• 제목/요약/키워드: in-situ process

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다중압출 공정을 이용한 마이크로 채널 다중 원통형 고체산화물 연료전지의 in-situ 제조 (In-Situ Fabrication of Micro-channeled Multi Tubular Solid Oxide Fuel Cell using Multi-pass Extrusion Process)

  • 변기천;;김종희;이병택
    • 한국재료학회지
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    • 제17권6호
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    • pp.313-317
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    • 2007
  • In-situ micro-channeled multi tubular solid oxide fuel cell(SOFC) was fabricated using multi-pass extrusion process with out side diameter of 2.7 mm and active length of 5 mm that contained 61 individual cells. Cell materials used in this work were NiO-YSZ (50 : 50 vol.%), 8 mol% yttria-stabilized zirconia(8YSZ), $La_{0.8}Sr_{0.2}MnO_3(LSM)$ as anode, electrolyte, and cathode, respectively. The arrangement of each electrode and electrolyte layer in green bodies showed uniformity and integrity after extrusion and sintering. The XRD analysis confirmed that no reaction phases appeared and the microstructure of the electrolyte was fairly dense (relative density > 96%) after sintering.

In situ analysis of chemical components induced by steaming between fresh ginseng, steamed ginseng, and red ginseng

  • In, Gyo;Ahn, Nam-Geun;Bae, Bong-Seok;Lee, Myoung-Woo;Park, Hee-Won;Jang, Kyoung Hwa;Cho, Byung-Goo;Han, Chang Kyun;Park, Chae Kyu;Kwak, Yi-Seong
    • Journal of Ginseng Research
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    • 제41권3호
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    • pp.361-369
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    • 2017
  • Background: The chemical constituents of Panax ginseng are changed by processing methods such as steaming or sun drying. In the present study, the chemical change of Panax ginseng induced by steaming was monitored in situ. Methods: Samples were separated from the same ginseng root by incision during the steaming process, for in situ monitoring. Sampling was sequentially performed in three stages; FG (fresh ginseng) ${\rightarrow}$ SG (steamed ginseng) ${\rightarrow}$ RG (red ginseng) and 60 samples were prepared and freeze dried. The samples were then analyzed to determine 43 constituents among three stages of P. ginseng. Results: The results showed that six malonyl-ginsenoside (Rg1, Rb1, Rb3, Rc, Rd, Rb2) and 15 amino acids were decreased in concentration during the steaming process. In contrast, ginsenoside-Rh1, 20(S)-Rg2, 20(S, R)-Rg3 and Maillard reaction product such as AF (arginine-fructose), AFG (arginine-fructose-glucose), and maltol were newly generated or their concentrations were increased. Conclusion: This study elucidates the dynamic changes in the chemical components of P. ginseng when the steaming process was induced. These results are thought to be helpful for quality control and standardization of herbal drugs using P. ginseng and they also provide a scientific basis for pharmacological research of processed ginseng (Red ginseng).

Utilizing Advanced Pad Conditioning and Pad Motion in WCMP

  • Kim, Sang-Yong;Chung, Hun-Sang;Park, Min-Woo;Kim, Chang-Il;Chang, Eui-Goo
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 추계학술대회 논문집 Vol.14 No.1
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    • pp.171-175
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    • 2001
  • Chemical mechanical polishing(CMP) process has been widely used to planarize dielectrics and metal, which can apply to employed in integrated circuits for sub-micron technology. Despite the increased use of CMP process, it is difficult to accomplish the global planarization of free-defects in inter level dielectrics and metal. Especially, defects like (micro-scratch) lead to severe circuit failure, and affects yield. Current conditioning method - bladder type, orbital pad motion- usually provides unsuitable pad profile during ex-situ conditioning near the end of pad life. Since much of the pad wear occurs by the mechanism of bladder type conditioning and its orbital motion without rotation, we need to implement new ex-situ conditioner which can prevent abnormal regional force on pad caused by bladder-type and also need to rotate the pad during conditioning. Another important study of ADPC is related to the orbital scratch of which source is assumed as diamond grit dropped from the strip during ex-situ conditioning. Scratch from diamond grit damaged wafer severely so usually scraped. Figure 1 shows the typical shape of scratch damaged from diamond. e suspected that intensive forces to the edge area of bladder type stripper accelerated the drop of Diamond grit during conditioning. so new designed Flat stripper was introduced.

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진공 환경내 실시간 입자 모니터링 시스템의 개발 및 성능평가 (Development and Performance Test of In-situ Particle Monitoring System using Ion-counter in Vacuum Environments)

  • 안강호;김용민;권용택
    • 반도체디스플레이기술학회지
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    • 제5권1호
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    • pp.45-49
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    • 2006
  • In this paper, a new method that monitors the quantity of particles using ion-counter in vacuum environment is introduced. In-situ particle monitoring (ISPM) system is composed by Gerdien type ion-counter (house-made), DC power supply and electrometer. The ion-counter applied by positive voltage detects only positive charged particles. Therefore the particles to be detected should be in known charge state for further data analysis. ion-counter is installed at the exhaust line of process equipment where the pressure loss is structurally low. ISPM system performance has been verified with SMPS (Scanning Mobility Particle Sizer) system. The correlation coefficient is above 0.98 at the particle size range of $20{\sim}300nm$ in diameter with identified charge distribution under $0.1{\sim}10.0$ Torr.

