex shape and high density. Reactive sintered silicon carbide (RBSC) is prepared by covering Si powder on top of 0.5-5.0 wt% Y2O3-added carbon preforms at 1,450 and 1,500℃ for 2 hours; samples are analyzed to determine densification. Reactive sintering from the Y2O3-free carbon preform causes Si to be pushed to one side and cracking defects occur. However, when prepared from the Y2O3-added carbon preform, an SiC-Si composite in which Si is homogeneously distributed in the SiC matrix without cracking can be produced. Using the Si + C = SiC reaction, 3C and 6H of SiC, crystalline Si, and Y2O3 phases are detected by XRD analysis without the appearance of graphite. As the content of Y2O3 in the carbon preform increases, the prepared RBSC accelerates the SiC conversion reaction, increasing the density and decreasing the pores, resulting in densification. The dense RBSC obtained by reaction sintering at 1,500 ℃ for 2 hours from a carbon preform with 2.0 wt% Y2O3 added has 0.20 % apparent porosity and 96.9 % relative density.

Enhanced Oxidation Resistance of LSI-Cf/SiC Composite by De-siliconization (탈규소화를 통한 LSI-Cf/SiC 복합재료의 내산화성 향상)

  • Jung Hwan Song;Jung Hoon Kong;Seung Yong Lee;Young Il Son;Do Kyung Kim
    • Journal of the Korean Society of Propulsion Engineers
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    • v.26 no.6
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    • pp.21-27
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    • 2022
  • Cf/SiC composites have low density, high mechanical strength, and good thermal stability, making them promising materials for high-temperature applications such as rocket propulsion and military fields. However, the remaining Si deteriorates physical and thermal properties. In this paper, the de-siliconization was introduced as a method to remove the Si of the Cf/SiC composite fabricated through Liquid Silicon Infiltration(LSI) process. The stability of composite has been tested under an oxyacetylene torch flame for up to 5 minutes. The oxidized surface and cross section of specimens were characterized by 3D scanning, X-ray diffraction(XRD), Optical microscope(OM) and Scanning electron microscope(SEM).

Preparation of Alumina Ceramics by Pressureless Powder Packing Forming Method: (I) Development of Pressureless Powders Packing Forming Method and Characterization of Green Body (무가압 분말 충전 성형법을 이용한 알루미나 세라믹스의 제조: (I) 무가압 분말 충전 성형법 개발 및 성형체 특성 관찰)

  • 박정현;성재석;이상진
    • Journal of the Korean Ceramic Society
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    • v.31 no.1
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    • pp.31-38
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    • 1994
  • To overcome the demerit of conventional forming method, new forming method, pressureless powder packing forming method, was investigated. This technique is performed by powder packing followed by the infiltration of binder solution. Various alumina powders were used as starting materials and the powders showing good packing condition through powder packing experiment were chosen. The green densities prepared by this new forming method with these powders were lower than those of specimens by pressing method, but, nearly same density was obtained in case of green body prepared with the powders having high packing density. The distribution of binder in a green body was homogeneous and it was possible to a complex shape form by this forming method.

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Artificial Groundwater Recharge by Underground Piping Method (지하관리에 의한 지하수함양 연구)

  • 안상진;이종형
    • Water for future
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    • v.23 no.2
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    • pp.239-250
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    • 1990
  • The method for artificial grondwater recharge can be categorized into two groups, one is well method and the other one is scattering method. Underground piping method belongs to the latter group and it is to infiltrate water from porous pipes buried underground. This paper shows the result of indoor experiment and numerical analysis concerning this method. The purpose of the study is to maky the infiltration aspects and groundwater recharge in underground piping method. We have found that the recharge height is effect by the difference of water level and a distance of pipe laying.

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Artificial Groundwater Recharge by Underground piping method (지하매관에 의한 지하수함양 연구)

  • 안상진;이종형
    • Proceedings of the Korea Water Resources Association Conference
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    • 1990.07a
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    • pp.61-79
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    • 1990
  • The method for artificial groundwater recharge can be categorized into two groups, one is well method and the other one is scattering method. Underground piping method belongs to the latter group and it is to infiltrate water from porous pipes buried underground. This paper shows the result of indoor experiment and numerical analysis concerning this method. The purpose of the study is to make the infiltration aspects and groundwater recharge in underground piping method. We have fround that the recharge height is effect by the difference of water level and a distance of pipe laying.

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Rehabilitation Priority Decision Model for Sewer Systems (하수관거시스템 개량 우선순위 결정 모형)

  • Lee, Jung-Ho;Park, Moo-Jong;Kim, Joong-Hoon
    • Journal of the Korean Society of Hazard Mitigation
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    • v.8 no.6
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    • pp.7-14
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    • 2008
  • The main objective of sewer rehabilitation is to improve its function while eliminating inflow/infiltration (I/I). If we can identify the amount of I/I for an individual pipe, it is possible to estimate the I/Is of sub-areas clearly. However, in real, the amount of I/I for an individual pipe is almost impossible to be obtained due to the limitation of cost and time. In this study, I/I occurrence of each sewer pipe is estimated using AHP (Analytic Hierarch Process) and RPDM (Rehabilitation Priority Decision Model for sewer system) was developed using the estimated I/I of each pipe to perform the efficient sewer rehabilitation. Based on the determined amount of I/I for an individual pipe, the RPDM determines the optimal rehabilitation priority (ORP) using a genetic algorithm for sub-areas in term of minimizing the amount of I/I occurring while the rehabilitation process is performed. The benefit obtained by implementing the ORP for rehabilitation of sub-areas is estimated by the only waste water treatment cost (WWTC) of I/I which occurs during the sewer rehabilitation period. The results of the ORP were compared with those of a numerical weighting method (NWM) which is the decision method for the rehabilitation priority in the general sewer rehabilitation practices and the worst order which are other methods to determine the rehabilitation order of sub-areas in field. The ORP reduced the WWTC by 22% compared to the NWM and by 40% compared to the worst order.

