• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2018.06a
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• pp.110-110
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• 2018

여러 니켈합금 중 인코넬 600은 원전 가압경수로(PWR)의 튜브 재료로 널리 사용되는 재료이다. 스테인리스강과 비교하여 우수한 내식성과 기계적 특성으로 인해 화학설비, 발전설비, 그리고 해양설비 등과 같은 여러 산업분야에서도 널리 사용되고 있다. 그러나 가압경수로용 증기 발생기의 튜브 재료와 같은 특수 환경에서 예민화에 따른 입계부식 및 입계응력부식 등의 문제가 흔히 보고되고 있다. 이러한 내구성 문제는 설비 및 장비의 수명, 내구성 그리고 안정성 등의 치명적인 영향을 미친다. 따라서 용접, 열처리, 그리고 가공과정에서 발생하는 Inconel 600의 예민화 및 입계부식에 관한 연구가 활발히 진행되고 있다. 그러나 100시간 이상 장시간 열화된 시편에 대한 예민화 연구는 전무한 실정이다. 본 연구에서는 장시간 열화된 Inconel 600의 예민화를 평가하기 위해 최대 1,000시간까지 열화를 실시하였으며, 이에 대한 평가방법으로 Double-Loop Electrochemical Potentiokinetic Reactivation(DL-EPR) 시험법을 적용하였다. 본 실험에서 사용된 인코넬 600의 화학성분(wt, %)은 0.01 C, 0.05 Si, 0.14 Mn, 15.3 Cr, 0.5 Cu, 0.015 S, 그리고 나머지는 Ni 이다. 예민화 평가를 위한 등온 열화는 전기열처리로를 이용하여, $550^{\circ}C$와 $650^{\circ}C$에서 최대 1000시간까지 실시하였다. 열화에 따른 미세조직 변화는 scanning electron microscope와 energy dispersive x-ray spectroscopy를 이용하여 실시하였다. DL-EPR 실험은 $25^{\circ}C$의 0.1M $H_2SO_4$ + 0.001M KSCN(potasium thiocyanate) 수용액 하에서 실시하였으며, 분극은 OCP로부터 600 mV(SSE vs.)까지 1.67mV/s 주사속도로 forward scan을 실시 후, 동일한 속도로 OCP까지 reverse scan을 실시하였다. Degree Of Sensitization(DOS)값은 anodic scan peak($I_a$) 값과 reverse scan peak($I_r$) 값의 비로 산출하였다. $$i.e.\;DOS=I_r/I_a{\times}100$$. 그 결과, 온도 변수에 따른 Inconel 600강의 예민화 거동은 서로 상이한 경향을 나타내었다. $550^{\circ}C$의 경우, 열화가 진행됨에 따라 DOS값은 급격하게 증가하는 경향을 나타냈다. 반면, $650^{\circ}C$에서는 일정시간 이후부터 Cr 확산 현상에 의한 탈 예민화 현상이 관찰되었다.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2005.11a
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• pp.177-183
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• 2005

In this work, Inconel 600, Inconel 625 and Haynes 230 are welding using Nd:YAG laser and electron bear. These heat-resistant alloys are typically used for the liquid thruster. To examine, the affects of experimental parameters on weld ability, the plate welding of these materials were carried out using both Nd:YAG laser and electron bear. Also, the micro-structure, micro-hardness, and tensile strength of the specimens were analyzed. from the analysis of the experimental results of laser and electron beam welding, we have obtained the optimal welding conditions.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2004.04a
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• pp.203-208
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• 2004

The laser welding process is one of the most advanced manufacturing technologies owing to its high speed and deep penetration. Welding characteristics of Inconel 600 Alloy using a continuous wave Nd:YAG laser are experimentally investigated. The major process parameters studied in the present laser welding experiment were position of focus, laser power, travel speed. The gap and offset maintained as small as possible. Optical microscope were used to investigate the microstructures of the welded zone. The follow conclusions can be drawn the laser power and travel speed have a pronounced effect the fusion zone size and shape.

• Transactions of the Korean Society of Machine Tool Engineers
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• v.13 no.6
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• pp.119-126
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• 2004

The welding characteristics of Inconel 600 Alloy using a continuous wave Nd:YAG laser are experimentally investigated. The major process parameters studied in the present laser welding experiment were the positions of focus, laser power and travel speed of laser bean We measured the fusion zone size and its shape using an optical microscope for the observation of cross-sectional area. We performed two tests regarding the tension and the micro hardness for welding quality estimation. Then we measured residual stress in welds by electronic speckle pattern interferometry(ESPI). In conclusion the optimum butt welding process parameters were 0.5mm focus position, 1.6kW laser power, 1m/min travel speed and 5.5$\ell$/min assist gas discharge.