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현장조건을 고려한 PVDs의 압밀도 산정에 관한 연구 (A Study on the PVDs Consolidation Degree Considering In-Situ Conditions)

  • 신은철;박정준;권형택
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2006년도 춘계 학술발표회 논문집
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    • pp.824-827
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    • 2006
  • The Prefabricated Vertical Drains (PVDs) method is one of the most widely used techniques to accelerate the consolidation process in-situ and hence increase its bearing capacity. In this paper, the degree of consolidation incorporated with PVDs was evaluated in O construction work site which composed with dredged soil. O Program PVD(Version 2.3) which developed by Asian Institute of Technology was used. The purpose of this analysis is efficiently to estimate the degree of consolidation by analyzing the surface settlement with time, and drainage at initial stage and final stage by using design-parameter which based on the in-situ tests and laboratory tests. This result can be compared with analysis of the degree of consolidation using Program PVD(Version 2.3) and the field observed data in the future studies.

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Feasibility study of an earth-retaining structure using in-situ soil with dual sheet piles

  • An, Joon-Sang;Yoon, Yeo-Won;Song, Ki-Il
    • Geomechanics and Engineering
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    • 제16권3호
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    • pp.321-329
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    • 2018
  • Classic braced walls use struts and wales to minimize ground movements induced by deep excavation. However, the installation of struts and wales is a time-consuming process and confines the work space. To secure a work space around the retaining structure, an anchoring system works in conjunction with a braced wall. However, anchoring cannot perform well when the shear strength of soil is low. In such a case, innovative retaining systems are required in excavation. This study proposes an innovative earth-retaining wall that uses in situ soil confined in dual sheet piles as a structural component. A numerical study was conducted to evaluate the stability of the proposed structure in cohesionless dry soil and establish a design chart. The displacement and factor of safety of the structural member were monitored and evaluated. According to the results, an increase in the clearance distance increases the depth of safe excavation. For a conservative design to secure the stability of the earth-retaining structure in cohesionless dry soil, the clearance distance should exceed 2 m, and the embedded depth should exceed 40% of the wall height. The results suggest that the proposed method can be used for 14 m of excavation without any internal support structure. The design chart can be used for the preliminary design of an earth-retaining structure using in situ soil with dual steel sheet piles in cohesionless dry soil.

유-무기 하이브리드 화합물과 Particle-Binder 공정을 이용한 소수성 코팅막 제조 (Preparation of Hydrophobic Coating Layers Using Organic-Inorganic Hybrid Compounds Through Particle-to-Binder Process)

  • 황승희;김효원;김주영
    • 접착 및 계면
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    • 제21권4호
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    • pp.143-155
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    • 2020
  • Sol-Gel 공정을 통해서 제조되는 유-무기 하이브리드 화합물들은 방청 코팅, 방빙 코팅(Anticing), 자가 세정 코팅, 반사 방지 코팅 등과 같은 기능성 코팅 재료로 널리 사용되어져 왔다. 특히 소수성 코팅 표면을 제조하기 위해서는 코팅표면의 표면에너지가 낮고 코팅 표면의 조도를 제어가 요구된다. 표면에너지와 표면 조도를 조절하는 전형적인 공정은 in-situ fabrication 공정, 'Pre-fluorinating/Post-roughening', 'Pre-roughening/ Post-fluorinating이다. 본 연구에서는 in-situ fabrication 공정인 Particle-Binder 공정을 이용해서 소수성 코팅표면을 제조하였다. 3관능기 유기실란화합물과 불소 함유 유기실란 화합물과의 가수분해 및 축합반응을 통해 제조된 불소함유 유-무기 하이브리드를 바인더로 사용하여서 무기물 나노입자와 혼합하여 소수성 코팅액을 제조하고 유리 기재 위에 스핀코팅 후 열건조하여서 코팅막을 제조하였다. 바인더인 유-무기 하이브리드 화합물의 불소 함유 실란화합물의 첨가량, 첨가순서, 무기물 나노입자 첨가량에 따른 코팅막의 물성 변화를 조사하였다. 분석결과 불소 함량이 10 wt%인 유-무기 하이브리드 화합물(GPTi-HF10)을 바인더로 사용하여서 제조된 코팅막이 가장 소수성이 우수하였으며 수접촉각은 (107.52 ± 1.6°), 이 바인더와 무기물 나노입자의 무게비가 1:3인 경우(GPTi-HF10-MS 3.0)에 가장 높은 수접촉각(130.84±1.99°)을 나타내었다.