Slope Stability Analysis under Rainfall Condition by Using Multiple Slip Surfaces (다중 파괴면을 이용한 강우시 사면의 안정성 해석)

  • Kim, Minseok;Sagong, Myung;Kim, Soosam
    • Journal of the Korean GEO-environmental Society
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    • v.8 no.2
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    • pp.11-18
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    • 2007
  • Slope failure triggered by rainfall produces severe effects on the serviceability and stability of railway, Therefore, slope stability problem is one of the major concerns on the operation of railway. In this study, the rainfall conditions triggering slopes failure adjacent to railroads are investigated and the numerical analysis approach in consideration of infiltration and limit equilibrium method based upon multiple slip surfaces are proposed. The rainfall conditions triggering slope failure are as follow: cumulative rainfall is in the range of 150~500 mm, and duration is from 3 to 24 hours. Base upon the rainfall conditions, infiltration analysis and limit equilibrium method for infinite slope condition are carried out. The depth of infinite slope is assumed as 2 m and the multiple slip surfaces modeled with 16.7 cm interval from the bottom slip surface located at the 2 m depth. The assumed bottom slip surface is the location at which factor of safety is converging. The proposed approach shows more reasonable results than the results from the general codes assuming water table at slope surface. In addition, three dimensional plot of cumulative rainfall, rainfall duration, and factor of safety shows that slope stability analysis in consideration of rainfalll must account for cumulative rainfall (rainfall duration).

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Mechanical Properties and Wear Behaviour of $Al/SiC/Al_{2}O_{3}$ Composite Materials ($Al/SiC/Al_{2}O_{3}$복합재료의 기계적 성질 및 마멸특성)

  • 임흥준;김영한;한경섭
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.17 no.10
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    • pp.2498-2508
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    • 1993
  • $Al/SiC/Al_{2}O_{3}$ hybrid composites are fabricated by squeeze infiltration method. From the misconstructive of $Al/SiC/Al_{2}O_{3}$ hybrid composites fabricated by squeeze infiltration method, uniform distribution of reinforcements and good bondings are found. Hardness value of $Al/SiC/Al_{2}O_{3}$ hybrid composites increases linearly with the volume fraction of reinforcement because SiC whisker and $Al_{2}$O$_{3}$ fiber have an outstanding hardness. Optimal aging conditions are obtained by examining the hardness of $Al/SiC/Al_{2}O_{3}$ hybrid composites with different aging time. Tensile properties such as Young's modulus and ultimate tensile strength are improved up to 30% and 40% by the addition of reinforcements, respectively. Failure mode of $Al/SiC/Al_{2}O_{3}$ hybrid composites is ductile on microstructural level. Through the abrasive wear test and wear surface analysis, wear behaviour and mechanism of 6061 aluminum and $Al/SiC/Al_{2}O_{3}$ hybrid composites are characterized under various testing conditions. The addition of SiC whisker to $Al/SiC/Al_{2}O_{3}$ composites gives rise to improvement of the wear resistance. The wear resistance of $Al/SiC/Al_{2}O_{3}$ hybrid composites is superior to that of Al/SiC composites. The wear mechanism of aluminum alloy is mainly abrasive wear at low speed range and adhesive and melt wear at high speed range. In contrast, that of $Al/SiC/Al_{2}O_{3}$ hybrid composites is abrasive wear at all speed range, but severe wear when counter material is stainless steel. As the testing temperature increases, wear loss of aluminum alloy decreases because the matrix is getting more ductile, but that of $Al/SiC/Al_{2}O_{3}$ hybrid composites is hardly varied. Oil lubricant is more effective to reduce the wear loss of aluminum alloy and $Al/SiC/Al_{2}O_{3}$ hybrid composites at high speed range.

A Particle Tracking Method for the Lagrangian-Eulerian Finite Element Method in 3-D Subsurface System (3차원 지표하 시스템에서 Lagrangian-Eulerian 유한요소법에 대한 입자추적 알고리즘)

  • Lee, Jae-Young;Kang, Mee-A
    • The Journal of Engineering Geology
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    • v.19 no.2
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    • pp.205-215
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    • 2009
  • The conventional numerical models to analyze flow in subsurface porous media under the transient state usually generate numerical oscillation and unstability due to local flux domain for critical cases such as infiltration into initially dry soil during rainfall period. In this case, it is required refined mesh and small time step, but it decrease efficiency of computation. In this study, numerical unstability in discontinuity domain is removed by applying particle tracking algorithm to simulate unsteady subsurface flow with inflow boundary condition. Finally the hybrid LE FEM improving numerical stability is proposed. The hypothetical domains with unsteady uniform and nonuniform flow field were used to demonstrated algorithm verification. In comparison with analytic solution, we obtained reasonable results and conducted simulation of hypothetical 3-D recharge/pumping area. The proposed algorithm can simulate saturated/unsaturated porous media with more practical problems and will greatly contribute to accuracy and stability of numerical computation.