• Proceedings of the KWS Conference
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• 1998.10a
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• pp.288-291
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• 1998

Inconel 600 alloy is used as the material of nuclear steam generator tubing because of its mechanical properties, formability, and corrosion properties. According to reports, the life time of nuclear power plants decreases because of the pitting, intergranular attack, primary water stress corrosion cracking(PWSCC), and intergranular stress corrosion cracking(IGSCC), and denting in the steam generator. The SCC test is very important because of SCC appears in various environment such as solutions, materials, and stress. The C-Rig specimen was made of the steam generator welded sleeve repairing by the pulsed Nd:YAG laser. In the corrosion invironment, corrosion solutions are Primary Water, Caustic, and Sulfate solution and corrosion time is 1624-4877hr. The permitted stress is 30-60ksi.In this C-Ring SCC test is the relationship between corrosion depth, crack and corrosion environment is evaluated. SCC was happens in Sulfate and Corrosion solution but doesn't happen in Primary Water. The corrosion time and stress is very affected by the severely environment of Sulfate or Caustic solution. The microstructure observation indicates that SCC causes interganular failure in the grain boundary of vertical direction.

• Journal of the Korean institute of surface engineering
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• v.28 no.3
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• pp.133-141
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• 1995

The deposition characteristics of diamond films were investigated for three different substrates : Si, Inconel 600 and steel. Diamond films were prepared by microwave plasma CVD method using $CH_4$, $H_2$ and $O_2$ as reaction gases. The deposited films were analyzed with SEM, Raman spectroscopy and ellipsometer. For Si substrate, diamond films were successfully obtained for most of the deposition conditions used in this study. As the $CH_4$ flow rate decreased and the $O_2$ flow rate increased, the quality of the film was improved due to the reduced non-diamond phase in the film. For Inconel 600 substrate, the surface pretreatment with diamond powders was required to deposit a continuous diamond film. The films deposited at temperatures of $600^{\circ}C$ and $700^{\circ}C$ had mainly diamond phase, but they were peeled off locally due to the difference in the thermal expansion coefficient between the substrate and the deposited films. The films deposited at $500^{\circ}C$ and $850^{\circ}C$ had only the graphitic carbon phase. For steel substrate, all of the films deposited had only the graphitie carbon phase. We speculated that the formation of diamond nuclei on the steel substrate was inhibited due to the diffusion of carbon atoms into the steel substrate which has a large amount of carbon solubility.

• Proceedings of the Korean Magnestics Society Conference
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• 2004.12a
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• pp.181-182
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• 2004

• Proceedings of the Korean Magnestics Society Conference
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• 2004.06a
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• pp.236-237
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• 2004

• Proceedings of the Korean Nuclear Society Conference
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• 1996.05d
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• pp.455-460
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• 1996

원자력발전소의 전열관 보수용접 기술 개발을 위해 Inconel 600 재질의 plate 판에 레이저 용접실험을 수행하였다. 레이저 발진기로 부터 발진된 레이저 빔은 광섬유를 통하여 전송되고, 집광렌즈군를 이용하여 용접이 이루어지도록 하였다. pulse 레이저 용접 변수인 펄스폭, 반복율, 첨두출력 및 용접속도를 변화시키면서 용접결과를 측정하였다. 이에 따른 적절한 용접범위를 제시하였다.

• Korean Journal of Materials Research
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• v.11 no.10
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• pp.841-845
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• 2001

The steam generator tubes of power plant damaged by sliding wear due to flow-induced motion of foreign object. Amount of wear have been predicted by Achard's wear equation until now. However, there are large error and low reliability, because this equation regards wear coefficient(k) as constant. The sliding wears tests have been performed at room temperature to examine parameters of wear (wear distance, contact stress). The steam generator tube material for wear test is used Inconel 600 and foreign object material is used 304 austenite stainless steel. The sliding wear tests show that the amount of wear is not linearly proportional to the wear distance(for 374 austenite stainless steel). According to experimental result, wear coefficient is not constant k but function k(s) of wear distance. The newly modified wear predictive equation V=k(s)F have small error and high reliability.